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Anti-corrosion performance of Si-surface-alloying NdFeB magnets obtained with magnetron sputtering and thermal diffusion

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Journal of Rare Earths 2023年第8期41卷 1203-1210,I0003页

作者： Jin Tao Bang Liu Pengjie Zhang Guangqing Xu jun lv jun Huang Jian Yan Wei Sun Bingshan Li Dongmei Wang Yucheng Wu School of Materials Science and Engineering Hefei University of TechnologyHefei 230009China BGRIMM Technology Group Co. Ltd.Beijing 102600China National Engineering Research Center for Magnetic Materials Beijing 102600China Key Laboratory of Advanced Functional Materials and Devices of Anhui Province Anhui Provincial International S&T Cooperation Base for Advanced Energy MaterialsHefei University of TechnologyHefei 230009China

Si alloying in the surface layer of NdFeB magnets was realized by thermal diffusion combined with magnetron *** surface composition,phase structure and morphology of NdFeB(S-Si)specimens were characterized by an X-ray diffractometer,an X-ray photoelectron spectrometer and a field emission scanning electron microscope,*** corrosion resistance of bare NdFeB(S-Si)was analyzed by static full immersion corrosion test and electrochemical *** of sputtering and thermal diffusion on the microstructure and corrosion resistance of the surface layer were *** show that surface alloying layer can effectively improve the corrosion resistance of bare NdFeB with the optimized static total immersion corrosion test time in NdFeB(1S-Si)-800 of 36 h,which is much longer than that of the pristine NdFeB(less than 0.5 h).The E_(corr)of NdFeB(1S-Si)-800 positively shifts from-1.05 to-0.92 V,indicating that the corrosion tendency is obviously *** J_(corr)is1.45×10^(-6)A/cm^(2)which is 2 orders of magnitude lower than that of the pristine NdFeB(5.25×10^(-4)A/cm^(2)).The intergranular composite oxides existing in Nd-rich phase contribute to the enhancement of corrosion resistance of Si-surface-alloying NdFeB.

关键词： NdFeB magnets Si surface alloying Magnetron sputtering Thermal diffusion Corrosion resistance Rare earths

Cu(OH)2 supported on Fe(OH)3 as a synergistic and highly efficient system for the dehydrogenation of ammonia-borane

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Science Bulletin 2018年第23期63卷 1583-1590页

作者： Cheng-Yun Peng Chun-Chao Hou Qian-Qian Chen Chuan-jun Wang Xiao-jun lv jun Zhong Wen-Fu Fu Chi-Ming Che Yong Chen Key Laboratory of Photochemical Conversion and Optoelectronic Materials & HKU-CAS Joint Laboratory on New Materials Technical Institute of Physics and Chemistry Chinese Academy of SciencesBeijmg 100190China University of Chinese Academy of Sciences Beijing 100049China College of Chemistry and Material Science Shandong Agricultural UniversityTaian 271018China Institute of Functional Nano and Soft Materials Laboratory (FUNSOM) Jiangsu Key Laboratory for Carbon-Based Functional Materials and DevicesSoochow University Suzhou 215123China State Key Laboratory of Synthetic Chemistry and Department of Chemistry The University of Hong KongHongKongChina

Herein,we first describe the physical mixture of Cu(OH)_2/Fe(OH)_3 as a composite catalyst precursor for the dehydrogenation of ammonia borane(AB)in *** the initial period of catalytic reaction,Cu nanoparticles were formed *** catalytic activity of Cu nanoparticles can be significantly enhanced with the assistance of Fe species and OH~à.A maximum turnover frequency(TOF)of 50.3 mol_(H2)mol^(à1)_(total metal)min^(à1)(135.6 mol_(H2)mol_(Cu)^(à1)min^(à1))was achieved at ambient temperature,which is superior to those of previously reported Fe or Cu based systems.

关键词： Ammonia borane Dehydrogenation Cu(OH)2 Fe(OH)3

Tear inflammation related indexes after cataract surgery in elderly patients with type 2 diabetes mellitus

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World Journal of Clinical Cases 2023年第2期11卷 385-393页

作者： jun lv Cheng-Jian Cao Wei Li Shuang-Le Li jun Zheng Xiu-Li Yang Department of Optometry North Sichuan Medical CollegeNanchong 637000Sichuan ProvinceChina Zigong Academy of Medical Sciences Zigong First People’s HospitalZigong 643000Sichuan ProvinceChina FB Biologie Philipps-Universitaet MarburgMarburg 35043Germany Department of Ophthalmology Zigong First People’s HospitalZigong 643000Sichuan ProvinceChina

BACKGROUND Quantitative studies on the changes in inflammation-related content in tears,especially the effect of diabetes,are *** this study,we measured the preoperative and postoperative tear inflammatory mediator levels in cataract patients,focusing on the expression of inflammatory factors in postoperative cataracts in the diabetic,and investigated the effect of drugs on the control of postoperative *** To study the expression of inflammatory factors in elderly people with type 2 diabetes after cataract *** Patients with a mean age of 70.3±6.3 years were divided into group A(composed of elderly patients with cataracts and type 2 diabetes,n=20 eyes)and group B(patients with age-related cataract,n=20 eyes).Their tears were collected before each operation and on days 1 and 3,and weeks 1,2,3,and 4 ***(150μL)was dropped into the conjunctival sac of the surgical eye,followed by oculogyration in four *** fluid in the conjunctival sac was extracted using a sterile syringe and stored in Eppendorf tubes at-80°C until *** expression levels of matrix metalloproteinase-2(MMP-2),MMP-9,tissue inhibitor of metalloproteinase-1(TIMP-1),TIMP-2,interleukin-6(IL-6),and IL-20 in tear fluid were measured using enzyme-linked immunosorbent *** The postoperative expression levels of MMP-2,MMP-9,TIMP-2,IL-6,and IL-20 in group A were significantly higher than those in group B,whereas the concentration of TIMP-1 in group A remained lower than that in group *** levels of MMP-2 and IL-6 in both groups continuously increased until the peak in the first postoperative week,and then gradually decreased over the next three ***,MMP-2 declined to a lower level than that preoperatively at week 4,but IL-6 decreased to the same level as that *** level of MMP-9 peaked in the first two weeks postoperative and then returned to the same level as 1-day *** concentration of TIMP-1 pos

关键词： Type 2 diabetes mellitus Elderly patients Cataract surgery Tear inflammation-related indicators Temporal changes Prognosis

Increasing leaching rate of gold cyanide of two-stage calcination generated from refractory ore containing arsenopyrite and pyrrhotite

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Rare Metals 2016年第10期35卷 804-810页

作者： Xiao-E Dang Wen-Shuai Ke Chen Tang jun lv Xue Zhou Cheng-Peng Liu Key Laboratory for Gold and Resources of Shaanxi Xi'an University of Architecture and Technology Jin Rui Mining Technology Development Co. Ltd

For the gold locked within hematite in the two- stage calcination, which leads to a low gold leaching rate, the present work is aiming at pretreating the calcination to selectively dissolve hematite. The calcination was pre- treated by sulfuric acid with cosolvent B. The factors in- fluencing the hematite dissolution rate were studied, and the pretreatment parameters considered were H2SO4 con- tent, B dosage and added time, leaching temperature and time. Simultaneously, mineralogy analysis of the calcination, H2SO4 pretreatment residue and cyanide leaching residue were also carried out. Results indicate that the hematite dissolution rate is quicker, the dissolution tem- perature is lower and the dissolution time is shorter in the role of cosolvent B than without B. At the same time, the gold locked within hematite is effectively released, so the leaching rate of gold cyanide increases about 10 % than that in actual factory production. The results have an actual significance in guiding industrial production.

关键词： Locked gold Hematite Pretreatment Two-stage calcination Cosolvent B

A comparative proteomics approach to detect unintended effects in transgenic Arabidopsis

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Journal of Genetics and Genomics 2009年第10期36卷 629-639页

作者： Yanfei Ren jun lv Hua Wang Linchuan Li Yufa Peng Li-Jia Qu National Key Laboratory of Protein Engineering and Plant Genetic Engineering College of Life Sciences Peking University Beijing 100871 China lnstitute of Plant Protection Chinese Academy of Agricultural Sciences Beijing 100193 China

Recently, as part of biosafety assessments, unintended effects have been given much attention. In this study, we applied a proteomics approach to elucidate the unintended effects of random T-DNA insertion in transgenic plants. Separated proteins extracted from 12 transgenic Arabidopsis thaliana with different T-DNA insertion sites and from wild-type （ecotype Col-o） were analyzed. In the transgenic plants, 102 significantly altered protein spots were detected, in which 59 were up-regulated and 43 down-regulated. MALDI-TOF MS analysis showed that most of these expression level-altered proteins were involved in energy transfer, oxidative respiration and photosynthesis. However, none of these proteins was a toxic protein or allergen. Using plants with or without cold treatment, a natural environmental stress, as controls, we found that the number of the altered proteins was even less in those transgenic plants than those triggered by the cold treatment, suggesting that the transgenic events had a weaker impact on the plants than the environmental stresses. Interestingly, the phosphinothricin acetyl transferase （PAT）, the BAR-encoded protein, was detected in nine out of twelve different T-DNA insertion lines at five different insertion sites. These data suggest that the most significant impact of transgenic events on the host plants is from the transgene itself, i.e., from the predictable intended effects, rather than unintended effects. This study also suggests that the proteomics approach has the potential to detect the unintended effects in transgenic plants.

关键词： biosafety proteomics Arabidopsis thaliana 2-D PAGE MALDI-TOF unintended effect

Synthesis and properties of novel hole-transporting materials with triphenylamine units

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Chinese Chemical Letters 2012年第2期23卷 141-144页

作者： Wen Zheng Gao Xiang Gao Li Shi Rong Wang Hai jun lv School of Chemical Engineering and Technology Tianjin UniversityTianjin 300072China College of Chemical and Pharmaceutical Engineering Hebei University of Science and Technology Shijiazhuang 050018China

Two novel organic hole-transporting materials have been synthesized by combination of triphenylamines（TPA） viaπ-conjugated bonds using Wittig *** structures were characterized by NMR,FT-IR and *** optical,electrochemical and thermal properties of the materials were studied in *** results show that these two compounds have blue emission,proper HOMO levels and high thermal ***,a quantum chemical calculation on electron distribution of the two compounds was performed, which suggests the current synthesized materials would be promising candidates for hole-transporting materials.

关键词： Wittig reaction Triphenylamine Hole-transporting materials Quantum chemical calculation

Involvement of mind the gap in the organization of the tracheal apical extracellular matrix in Drosophila and Nilaparvata lugens

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Insect Science 2020年第4期27卷 756-770页

作者： Xiang-Zhao Yue Dan Li jun lv Kai Liu Jie Chen Wen-Qing Zhang State Key Laboratory of Biocontrol and School of Life Sciences Sun Yat-sen UniversityGuangzhouChina

The tracheal apical extracellular matrix(aECM)is vital for expansion of the tracheal lumen and supports the normal structure of the lumen to guarantee air entry and circulation in *** it has been found that some cuticular proteins are involved in the organization of the aECM,unidentified factors still ***,we found that mind the gap(Mtg),a predicted chitin-binding protein,is required for the normal formation of the apical chitin matrix of airway tubes in the model holometabolous insect Drosophila *** to chitin,the Mtg protein was linearly arranged in the tracheal dorsal trunk of the tracheae in *** mtg expression in the tracheae seriously affected the viability of larvae and caused tracheal chitin spiral defects in some *** of mtg mutant showed that mtg was required for normal development of tracheae in *** taenidial folds of some mtg mutant embryos were found on either lateral view of tracheal dorsal trunk or internal view of transmission electron microscopy *** abnormal tracheae were not fully filled with gas and accompanied by a reduction in tracheal width,which are characteristic phenotypes of tracheal aECM ***,in the hemimetabolous brown planthopper(BPH)Nilapat'vata lugens,downregulation of NICPAP1-N(a homolog of mtg)also led to the formation of abnormal tracheal chitin spirals and *** results suggest that mtg and its homolog are involved in the proper organization of the tracheal aECMs in flies and BPH,and that this function may be conserved in insects.

关键词： chitin Drosophila melanogaster,extracellular matrix mind the gap Nilapm vata lugens trachea

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液压泵高低温试验系统设计与应用

液压气动与密封 2024年第6期44卷 30-33页

作者：周创辉卿绿军晁文雄西安航空学院特种泵系统技术国家地方联合工程研究中心陕西西安710077

针对某型航空齿轮泵在极端温度环境下的工作特性测试需求,设计了一套液压泵高低温性能测试方案,并搭建测试试验台架,完成齿轮泵高低温性能测试。结果表明,被试泵的流量-压力特性满足技术指标要求,液压泵的容积效率与工作温度及加载压力... 详细信息

针对某型航空齿轮泵在极端温度环境下的工作特性测试需求,设计了一套液压泵高低温性能测试方案,并搭建测试试验台架,完成齿轮泵高低温性能测试。结果表明,被试泵的流量-压力特性满足技术指标要求,液压泵的容积效率与工作温度及加载压力成反比。

关键词：液压泵高低温试验容积效率试验研究

Wide-range tracking technique for process-variation-robust clock and data recovery applications

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Frontiers of Information Technology & Electronic Engineering 2017年第5期18卷 729-737页

作者： jun-sheng lv You LI Yu-mei ZHOU Jian-zhong ZHAO Hai-hua SHEN Feng ZHANG Institute of Microelectronics Chinese Academy of SciencesBeijing 100029China University of Chinese Academy of Sciences Beijing 100029China

A wide-range tracking technique for clock and data recovery(CDR) circuit is presented. Compared to the traditional technique, a digital CDR controller with calibration is adopted to extend the tracking range. Because of the use of digital circuits in the design, CDR is not sensitive to process and power supply variations. To verify the technique, the whole CDR circuit is implemented using 65-nm CMOS technology. Measurements show that the tracking range of CDR is greater than ±6×10-3 at 5 Gb/s. The receiver has good jitter tolerance performance and achieves a bit error rate of <10–12. The re-timed and re-multiplexed serial data has a root-mean-square jitter of 6.7 ps.

关键词： Clock and data recovery Digital loop filter Phase interpolator