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Layer-by-layer epitaxy growth of thickness-controllable two-dimensional tungsten disulfide

Science China(Information Sciences) 2024年第5期67卷 302-310页

作者： Jieyuan liang Zixing ZOU junwu liang Di WANG Biao WANG Anshi CHU Jiali YI Cheng ZHANG Lizhen FANG Tian ZHANG Huawei LIU Xiaoli ZHU Dong LI Anlian PAN Key Laboratory for Micro-Nano Physics and Technology of Hunan Province State Key Laboratory of Chemo/Biosensing and Chemometrics Hunan Institute of Optoelectronic IntegrationCollege of Materials Science and Engineering School of Physics and ElectronicsHunan University School of Electronic Information and Electrical Engineering Changsha University School of Physics and Telecommunication Engineering Yulin Normal University Units Semiconductor Technology Co. Ltd. School of Physics and Electronics Hunan Normal University

Bilayer transition metal dichalcogenides（TMDs） balance the high mobility of single layers with the high state density of multilayers and therefore have promising application prospects in high-performance electronics. However, the layer-controlled growth of 2D materials is still confronted with challenges such as poor repeatability between different labs and a limited understanding of the growth mechanism at the atomic scale. Herein, we report a new carbon-assisted chemical vapor deposition process that can realize the growth of WS2sheets with high yield, precise thickness controllability, and repeatability. We show that carbon can act as a reducing agent and catalyst that preferentially reacts with the WO3precursor to form intermediate WO3-xproducts with low-valence state W. The resulting oxycarbide gas has a low surface adsorption energy when deposited on the surface of as-grown WS2, which provides nucleation sites for the subsequent layer of WS2growth and leads to the vertical growth of WS2sheets. The growth mechanism is thoroughly investigated. Electrical transport measurements show that the produced bilayer WS2possesses a high carrier mobility(up to 58 cm2·V-1·s-1) and small subthreshold swing（estimated to be 148 mV/decade）,which are among the best reported results for TMDs produced using CVD.

关键词： WS2 thickness-controlled growth chemical vapor deposition additive carbon

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Investigation on N-doped FZ-Si Crystals by IR Absorption Spectrum

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Rare Metals 1989年第3期9卷 46-50页

作者： Luan, Hongfa liang, junwu Acad Sinica China

N-doped FZ-Si crystals and N-doped NTD FZ-Si crystals and their annealing behavior have been studied by IR spectrum. Two models of nitrogen configuration, nearly substitutional nitrogen and interstitial nitrogen pair,... 详细信息

关键词： Crystals Atomic Structure Molecules Vibrations Nitrogen Effects Spectroscopy, Absorption Applications Spectroscopy, Infrared Applications

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Engineering of geometrical configurations in dual-atom catalysts for electrocatalytic applications

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Journal of Energy Chemistry 2024年第7期94卷 273-287页

作者： Tao Zhang Yifan Liu liang Xue Jingwen Sun Pan Xiong junwu Zhu Key Laboratory for Soft Chemistry and Functional Materials of Ministry Education School of Chemistry and Chemical EngineeringNanjing University of Science and TechnologyNanjing210094JiangsuChina

Geometrical configurations play a crucial role in dual-atom catalysts(DACs)for electrocatalytic *** progress has been made to design DACs electrocatalysts with various geometri-cal configurations,but in-depth understanding the relationship between geometrical configurations and metal-metal interaction mechanisms for designing targeted DACs is still *** this review,the recent progress in engineering of geometrical configurations of DACs is systematically *** on the polarity of geometrical configuration,DACs can be classified into two different types that are homonuclear and heteronuclear ***,with regard to the geometrical configurations of the active sites,homonuclear DACs are identified into adjacent and bridged configurations,and heteronuclear DACs can be classified into adjacent,bridged,and separated ***,metal-metal interactions in DACs with different geometrical configurations are ***,the applications of DACs in different electrocatalytic reactions are discussed,including the oxygen reduction reaction(ORR),oxygen evolution reaction(OER),hydrogen evolution reaction(HER),and other ***,the future challenges and perspectives for advancements in DACs are *** review aims to provide inspiration for the design of highly effcient DACs towards energy relatedapplications.

关键词： Dual-atom catalysts Geometrical configurations Homonuclear Heteronuclear Electrocatalysis

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Triboelectric nanogenerator integrated with a simple controlled switch for regularized water wave energy harvesting

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Nano Research 2024年第8期17卷 7585-7592页

作者： Hongbo Yang Xi liang junwu Kan Zhong Lin Wang Tao Jiang Zhanyong Hong College of Engineering Zhejiang Normal UniversityJinhua 321004China Beijing Key Laboratory of Micro-Nano Energy and Sensor Center for High-Entropy Energy and SystemsBeijing Institute of Nanoenergy and NanosystemsChinese Academy of SciencesBeijing 101400China The Beijing Key Laboratory for Nano-Photonics and Nano-Structure Department of PhysicsCapital Normal UniversityBeijing 100048China Guangzhou Institute of Blue Energy Guangzhou 510555China Georgia Institute of Technology AtlantaGA 30332-0245USA Yonsei Frontier Lab Yonsei UniversitySeoul 03722Republic of Korea

Ocean is full of low-frequency,irregular,and widely distributed wave energy,which is suitable as the energy source for maritime Internet of Things(IoTs).Utilizing triboelectric nanogenerators(TENGs)to harvest ocean wave energy and power sensors is proven to be an effective ***,in random ocean waves,the irregular electrical energy output by general TENGs restricts the *** present,achieving regularized water wave energy harvesting relies on rather complex mechanical structure designs,which is not conducive to *** this work,we proposed a novel mechanical controlled TENG(MCTENG)with a simple controlled switch to realize the regularization *** structural parameters of the MC-TENG are optimized,and the optimal output voltage,output current,and transferred charge respectively reach 1684.2 V,85.4μA,and 389.9 nC,generating a peak power density of 38.46 W·m^(−3)·Hz^(−1).Under real water wave environment,the output of the MC-TENG is regularized and keeps stable regardless of any wave ***,the potential applications of the MC-TENG are demonstrated in powering environmental temperature,humidity,and wind speed *** work renders a simple approach to achieve effective regularized ocean wave energy harvesting,promoting the TENG industrialization toward practical application of maritime IoTs.

关键词： water wave energy harvesting triboelectric nanogenerators random excitation mechanical control regular output

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COMPUTATIONAL MODELLING OF HORIZONTAL AND RECTANGULAR SILICON EPITAXIAL REACTOR

COMPUTATIONAL MODELLING OF HORIZONTAL AND RECTANGULAR SILICO...

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The Second International Conference on Solid State and Integrated Circuit Technology

作者： GUO Yulong liang junwu Institute of Semiconductors Academia Sinica

＜正＞Most of the reported models of CVD processes of silicon are based on simplified assumptions[1-6].Nevertheless these simplified assumptions did not precisely reflect the complicated processes occuring In the epitaxial reactors. Basing on the physical analysis,we have abandon the stagnant and boundary sublayers *** this work,the various temperature zones and the effects of temperature distribution on velocity and physical properties of mixed gas are *** addition,thermodiffusion was taken into account. Calculating results are compared with experimental data.

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Tortuosity regulation of two-dimensional nanofluidic films for water evaporation-induced electricity generation

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Nano Research 2024年第7期17卷 6192-6202页

作者： Zhihang Liu Chao Liu Anqi Ni Kunpeng Mao Long Chen liang Xue Jingwen Sun Xin Wang Pan Xiong junwu Zhu Key Laboratory for Soft Chemistry and Functional Materials of Ministry Education School of Chemistry and Chemical EngineeringNanjing University of Science and TechnologyNanjing 210094China

Water evaporation-induced electricity generation is a promising technology for renewable energy ***,the output power of some reported two-dimensional(2D)nanofluidic films is still restricted by the relatively weak water–solid interactions within the tortuous *** further enhance the comprehension and utilization of water–solid interactions,it is of utmost importance to conduct an in-depth investigation and propose a regulatory concept encompassing ion ***,we propose tortuosity regulation of 2D nanofluidic titanium oxide(Ti_(0.87)O_(2))films to optimize the ion transport within the interlayer nanochannel for enhanced efficiency in water evaporation-induced electricity generation for the first *** significance of tortuosity in ion transport is elucidated by designing three 2D nanofluidic films with different *** analysis and in situ Raman measurement demonstrate that low tortuosity can facilitate the formation of efficient pathways for hydrated proton transport and promote water–solid ***,devices fabricated with the optimized 2D nanofluidic films exhibited a significantly enhanced output power density of approximately 204.01μW·cm^(−2),far exceeding those prepared by the high-tortuosity 2D nanofluidic *** work highlights the significance of the construction of low tortuosity channels for 2D nanofluidic films with excellent performance.

关键词： water evaporation-induced electricity generation tortuosity ion transport two-dimensional nanofluidic films

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Control of arsenic Pollution from waste gases during fabrication of semiconductor

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Journal of Environmental Sciences 1994年第1期6卷 123-127页

作者： Wen Ruimei liang junwu Deng Lisheng Peng Yongqing(Institute of Semiconductors, Chinese Academy of Sciences Beijing 100083,China)

The abatement technology of toxic arsenic pollution during fabrication of semiconductormaterials and devices has been studied.

关键词： Semiconductoro arsenic pollution abatement.

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Multiscale confinement nitridation in molybdenum carbide for efficient hydrogen production

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Journal of Energy Chemistry 2024年第7期94卷 61-69页

作者： Liming Dai Chenchen Fang Xiaoyuan Zhang Xuefeng Xu Xuanxuan Chen Xinyue Zong Xueming Hu Wenyao Zhang liang Xue Pan Xiong Yongsheng Fu Jingwen Sun junwu Zhu Key Laboratory for Soft Chemistry and Functional Materials Ministry of EducationNanjing University of Science and TechnologyNanjing 210094JiangsuChina

The molybdenum carbide(Mo_(2)C)has been regarded as one of the most cost-efficient and stable electrocatalyst for the hydrogen evolution reaction(HER)by the virtue of its Pt-like electronic ***,the inherent limitation of high density of empty valence band significantly reduces its catalytic reactivity by reason of strong hydrogen desorption ***,we propose a multiscale confinement synthesis method to design the nitrogen-rich Mo_(2)C for modulating the band structure via decomposing the pre-coordination bonded polymer in a pressure-tight tube sealing ***-bonded c/N-Mo in the coordination precursor constructs a micro-confinement space,enabling the homogeneous nitrogenization in-situ happened during the formation of Mo_(2)***,the evolved gases from the precursor decomposition in tube sealing system establish a macro-confinement environment,preventing the lattice N escape and further endowing a continuous *** the multiscale confinement effects,the nitrogen-rich Mo2C displays as high as 25%N-Mo concentration in carbide lattice,leading to a satisfactory band ***,the constructed nitrogen-rich Mo_(2)C reveals an adorable catalytic activity for HER in both alkaline and acid *** is anticipated that the multiscale confinement synthesis strategy presents guideline for the rational design of electrocatalysts and beyond.

关键词： Molybdenum carbide Hydrogen evolution reaction Multiscale confinement synthesis Valence band modulation Nitrogen doping

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电子级多晶硅的生产工艺

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中国工程科学 2000年第12期2卷 34-39页

作者：梁骏吾中国科学院半导体研究所北京100083

就建设 10 0 0t电子级多晶硅厂的技术进行了探讨。对三氯氢硅法、四氯化硅法、二氯二氢硅法和硅烷法生产的多晶硅质量、安全性、运输和存贮的可行性、有用沉积比、沉积速率、一次转换率、生长温度、电耗和价格进行了对比 ;对还原或热分... 详细信息

就建设 10 0 0t电子级多晶硅厂的技术进行了探讨。对三氯氢硅法、四氯化硅法、二氯二氢硅法和硅烷法生产的多晶硅质量、安全性、运输和存贮的可行性、有用沉积比、沉积速率、一次转换率、生长温度、电耗和价格进行了对比 ;对还原或热分解使用的反应器即钟罩式反应器、流床反应器和自由空间反应器也进行了比较。介绍了用三氯氢硅钟罩式反应器法生产多晶硅三代流程。第三代多晶硅流程适于 10 0 0t/a级的电子级多晶硅生产。

关键词：电子级多晶硅三氯氢硅法半导体材料硅烷法生产工艺钟罩式反应器

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变转速下L_(1,1,2)范数与张量核范数联合约束的TRPCA滚动轴承故障特征提取方法

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振动与冲击 2024年第7期43卷 84-93页

作者：王冉曹徐张军武余亮上海海事大学物流工程学院上海201306 上海交通大学机械系统与振动国家重点实验室上海200240

滚动轴承作为旋转机械设备的重要部件之一,其工作状态直接影响旋转设备的运行安全,因此其故障特征的有效提取对于保障机械设备正常运行具有重要的意义。实际应用中滚动轴承通常以变化的速度运行,并且单一传感器采集的轴承的非平稳信号... 详细信息

滚动轴承作为旋转机械设备的重要部件之一,其工作状态直接影响旋转设备的运行安全,因此其故障特征的有效提取对于保障机械设备正常运行具有重要的意义。实际应用中滚动轴承通常以变化的速度运行,并且单一传感器采集的轴承的非平稳信号往往被严重的背景噪声覆盖,使得故障特征的提取非常困难。为了解决这一问题,提出一种变转速下L_(1,1,2)范数与张量核范数联合约束的张量主成分分析(tensor robust principal component analysis,TRPCA)滚动轴承故障特征提取方法。首先,使用时频表示(time-frequency representation,TFR)作为正向切片构建张量,分别探讨滚动轴承时变故障特征在张量域中的管稀疏性和背景噪声在张量域中的低管秩性。进而使用L_(1,1,2)范数与张量核范数联合约束的TRPCA对故障特征张量进行提取,得到管稀疏的故障特征张量。最后将提取的故障特征张量在通道索引中进行融合,得到能够有效表征故障特征的时频表示。仿真和试验分析验证了该方法在轴承故障特征提取中的有效性。

关键词：张量故障特征提取变转速工况张量主成分分析(TRPCA) 管稀疏

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