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High strength Al-Cu-Mg based alloy with synchronous improved tensile properties and hot-cracking resistance suitable for laser powder b e d fusion

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Journal of Materials Science & Technology 2023年第10期141卷 155-170页

作者： Q.Z.wang N.Kang X.Lin M.EL Mansori w.d.huang State Key Laboratory of Solidification Processing Northwestern Polytechnical UniversityXi’an 710072China Arts et Metiers Institute of Technology MSMPHESAM UniversitéChâlons-en-Champagne F-51006France Key Laboratory of Metal High Performance Additive Manufacturing and Innovative design MIIT ChinaNorthwestern Polytechnical UniversityXi’an 710072China Texas A&M Engineering Experiment Station Institute for Manufacturing SystemsCollege StationTX 77843USA

In present work,a novel crack-free Al-Cu-Mg-Si-Ti alloy with synchronous improved tensile properties and hot-cracking resistance was proposed and successfully manufactured by laser powder bed fusion(LPBF).The microstructure evolution behaviors and the corresponding strengthening mechanisms were investigated in *** LPBF-processed Al-Cu-Mg-Si-Ti alloy presents a heterogeneous microstructure consisting of ultrafine equiaxed grains(UFGs)at the boundary and coarse columnar grains(CGs)at the center of the single molten ***-precipitated d022-Al 3 Ti particles were found to act as the nuclei to refine the grains at the boundary of the molten pool during solidification process,which is attributed to the low cooling rate providing the sufficient incubation time for the precipitation of d022-Al 3 *** are two orientation relationships(ORs)betweenα-Al and d022-Al 3 Ti,i.e.[001]α-Al//[001]d022-Al3Ti,(200)α-Al//(200)d022-Al3Ti and[1¯1¯2]α-Al//[¯111]d022-Al3Ti,(1¯11)α-Al//(¯11¯2)d022-Al3Ti,which are two of the eight ORs predicted with the E2EM *** grains in present alloy,no matter for UFGs or CG,exhibited high critical hot-cracking stress,which means a strong hot-cracking ***-nanoprecipitation of Cu-,Mg-,and Si-rich Q’and S’phases was introduced to enhance the mechanical performance ofα-Al *** as-built sample exhibits superior tensile properties,with the yield strength(YS)of 473±8 MPa,ultimate tensile strength(UTS)of 541±2 MPa and elongation(EI)of 10.9%±1.2%.

关键词： Laser powder bed fusion High strength Al-Cu-Mg alloys duplex microstructure Precipitation Tensile properties

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Microstructure evolution and mechanical properties at high temperature of selective laser melted AlSi10Mg

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Journal of Materials Science & Technology 2021年第3期62卷 162-172页

作者： Y.Cao X.Lin Q.Z.wang S.Q.Shi L.Ma N.Kang w.d.huang State Key Laboratory of Solidification Processing Northwestern Polytechnical UniversityXi’an 710072China Key Laboratory of Metal High Performance Additive Manufacturing and Innovative design MIIT ChinaNorthwestern Polytechnical UniversityXi’an 710072China

In this study,the microstructure and tensile properties of selective laser melted AlSilOMg at elevated temperature were investigated with focus on the interfacial ***-situ SEM and in-situ EBSd analysis were proposed to characterize the microstructural evolution with *** as-fabricated AlSilOMg sample presents high tensile strength with the ultimate tensile strength(UTS)of~450 MPa and yield strength(YS)of~300 MPa,which results from the mixed strengthening mechanism among grain boundary,solid solution,dislocation and Orowan looping *** holding at the temperature below 200℃for 30 min,the micro structure presents little change,and only a slight decrement of yield strength appears due to the relief of the residual ***,when the holding temperature further increases to 300℃and 400℃,the coarsening and precipitation of Si particles inα-Al matrix occur obviously,which leads to an obvious decrease of solid solution *** the same time,matrix softening and the weakness of dislocation strengthening also play important *** the holding temperature reaches to 400℃,the yield strength decreases significantly to about 25 MPa which is very similar to the as-cast Al *** might be concluded that the YS is dominated by the matrix *** the softening mechanism counteracts work hardening,the extremely high elongation occurs.

关键词： Selective laser melting AlSi10Mg Microstructure In-situ EBSd High temperature tensile property

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CELLULAR SPACING SELECTION OF Al-0.53wt%Zn ALLOY UNdER NEAR-RAPId dIRECTIONAL SOLIdIFICATION CONdITION

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Acta Metallurgica Sinica(English Letters) 1998年第5期11卷 320-324页

作者： J.Feng w.d.huang X.Lin T.Li Y.F.Xue Y.H.Zhou Northwestern Polytechnical Univ Xi'an China

In order to investigate the response of cellular spacing to the variation of growth velocity under near-rapid directional solidification condition, Al-0.53wt%Zn alloy is directionally solidified with Bridgman apparatus. The results show that at the given temperature gradient the obtained microstrvctures are all cells and there exists a wide distribution range of cellular spacing. The maximum, λmax, minimum, λmin, and average cellular spacing, λ, as functions of growth rate, V, can be given by λmax=948.51V-0.4961, λmin= 661.16V-0.5015 and λ=412.41V-0.5049, respectively. The experimental results are compared with that predicted by KGT model, and a good agreement is found. Moreover,it is found that the average cellular spacing is also remarkably history-dependent.

关键词： Al-Zn alloy near-rapid directional solidification cellular spacing history-dependence

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Microstructural features of Ti-6Al-4V manufactured via high power laser directed energy deposition under low-cycle fatigue

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Journal of Materials Science & Technology 2021年第24期83卷 18-33页

作者： Y.M.Ren X.Lin H.O.Yang H.Tan J.Chen Z.Y.Jian J.Q.Li w.d.huang School of Materials and Chemical Engineering Xi’an Technological UniversityXi’an710021China State Key Laboratory of Solidification Processing Northwestern Polytechnical UniversityXi’an710072China

Laser additive manufacturing(LAM)technique has unique advantages in producing geometrically complex metallic ***,the poor low-cycle fatigue property(LCF)of LAM parts restricts its widely ***,the microstructural features of a Ti-6 Al-4 V alloy manufactured via high power laser directed energy deposition subjected to low-cycle fatigue loading were *** fatigue loading,the microstructure of the as-deposited parts was found to exhibit a non-homogeneous distribution of columnar prior-βgrains(200-4000μm)at various scanning velocities(300-1500 mm/min)and relatively coarseα-laths(1.0-4.5μm).Under cyclic loading,fatigue microcracks typically initiated within the alignedαphases in the preferred orientation(45°to the loading direction)at the surface of the fatigue *** Ti-6 Al-4 V exhibited a single straight dislocation character at low strain amplitudes(d dislocation dipoles or even tangled dislocations at high strain amplitudes(>1.1%).In addition,dislocation substructure features,such as dislocation walls,stacking faults,and dislocation networks,were also *** findings may provide opportunities to understand the fatigue failure mechanism of additive manufactured titanium parts.

关键词： Laser additive manufacturing directed energy deposition Titanium alloy Low-cycle fatigue Microstructure

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Carbene chemistry for unnatural biosynthesis

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Science China(Life Sciences) 2024年第1期67卷 204-207页

作者： Jing huang Jay d.Keasling department of Chemical and Biomolecular Engineering University of CaliforniaBerkeley 94720USA Joint BioEnergy Institute Lawrence Berkeley National LaboratoryEmeryville 94608USA Biological Systems and Engineering division Lawrence Berkeley National LaboratoryBerkeley 94720USA Novo Nordisk Foundation Center for Biosustainability Technical University of DenmarkKongens Lyngby 2800Denmark department of Bioengineering University of CaliforniaBerkeley 94720USA Synthetic Biochemistry Center Institute for Synthetic BiologyShenzhen Institutes for Advanced TechnologiesShenzhen 518055China

Previously,chemists working in synthesis were jealous of biologists since the enzymes found in nature usually exhibited great catalytic properties(e.g.,high catalytic efficiency,excellent selectivity such as substrate selectivity,regioselectivity and stereoselectivity).However,biological systems lack many counterparts of reactions widely used in chemical synthesis.

关键词： synthesis selectivity catalytic

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THE MULTI-LAYER LASER CLAddING OF Ni60 ALLOY

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Acta Metallurgica Sinica(English Letters) 1999年第5期12卷 1025-1028页

作者： Y.M.Li,w.d.huang,L.P.Feng and J.Chen State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi’an 710072, China

The Multi layer coating of Ni60 alloy was got by multi layer laser cladding. The height of the coating was about 12mm and the wall of the coating was perpendicular to the base. The microstructure of the coating was ... 详细信息

关键词： laser near net shaping multi layer laser cladding Ni60 alloy

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A thermodynamic perspective on electrode poisoning in solid oxide fuel cells

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International Journal of Minerals,Metallurgy and Materials 2024年第6期31卷 1449-1455页

作者： Kevin huang department of Mechanical Engineering University of South CarolinaColumbiaUSA

A critical challenge to the commercialization of clean and high-efficiency solid oxide fuel cell(SOFC)technology is the insuf-ficient stack lifespan caused by a variety of degradation mechanisms,which are associated with cell components and chemical *** components related degradation refers to thermal/chemical/electrochemical deterioration of cell materials under operating conditions,whereas the latter regards impurities in feedstocks of oxidant(air)and reductant(fuel).This article provides a thermodynamic perspective on the understanding of the impurities-induced degradation mechanisms in *** discussion focuses on using thermodynamic ana-lysis to elucidate poisoning mechanisms in cathodes by impurity species such as Cr,CO_(2),H_(2)O,and SO_(2) and in the anode by species such as S(or H_(2)S),SiO_(2),and P_(2)(or PH_(3)).The author hopes the presented fundamental insights can provide a theoretical foundation for search-ing for better technical solutions to address the critical degradation challenges.

关键词： impurities air fuel reaction activity

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Responses of growth performance,antioxidant function,small intestinal morphology and mRNA expression of jejunal tight junction protein to dietary iron in yellow-feathered broilers

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Journal of Integrative Agriculture 2024年第4期23卷 1329-1337页

作者： Kaiwen Lei Hao wu Jerry w Spears Xi Lin Xi wang Xue Bai Yanling huang Key Laboratory of Animal Science of State Ethnic Affairs Commission Southwest Minzu UniversityChengdu 610041China Key Laboratory of Qinghai-Tibetan Plateau Animal Genetic Resource Reservation and Utilization Southwest Minzu UniversityChengdu 610041China department of Animal Science North Carolina State UniversityRaleighNC 27695-7621USA

This study aimed to investigate the dose-effect of iron on growth performance,antioxidant *** morphology,and mRNA expression of jejunal tight junction protein in 1-to21-d-old yellow-feathered broilers.A total of 7201-d-old yellow-feathered maleb roilers were allocated to 9 treatments with 8 replicate cages of 10 birds per *** dietary treatments were consisted of a basal diet(contained 79.6 mg Fe kg^(-1))supplemented with 0,20,40,60,80,160,320,640,and 1,280 mg Fe kg^(-1)in the form of FeSO_(4)·7H_(2)*** with the birds in the control group,birds supplemented with 20mg Fe kg^(-1)had higher average daily gain(AdG)(Pdding 640 and 1,280 mg Fe kg^(-1)significantly decreased AdG(Pd average daily feed intake(AdFI)(Pd with supplementation of 20mg Fe kg^(-1).Malondialdehyde(MdA)concentration in plasma and duodenum increased linearly(PdA concentration in liver and jejunum increased linearly(Pdratically(Pwith increased dietary Fe *** villus height(VH)in duodenum and jejunum,and the ratio of villus height to crypt depth(V/C)in duodenum decreased linearly(P?0.05)as dietary *** dietary Fe increased,the jejunal relative mRNA abundance of claudin-1 decreased linearly(P=0.001),but the jejunal relative mRNA abundance of zona occludens-1(ZO-1)and occludin decreased linearly(P?0.05)or quadratically(P?0.05).Compared with the supplementation of 20 mg Fe kg^(-1),the supplementation of640 mg Fe kg^(-1)or higher increased(P?0.05)MdA concentrations in plasma,duodenum,and jejunum,decreased VH in the duodenum and jejunum,and the addition of 1,280 mg Fe kg^(-1)reduced(P?0.05)the jejunal tight junction protein(claudin-1,ZO-1,occludin)mRNA *** summary,640 mg of supplemental Fe kg^(-1)or greater was associated with decreased growth performance,increased oxidative stress,disrupted intestinal morphology,and reduced mRNA expression of jejunal tight junction protein.

关键词： iron yellow-feathered broiler antioxidant function intestinal morphology tight junction protein

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Sintering of phosphor-glass composites goes ultrafast

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Science China Materials 2024年第8期67卷 2711-2712页

作者： Xiaoyong huang College of Electronic Information and Optical Engineering Taiyuan University of TechnologyTaiyuan 030024China

Nowadays,with the rapid technological progress of high-quality lightings and high-end displays,high-power white light-emitting diodes(wLEds)and high-brightness white laser diodes(wLds)featuring with high energy density excitation,high output power and high device stability have been extensively investigated and regarded as the new-generation solid-state light sources[1–6].

关键词： diodes wLEd white

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A theory for three-dimensional response of micropolar plates

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Applied Mathematics and Mechanics(English Edition) 2024年第8期45卷 1403-1414页

作者： dianwu huang Linghui HE College of Civil Engineering and Architectural Jiaxing University department of Modern Mechanics and State Key Laboratory of Fire Science University of Science and Technology of China

Through combined applications of the transfer-matrix method and asymptotic expansion technique, we formulate a theory to predict the three-dimensional response of micropolar plates. No ad hoc assumptions regarding through-thickness assumptions of the field variables are made, and the governing equations are two-dimensional, with the displacements and microrotations of the mid-plane as the unknowns. Once the deformation of the mid-plane is solved, a three-dimensional micropolar elastic field within the plate is generated, which is exact up to the second order except in the boundary region close to the plate edge. As an illustrative example, the bending of a clamped infinitely long plate caused by a uniformly distributed transverse force is analyzed and discussed in detail.

关键词： 74H45 asymptotic expansion micropolar plate O341 three-dimensional response transfer-matrix

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