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Development and characterization of 3D-printed electroconductive pHEMA-co-MAA nP-laden hydrogels for tissue engineering

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Bio-Design and Manufacturing 2024年第3期7卷 262-276页

作者： Sara De nitto Aleksandra Serafin Alexandra Karadimou Achim Schmalenberger John J.EMulvihill maur.ce n.collins DIBRIS Polytechnic Inter-School Section University of Genoa16126 GenoaItaly School of Engineering Bernal InstituteUniversity of LimerickLimerick V94 T9PXIreland School of natural Sciences Department of Biological SciencesUniversity of LimerickLimerick V94 T9PXIreland Health Research Institute University of LimerickLimerick V94 T9PXIreland AMBER University of LimerickLimerick V94 T9PXIreland

Tissue engineering(TE)continues to be widely explored as a potential solution to meet critical clinical needs for diseased tissue replacement and tissue *** this study,we developed a poly(2-hydroxyethyl methacrylate-co-methacrylic acid)(pHEMA-co-MAA)based hydrogel loaded with newly synthesized conductive poly(3,4-ethylene-dioxythiophene)(PEDOT)and polypyrrole(PPy)nanoparticles(nPs),and subsequently processed these hydrogels into tissue engineered constructs via three-dimensional(3D)*** presence of the nPs was critical as they altered the rheological properties during ***,all samples exhibited suitable shear thinning properties,allowing for the development of an optimized processing window for 3D *** were 3D printed into pre-determined disk-shaped configurations of 2 and 10 mm in height and diameter,*** observed that the nPs disrupted the gel crosslinking efficiencies,leading to shorter degradation times and compressive mechanical properties ranging between 450 and 550 *** conductivity of the printed hydrogels increased along with the nP concentration to(5.10±0.37)×10^(−7)S/*** vitro studies with cortical astrocyte cell cultures demonstrated that exposure to the pHEMA-co-MAA nP hydrogels yielded high cellular viability and proliferation ***,hydrogel antimicrobial studies with staphylococcus epidermidis bacteria revealed that the developed hydrogels affected bacterial *** together,these materials show promise for various TE strategies.

关键词： Conductive nanoparticles Hydroxyethyl methacrylate(HEMA) Ultraviolet(UV)polymerization 3D printing

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Immune response to inactivated bacterial vector carrying the recombinant K39 antigen of Leishmania infantum in mice

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Asian Pacific Journal of Tropical Biomedicine 2024年第5期14卷 199-206页

作者： Lucelina S.Araújo Bruno B.Silva Eduarda n.F.n.Santos Arnaldo S.Bezerra Samuel S.Frota Assis R.Montenegro Eridan O.P.T.Florean maurício Fvan Tilburg Maria Izabel F.Guedes Laboratory of Biotechnology and Molecular Biology Northeast Biotechnology NetworkState University of CearáFortalezaBrazil Faculty of Veterinary Medicine State University of CearáFortalezaBrazil

Objective:To evaluate the immunological response elicited by an inactivated bacterial vector carrying the K39 antigen of Leishmania infantum,and a purified ***:Mice were subjected to the following treatments:(1)Purified recombinant K39(rK39)protein at a 20μg dose with complete Freund’s adjuvant;(2)Inactivated Escherichia coli(BL21 DE3)carrying the K39 protein at an equivalent total protein content of 200μg;(3)Inactivated bacteria lacking the K39 protein;(4)non-immunized control *** monitoring was *** groups were challenged by intraperitoneal injection of 10^(7) Leishmania infantum *** euthanasia,the liver and spleen were collected to analyze the levels of TnF,IFn-γ,IL-12,IL-4,and ***:Mice immunized with purified rK39 or the inactivated bacterial vector carrying the K39 antigen of Leishmania infantum showed a long-lasting immune response with high levels of polyclonal antibodies specifically recognizing the recombinant *** IgG1 subclass was the predominant immunoglobulin;however,the induction of IgG2a and the profile of cytokines produced were indicative of the induction of a mixed-type ***:The inactivated bacterial vector carrying the K39 antigen,as well as the purified antigen can induce a long-lasting immune response in immunized mice,predominantly favouring a Th2 profile response.

关键词： Visceral leishmaniasis K39 Inactivated bacterial vector Vaccine Immune response Th1 Th2 Leishmania infantum

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Heterostructured Pt-ni_(3)Mo_(3)n formed via ammonia-containing polyoxometalates for highly efficient electrocatalytic hydrogen evolution in acid medium

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Journal of Energy Chemistry 2024年第5期92卷 698-704页

作者： Bianqing Ren Xue Gong Jing Cao Dezheng Zhang Zizhun Wang Ping Song ce Han Weilin Xu State Key Laboratory of Electroanalytical Chemistry Jilin Province Key Laboratory of Low Carbon Chemical PowerChangchun Institute of Applied ChemistryChinese Academy of SciencesChangchun 130022JilinChina School of Applied Chemistry and Engineering University of Science and Technology of ChinaHefei 230026AnhuiChina Key Laboratory of Automobile Materials MOE School of Materials Science&EngineeringJilin Provincial International Cooperation Key Laboratory of High-Efficiency Clean Energy MaterialsElectron Microscopy Centerand International Center of Future ScienceJilin UniversityChangchun 130012JilinChina

Constructing heterostructured nanohybrid is considered as a prominent route to fabricate alternative electrocatalysts to commercial Pt/C for hydrogen evolution reaction(HER).In this work,(nH_(4))_(4)[niH_(6)Mo_(6)O_(4)]·5H_(2)O polyoxometalates(niMo_(6))are adopted as the cluster precursors for simple fabrication of heterostructured Pt-ni_(3)Mo_(3)n nanohybrids supported by carbon black(Pt-ni_(3)Mo_(3)n/C)without using additional n *** improved porosity and enhanced electronic interaction of Pt-ni_(3)Mo_(3)n/C should be attributed to the integration of Pt with niMo_(6),which favors the mass transport,promotes the formation of exposed catalytic sites,and benefits the regulation of intrinsic ***,the as-obtained Pt-ni_(3)Mo_(3)n/C exhibits impressive and durable HER performance as indicated by the low overpotential of 13.7 mV at the current density of 10 mA cm^(-2) and the stable overpotential during continuous working at 100 mA cm^(-2) for 100 *** work provides significant insights for the synthesis of new highly active heterostructured electrocatalysts for renewable energy devices.

关键词： Polyoxometalates Cluster precursors Heterostructured nanohybrids Hydrogen evolution reaction Electrocatalysis

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Hyaluronic acid association with bacterial,fungal and viral infections:Can hyaluronic acid be used as an antimicrobial polymer for biomedical and pharmaceutical applications?

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Bioactive Materials 2023年第1期19卷 458-473页

作者： Fernanda Zamboni Chun Kwok Wong maur.ce n.collins Bernal Institute School of EngineeringUniversity of LimerickIreland Health Research Institute University of LimerickIreland Department of Chemical Pathology The Chinese University of Hong KongHong Kong Special Administrative Region

The relationships between hyaluronic acid(HA)and pathological microorganisms incite new understandings on microbial infection,tissue penetration,disease progression and lastly,potential *** understandings are important for the advancement of next generation antimicrobial therapeutical strategies for the control of healthcare-associated ***,this review will focus on the interplay between HA,bacteria,fungi,and *** review will also comprehensively detail and discuss the antimicrobial activity displayed by various HA molecular weights for a variety of biomedical and pharmaceutical applications,including microbiology,pharmaceutics,and tissue engineering.

关键词： Hyaluronic acid Hyaluronidase Virulence Antibacterial Antifungal Antiviral

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Influence of broken kernels content on soybean quality during storage

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Grain & Oil Science and Technology 2024年第2期7卷 105-112页

作者： Lazaro da Costa Correa Canizares cesar Augusto Gaioso newiton da Silva Timm Silvia Leticia Rivero Meza Adriano Hirsch Ramos maurício de Oliveira Everton Lutz Moacir Cardoso Elias Department of Agroindustry Science and Technology Federal University of PelotasPelotasRio Grande do Sul 96010-900Brazil Information and Communication Technological Axis Federal Institute of EducationScienceand Technology FarroupilhaCampus PanambiPanambiRio Grande do Sul 98280-000Brazil

Although it is recognized that the post-harvest system is most responsible for the loss of soybean quality,the real impact of this loss is still *** regulation allows 15%and 30%of broken soybean for group I and group II(quality groups),***,the industry is not informed about the loss in the quality parameters of soybeans and its impacts during long-term ***,the objective was to evaluate the effect of the breakage kernel percentage of soybean stored for 12 *** of 15% of breakage kernels did not affect soybean ***,content of 30% of breakage kernels affected significantly soybean quality,which was evidenced by the increase of up to 75% in moldy soybeans,72% in acidity,50% in leached solids,27% in electrical conductivity,and the decrease of up to 12% in soluble protein,6.4% in germination and 3.5% in thousand kernel weight after 8 months of *** the legislation establishes a percentage limit,it is recommended to store soybeans with up to 15% breakage *** the contrary,values higher than that can cause a significant reduction in soybean quality,resulting in commercial losses.

关键词： Soybean quality Breakage kernels Storage problems Grain defects Quality parameters

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Magnetic,dielectric and electrical modulus of ce^(3+) doped cobalt-magnesium ferrite nanoparticles

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Journal of Rare Earths 2024年第2期42卷 373-382,I0005页

作者： n.M.Basfer Hanaa Almaghamsi Department of Physics Umm AL-Qura UniversityMakkahSaudi Arabia Physics Department College of Science and ArtKing Abdulaziz UniversityPOB344Rabigh291Saudi Arabi

In this work,the magnetic,dielectric properties and electric modulus of ce^(3+) substituted cobaltmagnesium(Co_(0.7)Mg_(0.3)ce_(x)Fe_(2-x)O_4)(labeled as CMCF) ferrite nanoparticles were investigated in *** magnetization decreases from 50.05 to 34.87 emu/g for further substituting ce^(3+) ***,coercivity increases from 738.22 Gs for the CMCFO sample to 912.10 Gs for the CMCF2 sample,then decreases monotonically to 762.1 Gs for the CMCF5 *** cerium content and particle size play important roles in controlling the magnetization and coercivity of the CMCF *** CMCF nanoferrites are suitable for microwave applications since their high-frequency response ranges from 7.72 to 11.07 *** CMCF nanoferrites' dielectric parameter dispersion exhibits normal *** pristine Co-Mg nanoferrite only has ε' value of 28.25,but the nanoferrite MCMF2 has ε' value of365.03,with an enhancing ratio of 1192%.The conduction mechanism of the MCMF nanoferrites was determined by fitting the σ_(ac) results via the Jonscher power *** 653 K,large polaron tunnelling is thought to be responsible for this conduction process,which is followed by electron barrier hopping at higher ***-Cole diagrams at different temperatures,assuring the contributions of the grains and their boundaries at lower temperatures(653 K) and only the grains at higher *** on our results,the CMCF nanoferrites hold magnetic and semiconducting nature,which can be used in magnetic devices and dielectrics in lower-frequencies or conductors in higher-frequencies.

关键词： nanoferrites Rare earth ions Magnetic properties Dielectric parameters Impedance spectroscopy

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基于高阶累积量张量分解的联合盲源分离算法

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东北大学学报（自然科学版） 2024年第1期45卷 26-32页

作者：季策刘明欣东北大学计算机科学与工程学院辽宁沈阳110169

提出一种基于高阶累积量张量分解的联合盲源分离(JBSS)算法,该算法可以从多组数据集的观测信号中恢复出源信号.首先通过计算多组数据集观测信号的高阶互累积量张量,利用累积量张量潜在的对角结构,将JBSS问题转化为高阶张量CP分解(CPD)问... 详细信息

提出一种基于高阶累积量张量分解的联合盲源分离(JBSS)算法,该算法可以从多组数据集的观测信号中恢复出源信号.首先通过计算多组数据集观测信号的高阶互累积量张量,利用累积量张量潜在的对角结构,将JBSS问题转化为高阶张量CP分解(CPD)问题.接下来,通过张量列分解(TTD)将高阶张量分解为由不高于3阶的多个互连的核张量组成的简单张量网络,由此将高阶CPD问题转化为多个3阶CPD问题.最后,根据TTD与CPD之间的关系,在多次3阶CPD之后,通过依次对因子矩阵进行重新排序与缩放得到多数据集的混合矩阵,进而实现对源信号的分离.实验结果表明,该算法具有较快的运行速度.

关键词：联合盲源分离张量列分解 CP分解高阶累积量

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Comparison of Perovskite Systems Based on AFeO_(3)(A=ce,La,Y)in CO_(2) Hydrogenation to CO

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Transactions of Tianjin University 2024年第4期30卷 337-358页

作者： Anna n.Matveyeva Shamil O.Omarov Laboratory of Materials and Processes for Hydrogen Energy Ioff e Institute194021 St.PetersburgRussia

CO_(2) is the most cost-eff ective and abundant carbon resource,while the reverse water-gas reaction(rWGS)is one of the most eff ective methods of CO_(2) *** work presents a comparative study of rWGS activity for perovskite systems based on AFeO_(3)(where A=ce,La,Y).These systems were synthesized by solution combustion synthesis(SCS)with diff erent ratios of fuel(glycine)and oxidizer(φ),diff erent amounts of nH 4 nO_(3),and the addition of alumina or silica as *** techniques,including X-ray diff raction analysis,thermogravimetric analysis,Fourier transform infrared spectroscopy(FTIR),scanning electron microscopy,energy-dispersive X-ray spectroscopy,n 2-physisorption,H_(2) temper-ature-programmed reduction,temperature-programmed desorption of H_(2) and CO_(2),Raman spectroscopy,and in situ FTIR,were used to relate the physicochemical properties with the catalytic performance of the obtained *** specifi c perovskite-containing system(either bulk or supported)has its own optimalφand nH_(4) nO_(3) amount to achieve the highest yield and dispersion of the perovskite *** all synthesized systems,bulk SCS-derived La-Fe-O systems showed the highest resistance to reducing environments and the easiest hydrogen desorption,outperforming La-Fe-O produced by solgel combustion(SGC).CO_(2) conversion into CO at 600°C for bulk ferrite systems,depending on the A-cation type and preparation method,follows the order La(SGC)cences in properties between La-Fe-O obtained by the SCS and SGC methods can be attributed to diff erent ratios of oxygen and lanthanum vacancy contributions,hydroxyl coverage,morphology,and free iron oxide *** situ FTIR data revealed that CO_(2) hydrogenation occurs through formates generated under reaction conditions on the bulk system based on La-Fe-O,obtained by the SCS method.γ-Al_(2)O_(3) improves the dispersion of ceFeO_(3) and LaFeO_(3) phases,the specifi c surface area,and the quant

关键词： Perovskites LaFeO_(3) ceFeO_(3) YFeO_(3) Solution combustion synthesis CO_(2) hydrogenation Reverse water–gas reaction(rWGS)

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A concise review on surface and structural modification of porous zeolite scaffold for enhanced hydrogen storage

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Chinese Journal of Chemical Engineering 2024年第6期70卷 33-53页

作者： B.A.Abdulkadir R.S.R.Mohd Zaki A.T.Abd Wahab S.n.Miskan Anh-Tam nguyen Dai-Viet n.Vo H.D.Setiabudi centre for Research in Advanced Fluid&Processes Universiti Malaysia Pahang Al-Sultan AbdullahLebuh Persiaran Tun Khalil YaakobGambangPahang 26300Malaysia Faculty of Chemical&Process Engineering Technology Universiti Malaysia Pahang Al-Sultan AbdullahLebuh Persiaran Tun Khalil YaakobGambangPahang 26300Malaysia center of Excellence for Green Energy and Environmental nanomaterials(ce@GrEEn) Nguyen Tat Thanh University300A Nguyen Tat ThanhDistrict 4Ho Chi Minh City 755414Viet Nam

Investigating zeolites as hydrogen storage scaffolds is imperative due to their porous nature and favorable physicochemical ***,the storage capacity of the unmodified zeolites has been rather unsatisfactory(0.224%-1.082%(mass))compared to its modified ***,the contemporary focus on enhancing hydrogen storage capacities has led to significant attention towards the utilization of modified zeolites,with studies exploring surface modifications through physical and chemical treatments,as well as the integration of various active *** enhanced hydrogen storage properties of zeolites are attributed to the presence of aluminosilicates from alkaline and alkaline-earth metals,resulting in increased storage capacity through interactions with the charge density of these ***,there is a great demand to critically review their role such as well-defined topology,pore structure,good thermal stability,and tunable hydrophilicity in enhanced hydrogen *** article aimed to critically review the recent research findings based on modified zeolite performance for enhanced hydrogen *** of the factors affecting the hydrogen storage capacities of zeolites that can affect the rate of reaction and the stability of the adsorbent,like pressure,structure,and morphology were studied,and ***,future perspectives,recommendations,and directions for modified zeolites were discussed.

关键词： Zeolites Hydrogen storage Surface modification Adsorption Active metal

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环渤海河流营养盐的向海输送及环境效应

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中国环境科学 2024年第1期44卷 178-192页

作者：孙策策刘军张爱军李梦露吴文涛臧家业冉祥滨自然资源部第一海洋研究所自然资源部海洋生态环境科学与技术重点实验室山东青岛266061 中国水产科学研究院黄海水产研究所农业农村部海洋渔业可持续发展重点实验室山东省渔业资源与生态环境重点实验室山东青岛266071 山东长岛近海渔业资源国家野外科学观测研究站山东烟台265800 崂山实验室海洋地质过程与环境功能实验室山东青岛266237 中国海洋大学海洋化学理论与工程技术教育部重点实验室山东青岛266100

对2017年枯水期、2019年丰水期、2020年丰水期和2021年丰水期环渤海24条主要入海河流溶解态无机营养盐向海输送的浓度、比值和通量进行了分析.结果表明:环渤海河流溶解无机氮(DIn)浓度在世界河流中处于较高水平,硝酸盐(nO_(3)^(-))为DI... 详细信息

对2017年枯水期、2019年丰水期、2020年丰水期和2021年丰水期环渤海24条主要入海河流溶解态无机营养盐向海输送的浓度、比值和通量进行了分析.结果表明:环渤海河流溶解无机氮(DIn)浓度在世界河流中处于较高水平,硝酸盐(nO_(3)^(-))为DIn的主要赋存形态,溶解硅(DSi)和溶解无机磷(DIP)浓度较低.环渤海河流每年向渤海输送约0.61Gmol氨盐(nH_(4)^(+))、0.24Gmol亚硝酸盐(nO_(2)^(-))、4.85Gmol nO_(3)^(-)、0.02Gmol DIP和3.27Gmol DSi.环渤海小河流在环渤海河流营养盐的向海输送中扮演着重要作用,尤其是DIP的输送可以占入海河流总通量的80%以上;小河流单位流域面积DIn、DIP和DSi输送通量均高于黄河.与世界河流相比,环渤海河流向海输送的营养盐比例失衡,具有高氮磷比、高硅磷比和低硅氮比的特点,磷限制显著.环渤海河流营养盐向海输送和结构失衡可能会进一步影响到渤海的初级生产和生态环境演变,值得深入研究.

关键词：环渤海河流营养盐营养盐结构通量渤海

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