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Progress in non-invasive detection of liver fibrosis

Cancer Biology & Medicine 2018年第2期15卷 124-136页

作者： Chengxi li rentao li Wei Zhang Department of Mechanical Engineering Massachusetts Institute of TechnologyCambridgeMA 02139USA Department of Hepatobiliary Surgery Tianjin Medical University Cancer Institute and HospitalNational Clinical Research Center for CancerKey Laboratory of Cancer Prevention and TherapyTianjin Tianjin's Clinical Research Center for Cancer Tianjin 300060China

liver fibrosis is an important pathological precondition for hepatocellular *** degree of hepatic fibrosis is positively correlated with liver *** fibrosis is a series of pathological and physiological process related to liver cell necrosis and degeneration after chronic liver injury,which finally leads to extracellular matrix and collagen *** early detection and precise staging of fibrosis and cirrhosis are very important for early diagnosis and timely initiation of appropriate therapeutic *** risk of severe liver fibrosis finally progressing to liver carcinoma is＆gt;50%.It is known that biopsy is the gold standard for the diagnosis and staging of liver ***,this method has some limitations,such as the potential for pain,sampling variability,and low patient ***,the necessity of obtaining a tissue diagnosis of liver fibrosis still remains *** increasing number of reliable non-invasive approaches are now available that are widely applied in clinical practice,mostly in cases of viral hepatitis,resulting in a significantly decreased need for liver *** fact,the noninvasive detection and evaluation of liver cirrhosis now has good accuracy due to current serum markers,ultrasound imaging,and magnetic resonance imaging quantification techniques.A prominent advantage of the non-invasive detection and assessment of liver fibrosis is that liver fibrosis can be monitored repeatedly and easily in the same *** biomarkers have the advantages of high applicability（〉95%）and good ***,their results can be influenced by different patient conditions because none of these markers are *** most promising techniques appear to be transient elastography and magnetic resonance elastography because they provide reliable results for the detection of fibrosis in the advanced stages,and future developments promise to increase the reliability and accuracy of the stag

关键词： liver fibrosis non-invasive detection computer-aided quantitative deep learning

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优化碱酸法提纯石墨的研究

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中国粉体技术 2024年第3期30卷 76-87页

作者：刘云泽孟繁荣崔学民王林杰何振全李仁涛盖国胜广西大学化学化工学院广西南宁530004 清华大学无锡应用技术研究院江苏无锡214100 山东省粉体材料中试示范基地山东东营257061 山东石油化工学院化学工程学院山东东营257061 淄博清大粉体材料工程有限公司山东淄博255086

【目的】优化天然石墨提纯效果,降低酸在提纯过程中的过多使用对环境造成的影响,满足各行各业对高品质石墨的需求,实现更环保、高效的石墨提纯。【方法】以鳞片石墨为原料,采取NaOH-HCl-HF联合处理的工艺对石墨进行提纯研究,提高石墨的... 详细信息

【目的】优化天然石墨提纯效果,降低酸在提纯过程中的过多使用对环境造成的影响,满足各行各业对高品质石墨的需求,实现更环保、高效的石墨提纯。【方法】以鳞片石墨为原料,采取NaOH-HCl-HF联合处理的工艺对石墨进行提纯研究,提高石墨的固定碳含量(质量分数,下同),降低石墨中的主要杂质元素如Si、Fe、Al、Cu等的含量,详细考察NaOH的用量以及焙烧温度2个关键因素对该工艺提纯效果的影响;通过扫描电子显微镜(SEM)观察石墨形貌特征,X射线荧光光谱仪(XRF)和电感耦合等离子体原子发射光谱仪(ICP)测定提纯处理前后石墨的杂质含量,X射线衍射仪(XRD)确定石墨及其灰分的晶体结构。【结果】当焙烧温度为500℃、焙烧时间为2.5h,HCl的体积与石墨的质量比为2∶1,氢氟酸的体积与石墨的质量比为2∶1时,石墨的平均固定碳含量从原来的95.3%提高到99.93%;当NaOH与石墨的质量比分别为0.5∶1和0.6∶1时,石墨的平均固定碳含量为99.91%和99.93%;考虑到成本效益等因素,确定当NaOH与石墨的质量比设定为0.5∶1时为理想工艺条件;经过提纯处理后的石墨层结构并不会出现明显的变化,基本性能不变,提纯处理后的石墨相比于提纯处理前的石墨,杂质含量明显地降低。【结论】该碱酸工艺不仅能有效地去除石墨中的杂质,盐酸和氢氟酸的组合还可以显著地提升提纯效果,可有望应用在石墨提纯处理和新能源材料领域。

关键词：石墨碱酸法加碱焙烧固定碳纯化

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Expansion and improvement of ChinaMu by MuT-seq and chromosome-level assembly of the Mu-starter genome

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Journal of Integrative Plant Biology 2024年第4期66卷 645-659页

作者： Lei liang Yuancong Wang Yanbin Han Yicong Chen Mengfei li Yibo Wu Zeyang Ma Han Zhao rentao Song State Key Laboratory of Maize Bio-breeding Frontiers Science Center for Molecular Design BreedingJoint International Research Laboratory of Crop Molecular BreedingNational Maize Improvement CenterCollege of Agronomy and BiotechnologyChina Agricultural UniversityBeijing 100091China Institute of Crop Germplasm and Biotechnology Jiangsu Provincial Key Laboratory of AgrobiologyJiangsu Academy of Agricultural SciencesNanjing 210014China Sanya Institute of China Agricultural University Sanya 572025China Hainan Yazhou Bay Seed Laboratory Sanya 572025China

ChinaMu is the largest sequence-indexed Mutator(Mu)transposon insertional library in maize(Zea mays).In this study,we made significant improvements to the size and quality of the ChinaMu *** developed a new Mu-tag isolation method Mu-Tn5-seq(MuT-seq).Compared to the previous method used by ChinaMu,MuT-seq recovered 1/3 more germinal insertions,while requiring only about 1/14 of the sequencing volume and 1/5 of the experimental *** MuT-seq,we identified 113,879 germinal insertions from 3,168 Mu-active F1 *** also assembled a high-quality genome for the Mu-active line Mu-starter,which harbors the initial active MuDR element and was used as the pollen donor for the mutation *** the Mu-starter genome,we recovered 33,662(15.6%)additional germinal insertions in 3,244(7.4%)genes in the Mu-starter *** Mu-starter genome also improved the assignment of 117,689(54.5%)germinal *** newly upgraded ChinaMu dataset currently contains 215,889 high-quality germinal *** insertions cover 32,224 pan-genes in the Mu-starter and B73Ref5 genomes,including 23,006(80.4%)core genes shared by the two *** a test model,we investigated Mu insertions in the pentatricopeptide repeat(PPR)superfamily,discovering insertions for 92%(449/487)of PPR genes in ChinaMu,demonstrating the usefulness of ChinaMu as a functional genomics resource for maize.

关键词： ChinaMu Mutator MuT-seq PPR gene Zea mays

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川西南美姑地区下三叠统飞仙关组地球化学特征及其对物源和构造环境的指示意义

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矿物岩石 2019年第3期39卷 52-59页

作者：张衡李仁涛巴金李小平马继跃四川省地质调查院四川成都610081 四川大凉山南红玛瑙有限责任公司四川西昌615000

针对川西南美姑地区飞仙关组碎屑岩进行岩石学和地球化学方面的研究,以探究其物质来源以及构造背景。川西南美姑地区飞仙关组为一套碎屑岩,三角洲相沉积。碎屑岩主量元素中w(TFe2O3)为3.46%~11.23%,w(MgO)为2%~7.98%,w(TiO2)为1.51%~2.... 详细信息

针对川西南美姑地区飞仙关组碎屑岩进行岩石学和地球化学方面的研究,以探究其物质来源以及构造背景。川西南美姑地区飞仙关组为一套碎屑岩,三角洲相沉积。碎屑岩主量元素中w(TFe2O3)为3.46%~11.23%,w(MgO)为2%~7.98%,w(TiO2)为1.51%~2.62%。微量元素中亲铁镁矿物元素w(Cr)为66×10^-6~426×10^-6,w(Co)为18.8×10^-6~30.6×10^-6,w(Sc)为16.9×10^-6~23.7×10^-6。REE分布模式和Al2O3/TiO2比值与峨眉山高钛玄武岩较为相似,指示着飞仙关组的物质来源于晚二叠世的峨眉山高钛玄武岩。样品的成分异变指数(ICV)值为0.95~3.49,普遍大于1,暗示着飞仙关组的物质来源大部分未经历过风化-沉积成岩的过程,为第一次循环碎屑。飞仙关组碎屑岩CIA值为60.49~72.44,反映了飞仙关组时期该地区经历了温暖、湿润环境下中等程度的化学风化作用。同时碎屑岩中的TFe2O3+MgO,TiO2,Al2O3/SiO2地球化学指标最接近大洋岛弧特征值,Th-Co-Zr/10,La-Th-Sc,Th-Sc-Zr/10图解亦指示着飞仙关组的源岩形成于大陆岛弧-大洋岛弧的构造环境中。结合飞仙关组的岩石学和地球化学特征,初步认为晚二叠世时期在大洋岛弧的构造背景下峨眉山玄武岩喷发溢流而出,而后隆升,为飞仙关组的沉积提供了充足的物质来源。同时,随着飞仙关组的不断沉积,亦逐渐有其他物源混入。

关键词：下三叠统飞仙关组物源构造环境

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Additives strategies to improving cycling stability of li metal batteries by modifying electrode electrolyte interphases

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Progress in Natural Science:Materials International 2024年第2期34卷 338-344页

作者： Yuan li Pengfei Huang Chunyu Cui Xiaoyuan Ma li Chen Zekun li linhai li Yuhong Tian School of Biological and Chemical Engineering Guangxi University of Science and Technology School of College of Chemistry and Chemical Engineering Hunan University Isky Future Energy Institute

li metal batteries（LMBs） have attracted much attention due to the ultra-high theoretical capacity of the li metal anode（LMA）.However,the uncontrollable dendrites growth and low coulombic efficiency hinder their practical ***,we explore 3,5-difluoropyridine（2F-BD） as a novel electrolyte additive to enable highperformance *** 2F-BD additive participates in and modifies the solvation structure of li ions by reducing the coordinated number of PF6-at the electrode surface,leading to the formation of a liF and li3N-rich solid electrolyte interphase（SEI）.The liF component increases the robustness of SEI and suppresses the formation of li dendrites,while the li3N component facilitates the transportation and reaction kinetics of li *** a result,the li‖li symmetric cell presents a stable cycling performance of up to 500 h at a current density of 1 mA *** coupling with liFePO4cathode,the obtained full cell achieves high specific capacities of 106.06 mA h g-1and 84.98 mA h g-1at 2.55 mA cm-2and 5.10 mA cm-2,respectively,and maintains a high capacity retention of84.0% after 1000 cycles at 0.13 mA cm-2,with an average cycling CE of 99.58%.

关键词： Electrolyte additive li dendrites li metal batteries liF and li3N-Rich electrode-electrolyte interphase liFePO4 cathode

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Leaching kinetics of fluorine during the aluminum removal from spent li-ion battery cathode materials

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Journal of Environmental Sciences 2024年第4期138卷 312-325页

作者： Shengjie li Jianxin Zhu Research Center for Eco-Environmental Sciences Chinese Academy of SciencesBeijing 100085China University of Chinese Academy of Sciences Beijing 100049China

The high content of aluminum(Al)impurity in the recycled cathode powder seriously affects the extraction efficiency of Nickel,Cobalt,Manganese,and lithium resources and the actual commercial value of recycled materials,so Al removal is crucially important to conform to the industrial standard of spent li-ion battery cathode *** this work,we systematically investigated the leaching process and optimum conditions associated with Al removal from the cathode powder materials collected in a wet cathode-powder peeling and recycling production line of spent li-ion batteries(liBs).Moreover,we specifically studied the leaching of fluorine(F)synergistically happened along with the removal process of Al,which was not concerned about in other studies,but one of the key factors affecting pollution prevention in the recovery *** mechanism of the whole process including the leaching of Al and F from the cathode powder was indicated by using NMR,FTIR,and XPS,and a defluoridation process was preliminarily investigated in this *** leaching kinetics of Al could be successfully described by the shrinking core model,controlled by the diffusion process and the activation energy was 11.14 kJ/***,the leaching of F was attributed to the dissolution of liPF6and decomposition of PVDF,and the kinetics associated was described by Avrami *** interaction of Al and F is advantageous to realize the defluoridation to some *** is expected that our investigation will provide theoretical support for the large-scale recycling of spent liBs.

关键词： Al removal F leaching Cathode powder Heating alkali leaching Leaching kinetics

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SEI/dead li-turning capacity loss for high-performance anode-free solid-state lithium batteries

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Journal of Energy Chemistry 2024年第9期96卷 145-152页

作者： Qianwen Yin Tianyu li Hongzhang Zhang Guiming Zhong Xiaofei Yang Xianfeng li Division of Energy Storage Dalian National Laboratory for Clean EnergyDalian Institute of Chemical PhysicsChinese Academy of SciencesDalian 116023LiaoningChina University of Chinese Academy of Sciences Beijing 100049China Key Laboratory of Long-Duration and Large-Scale Energy Storage Dalian Institute of Chemical PhysicsChinese Academy of SciencesDalian 116023LiaoningChina Laboratory of Advanced Spectro-Electrochemistry and lithium-Ion Batteries Dalian National Laboratory for Clean EnergyDalian Institute of Chemical PhysicsChinese Academy of SciencesDalian 116023LiaoningChina

Anode-free solid-state lithium metal batteries(AF-SSLBs)have the potential to deliver higher energy density and improved safety beyond lithium-metal ***,the unclear mechanism for the fast capacity decay in AF-SSLBs,either determined by dead li or solid electrolyte interface(SEI),limits the proposal of effective strategies to prolong cycling *** clarify the underlying mechanism,herein,the evolution of SEI and dead li is quantitatively analyzed by a solid-state nuclear magnetic resonance(ss-NMR)technology in a typical liPF6-based polymer *** results show that the initial capacity loss is attributed to the formation of SEI,while the dead li dominates the following capacity loss and the growth rate is 0.141 mA h cm^(−2)cycle−*** reduce the active li loss,the combination of inorganic-rich SEI and self-healing electrostatic shield effect is proposed to improve the reversibility of li deposition/dissolution behavior,which reduces the capacity loss rate for the initial SEI and following dead li generation by 2.3 and 20.1 folds,*** a result,the initial Coulombic efficiency(ICE)and stable CE increase by 15.1%and 15.3%in li-Cu cells,which guides the rational design of high-performance AF-SSLBs.

关键词： Solid-state lithium batteries Solid-state NMR Anode-free SEI Dead li

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Theoretical Design of Defects as a Driving Force for Ion Transport in li_(3)OBr Solid Electrolyte

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Energy & Environmental Materials 2024年第3期7卷 143-153页

作者： Xingyun Luo Yanlu li Xian Zhao State Key Lab of Crystal Materials and Institute of Crystal Materials Shandong UniversityJinan 250100China Center for Optics Research and Engineering Shandong UniversityQingdao 266237China

Due to ever-increasing concerns about safety issues in using li ionic batteries,solid electrolytes have extensively *** li-rich antiperovskite li_(3)OBr has been considered as a promising solid electrolyte candidate,but it still suffers challenges to achieve a high ionic conductivity owing to the high intrinsic symmetry of the crystal ***,we presented a design strategy that introduces various point defects and grain boundaries to break the high lattice symmetry of li_(3)OBr crystal,and their effect and microscopic mechanism of promoting the migration of li-ion were explored *** has been found that li_(i)are the dominant defects responsible for the fast li-ion diffusion in bulk li_(3)OBr and its surface,but they are easily trapped by the grain boundaries,leading to the annihilating of the Frenkel defect pair V'_(li)+li_(i),and thus limits the V'_(li)diffusion at the grain *** V_(Br)defect near the grain boundaries can effectively drive V'_(li)across the grain boundary,thereby converting the carrier of li^(+)migration from li,in the bulk and surface to V'_(li)at the grain boundary,and thus improving the ionic conductivity in the whole li_(3)OBr *** work provides a comprehensive insight into the li^(+)transport and conduction mechanism in the li_(3)OBr *** opens a new way of improving the conductivity for all-solid-state li electrolyte material through the defect design.

关键词： defects density functional theory ionic migration solid electrolyte

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不同年限红柳恢复川西北高寒沙地对土壤团聚体和有机碳的影响

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水土保持学报 2018年第1期32卷 197-203页

作者：江仁涛李富程沈凇涛西南科技大学环境与资源学院四川绵阳621010

利用土壤大团聚体含量(R_(0.25))、平均重量直径(MWD)、几何平均直径(GMD)、团聚体破坏率(PAD)和团聚体对有机碳贡献率(F)指标,研究不同时间尺度红柳恢复川西北高寒沙地对土壤团聚体稳定性和有机碳分布的影响。结果表明:红柳不同恢复年... 详细信息

利用土壤大团聚体含量(R_(0.25))、平均重量直径(MWD)、几何平均直径(GMD)、团聚体破坏率(PAD)和团聚体对有机碳贡献率(F)指标,研究不同时间尺度红柳恢复川西北高寒沙地对土壤团聚体稳定性和有机碳分布的影响。结果表明:红柳不同恢复年限土壤机械稳定性团聚体和水稳性团聚体都以微团聚体(2,0.5~2mm粒级土壤团聚体含量显著增加,表层(0—20cm)土壤团聚体R_(0.25)、MWD和GMD表现为0年2,0.5~2mm粒级团聚体有机碳含量显著提高,>0.5mm粒级团聚体对土壤有机碳贡献率高达34%~60%;红柳恢复对亚表层(20—40cm)土壤团聚体与有机碳分布特征影响不显著。研究表明土壤团聚体稳定性和有机碳指标可作为川西北高寒沙地土壤生态修复适应性指标,红柳恢复对该区沙化土壤改良具有重要作用。

关键词：高寒草地沙漠化生态恢复土壤团聚体土壤有机碳

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Highly polar CoP/Co_(2)P heterojunction composite as efficient cathode electrocatalyst for li-air battery

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Chinese Chemical Letters 2024年第9期35卷 486-490页

作者： Miaomiao li Mengwei Yuan Xingzi Zheng Kunyu Han Genban Sun Fujun li Huifeng li Beijing Key Laboratory of Energy Conversion and Storage Materials College of ChemistryBeijing Normal UniversityBeijing 100875China Key Laboratory of Advanced Energy Materials Chemistry(Ministry of Education) College of ChemistryNankai UniversityTianjin 300071China Center for Advanced Materials Research Beijing Normal UniversityZhuhai 519087China

In order to advance the commercialization of rechargeable li-air batteries,it is of importance to explore cathode catalyst with efficient catalytic *** metal oxides have poor electrical conductivity,while cobalt phosphide has excellent electrical conductivity and large specific surface ***,its application in organic li-air batteries has been much less studied,and the electrocatalytic activity desires to be further ***,CoP/Co_(2)P heterojunction composite with higher polarity was *** discharge product of high-polarity CoP/Co_(2)P had a new porous box-like morphology,which was easy to be decomposed and exposed more active *** highly polar CoP/Co_(2)P heterostructure composite had homogeneous pores,the synergistic effect existed between CoP and Co_(2)P,and the discharge product was porous box mixed with li_(2)O_(2)and liOH,which made CoP/Co_(2)P achieve high specific capacity of14632 m Ah/g and cycle stably 161 times when used as air electrode cathode *** work furnished a thought for the construction of cathode catalysts with efficient catalytic activity for li-air batteries.

关键词： li-air battery Cathode catalyst CoP/Co_(2)P Heterojunction structure High polarity

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