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Materials Sciences and Applications 2024年第9期15卷 336-349页

作者： Farzana Rashid Suraya Sabrin Soshi Md. Abdul gafur Department of Medicine Hallym University Chuncheon-si South Korea Department of MPE AUST Dhaka Bangladesh PP&PDC Bangladesh Council of Scientific and Industrial Research Dhaka Bangladesh

With the modern advancement of treatment approaches in medical science, the application of biomaterials in tissue engineering provides a remarkable opportunity to overcome graft rejection as well as proper wound healing. In this study, novel hybrid films have been synthesized by incorporation of polyvinyl alcohol (PVA), gelatin, and gelatin with glycerin along with different concentrations of pre-prepared hydroxyapatite (HAP) by solution casting method at room temperature in a biosafety cabinet. Glutaraldehyde has been added as a crosslinker in this whole procedure. Fourier-transform infrared spectroscopy (FTIR), X-Ray Diffraction (XRD) have been conducted to observe and compare the structural and chemical stability of the synthesized hybrid film properties. The FTIR results and X-Ray Diffraction analyses confirmed the chemical interactions between HAP, PVA, gelatin, and glycerin have occurred. The crystallinity of HAP also remains in all the prepared hybrid film samples that are observed in XRD. It is expected that these newly synthesized hybrid films could be a better opportunity for various sectors of tissue engineering such as skin, bone, tendon, and cartilage. These synthesized hybrid films can be suitable for wound healing covering. These studies could be a new scope for long-term drug delivery directly on wound sites in diabetic gangrene foot or burn patients as well as cartilage or joint replacement therapy.

关键词： XRD FTIR HAP PVA Gelatin

Development and Characterization of Hybrid Film Made of Hydroxyapatite, Poly Vinyl Alcohol and Gelatin for Biomedical Application

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Materials Sciences and Applications 2024年第9期15卷 320-335页

In the recent research field of bone tissue engineering, polymeric materials play an implacable role in mimes the natural behavior of hard and soft tissues. In some medical conditions such as diabetics, osteoarthritis, burns, or joint replacement conditions, this polymeric materials implication enhances the internal mechanical activities which result in the early recovery of disease by facilitating the wound healing process. In this study, hybrid films have been synthesized based on polyvinyl alcohol (PVA), gelatin, and gelatin with glycerin incorporated with different concentrations of pre-prepared hydroxyapatite (HAP) by solution casting method at room temperature in biosafety cabinet. Glutaraldehyde has been added as a crosslinker in this whole procedure. The mechanical property, swelling, and porosity percentage have been conducted to characterize the structural stability of the synthesized hybrid films. Porosity and swelling of samples are also represented by proper biocompatibility (>90% porosity and swelling in DDW and PBF vary between 287%~72%). Tensile strength (TS), E modulus (Young’s modulus), Elongation at maximum, and Elongation at break are observed to perceive the mechanical properties of hybrid film samples, which are compatible with mechanical properties of different tissue such as trabecular bone, articular cartilage, tendon, nerve and skin tissue. Though, biocompatibility tests both in vivo and in vitro are essential for clinical application in the future. However, the experiment carried out till now explains the true possibility of newly synthesized hybrid films for long-term drug delivery directly on wound sites for wound healing and burn dressing patients in head-neck surgery reconstruction, diabetic gangrene foot, as well as cartilage or joint replacement therapy.

关键词： HAP PVA Gelatin Swelling Test Tensile Strength

Mechanical and Electrical Properties of Some Sn-Zn Based Lead-Free Quinary Alloys

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Materials Sciences and Applications 2024年第7期15卷 213-227页

作者： Shihab Uddin Md. Abdul gafur Suraya Sabrin Soshi Mohammad Obaidur Rahman Department of Physics Jahangirnagar University Savar Dhaka Bangladesh Pilot Plant and Process Development Centre Dhaka Bangladesh Department of Mechanical Engineering Ahsanullah University of Science and Technology Tejgaon Dhaka Bangladesh

Although there are many lead-free soldering alloys on the market, none of them have ideal qualities. The researchers are combining binary alloys with a variety of additional materials to create the soldering alloys’ features. The eutectic Sn-9Zn alloy is among them. This paper investigated the mechanical and electrical properties of Sn-9Zn-x (Ag, Cu, Sb);{x = 0.2, 0.4, and 0.6} lead-free solder alloys. The mechanical properties such as elastic modulus, ultimate tensile strength (UTS), yield strength (YS), and ductility were examined at the strain rates in a range from 4.17 10−3 s−1 to 208.5 10−3 s−1 at room temperature. It is found that increasing the content of the alloying elements and strain rate increases the elastic modulus, ultimate tensile strength, and yield strength while the ductility decreases. The electrical conductivity of the alloys is found to be a little smaller than that of the Sn-9Zn eutectic alloy.

关键词： Lead-Free Solder Strain Rate Ultimate Tensile Strength Ductility Electrical Conductivity

Development and Characterization of Calcium Based Biocomposites Using Waste Material (Calcite Stones) for Biomedical Applications

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Materials Sciences and Applications 2024年第5期15卷 113-135页

作者： Tasmim Adry Nuzhat Tabassum Maisha Md. Abdul gafur Suraya Sabrin Soshi Maruf Hasan Department of Biomedical Engineering Military Institute of Science and Technology Dhaka Bangladesh Pilot Plant and Process Development Center Bangladesh Council of Scientific and Industrial Research (BCSIR) Dhaka Bangladesh Department of Mechanical Engineering Ahsanullah University of Science and Tecnology (AUST) Tejgaong Dhaka Bangladesh

Calcium-based biocomposite materials have a pivotal role in the biomedical field with their diverse properties and applications in combating challenging medical problems. The study states the development and characterization of Calcium-based biocomposites: Hydroxyapatite (HAP), and PVA-Gelatin-HAP films. For the preparation of Calcium-based biocomposites, an unconventional source, the waste material calcite stone, was used as calcium raw material, and by the process of calcination, calcium oxide was synthesized. From calcium oxide, HAP was prepared by chemical precipitation method, which was later added in different proportions to PVA-Gelatin solution and finally dried to form biocomposite films. Then the different properties of PVA/Gelatin/HAP composite, for instance, chemical, mechanical, thermal, and swelling properties due to the incorporation of various proportions of HAP in PVA-Gelatin solution, were investigated. The characterization of the HAP was conducted by X-ray Diffraction Analysis, and the characterization of HAP-PVA-Gelatin composites was done by Fourier Transform Infrared Spectroscopy, Thermomechanical Analysis, Tensile test, Thermogravimetric Differential Thermal Analysis, and Swelling Test. The produced biocomposite films might have applications in orthopedic implants, drug delivery, bone tissue engineering, and wound healing.

关键词： Hydroxyapatite Calcium-Based Biocomposites PVA-Gelatin Films Drug Delivery Bone Tissue Engineering

Using pXRF and vis-NIR spectra for predicting properties of soils developed in loess

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Pedosphere 2022年第4期32卷 602-615页

作者： gafur GOZUKARA Yakun ZHANG Alfred E.HARTEMINK University of Wisconsin-Madison Department of Soil ScienceFD Hole Soils Lab1525 Observatory DriveMadison WI 53706USA Eskisehir Osmangazi University Department of Soil Science and Plant NutritionEskisehir 26160Turkey

Visible near-infrared (vis-NIR) and portable X-ray fluorescence (pXRF) spectrometers have been increasingly utilized for predicting soil properties worldwide. However, only a few studies have focused on splitting the predictive models by horizons to evaluate prediction performance and systematically compare prediction performance for A, B, and combined A+B horizons. Therefore, we investigated the performance of pXRF and vis-NIR spectra, as individual or combined, for predicting the clay, silt, sand, total carbon (TC), and pH of soils developed in loess, and compared their prediction performance for A, B, and A+B horizons. Soil samples (176 in A horizon and 172 in B horizon) were taken from Mollisols and Alfisols in 136 pedons in Wisconsin, USA and analyzed for clay, silt, sand, pH, and TC. The pXRF and vis-NIR spectrometers were used to measure the pXRF and vis-NIR soil spectra. Data were separated into calibration (n = 244, 70%) and validation (n = 104, 30%) datasets. The Savitzky-Golay filter was applied to preprocess the pXRF and vis-NIR spectra, and the first 10 principal components (PCs) were selected through principal component analysis (PCA). Five types of predictor, i.e., PCs from vis-NIR spectra, pXRF of beams at 0–40 and 0–10 keV (XRF40 and XRF10, respectively) spectra, combined XRF40 and XRF10 (XRF40+XRF10) spectra, and combined XRF40, XRF10, and vis-NIR (XRF40+XRF10+vis-NIR) spectra, were compared for predicting soil properties using a machine learning algorithm (Cubist model). A multiple linear regression (MLR) model was applied to predict clay, silt, sand, pH, and TC using pXRF elements. The results suggested that pXRF spectra had better prediction performance for clay, silt, and sand, whereas vis-NIR spectra produced better TC and pH predictions. The best prediction performance for sand (R2= 0.97), silt (R2= 0.95), and clay (R2= 0.84) was achieved using vis-NIR+XRF40+XRF10 spectra in B horizon, whereas the best prediction performance for TC (R2= 0.93)

关键词： Cubist model machine learning algorithm portable X-ray fluorescence spectra soil elements visible near-infrared spectra

Extraction and characterization of alumina nanopowders from aluminum dross by acid dissolution process

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International Journal of Minerals,Metallurgy and Materials 2015年第4期22卷 429-436页

作者： Saifur Rahman Sarker Zahangir Alam Rakibul Qadir M A gafur Mohammad Moniruzzaman Department of Applied Chemistry and Chemical Engineering University of Dhaka Pilot Plant & Project Development Centre (PP& PDC) Bangladesh Council of Scientific and Industrial Research (BCSIR) BCSIR Laboratories Dhaka

A significant amount of aluminum dross is available as a waste in foundry industries in Bangladesh. In this study, alumina was ex- tracted from aluminum dross collected from two foundry industries situated in Dhamrai and Manikgang, near the capital city, Dhaka. Alu- minum dross samples were found to approximately contain 75wt% A1203 and 12wt% SIO2. An acid dissolution process was used to recover the alumina value from the dross. The effects of various parameters, e.g., temperature, acid concentration, and leaching time, on the extrac- tion of alumina were studied to optimize the dissolution process. First, AI（OH）3 was produced in the form of a gel. Calcination of the AI（OH）3 gel at 1000℃, 1200℃, and 1400℃ for 2 h produced O-AlcOa, （t~＋O）-A1203, and u-alumina powder, respectively. Thermal charac- terization of the AI（OH）3 gel was performed by thermogravimetric/differential thermal analysis （TG/DTA） and differential scanning calo- rimetry （DSC）. The phases and crystallite size of the alumina were determined by X-ray diffraction analysis. The dimensions of the alumina were found to be on the nano level. The chemical compositions of the aluminum dross and alumina were determined by X-ray fluorescence （XRF） spectroscopy. The microstructure and morphology of the alumina were studied with scanning electron microscopy. The purity of the alumina extracted in this study was found to be 99.0%. Thus, it is expected that the obtained alumina powders can be potentially utilized as biomaterials.

关键词： aluminum dross alumina nanoparticles acid dissolution calcination X-ray fluorescence analysis

Soil chronosequence and biosequence on old lake sediments of the Burdur Lake in Turkey

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Pedosphere 2021年第6期31卷 882-891页

作者： gafur GOZUKARA Yakun ZHANG Alfred EHARTEMINK Sevda ALTUNBAS Mustafa SARI Department of Soil Science and Plant Nutrition Eskisehir Osmangazi UniversityEskisehir 26160(Turkey) Department of Soil Science FD Hole Soils Lab1525 Observatory DriveUniversity of Wisconsin-MadisonMadison 53706(USA) Department of Soil Science and Plant Nutrition Akdeniz UniversityAntalya 07059(Turkey)

The Burdur Lake is located in the southwest of Turkey,and its area has decreased by 40% from 211 km^(2) in 1975 to 126 km^(2) in *** this study,we investigated how the soil has changed in the lacustrine *** soil profiles were sampled from the former lakebed(chronosequence profiles:P1,2007;P2,1994;and P3,1975),and three soil profiles under different land use types(biosequence profiles:P4,native forest vegetation;P5,agriculture;and P6,lakebed)were *** chronosequence and biosequence soil profiles represented various distances from the Burdur Lake and showed different stages of lacustrine *** electrical conductivity(EC;18.1 to 0.4 dS m^(-1)),exchangeable Na^(+)(34.7 to 1.4 cmol kg^(-1))and K^(+)(0.61 to 0.56 cmol kg^(-1)),and water-soluble Cl^(-)(70.3 to 2.1 cmol L^(-1))and SO_(4)^(2-)(275.9 to 25.0 cmol L^(-1))decreased with increasing distance from the Burdur Lake,whereas the A horizon thickness(10 to 48 cm),structure formation(0 to 48 cm),gleization-oxidation depth(0 to 79 cm),and montmorillonite and organic matter(OM;25.9 to 46.0 g kg^(-1))contents increased in the chronosequence soil *** formation of P3 in the chronosequence and P5 in the biosequence soil profiles increased due to longer exposure to pedogenic processes(time,land use,vegetation,etc.).Changes in EC,exchangeable cation(Na^(+) and K^(+))and water-soluble anion(Cl^(-) and SO_(4)^(2-))concentrations of the salt-enriched horizon,OM,gleization-oxidation depth,A horizon thickness,and structure formation of the chronosequence and biosequence soil profiles(especially the topsoil horizon)were highly related to the distance from the Burdur Lake,time,and land use.

关键词： biosequence soil profile chronosequence soil profile lacustrine material lakebed soil formation

Photooxidation crosslinking to recover residual stress in decellularized blood vessel

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Regenerative Biomaterials 2021年第2期8卷 13-25页

作者： Jintao Wang Lingwen Kong alid.a gafur Xiaobo Peng Natalia Kristi Jing Xu Xingshuang Ma Nan Wang Rose Humphry Colm Durkan Haijun Zhang Zhiyi Ye Guixue Wang Key Laboratory of Biorheological Science and Technology(Chongqing University) Ministry of EducationState and Local Joint Engineering Laboratory for Vascular ImplantsBioengineering College of Chongqing UniversityChongqing 400030China Department of Cardiothoracic Surgery Central Hospital of Chongqing UniversityChongqing Emergency Medical CenterChongqing 400014China The Nanoscience Centre University of CambridgeCambridge CB30FFUK National Local Joint Engineering Laboratory for Biomedical Material Modification DezhouShandong 251100China

Decellularization method based on trypsin-digestion is widely used to construct small diameter vascular ***,this method will reduce the opening angle of the blood vessel and result in the reduction of residual *** stress reduced has an adverse effect on the compliance and permeability of small diameter vascular *** improve the situation,acellular blood vessels were treated with glutaraldehyde and photooxidation crosslinking respectively,and the changes of opening angle,circumferential residual strain of native blood vessels,decellularized arteries and crosslinked blood vessels were measured by means of histological examination,scanning electron microscopy(SEM)and transmission electron microscopy(TEM)in this *** opening angle of decellularized arteries significantly restored after photooxidation crosslinking(P紏0.0216),while that of glutaraldehyde crosslinking blood vessels *** elastic fibers inside the blood vessels became densely rearranged after photooxidation *** results of finite element simulation showed that the residual stress increased with the increase of opening *** this study,we found at the first time that photooxidation crosslinking method could significantly increase the residual stress of decellularized vessels,which provides biomechanical support for the development of new biomaterials of vascular grafts.

关键词： residual stress opening angle mechanical property decellularized artery photooxidation crosslinking finite element method

Photocatalytic Degradation of Oxytetracycline Dihydrate from Aqueous Solution Using Nano ZnO and ***3 (x = 3%, 18%, 33% and 48%)

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Materials Sciences and Applications 2023年第12期14卷 515-525页

作者： Preyanty Sen Suraya Sabrin Soshi Md. Abdul gafur Department of Applied Chemistry and Chemical Engineering University of Dhaka Dhaka Bangladesh Department of Mechanical Engineering Ahsanullah University of Science and Technology Dhaka Bangladesh Bangladesh Council of Scientific and Industrial Research (BCSIR) Dhaka Bangladesh

Traditional wastewater mostly contains pharmaceutical ingredients. Therefore, the wastewater must be completely free from antibiotics before its release into the environment. In the present study, photocatalytic degradation was done to investigate the removal efficiency of Oxytetracycline Dihydrate (OTC) using ZnO, ZnO/3%BaTiO3 (3 BZ), ZnO/18%BaTiO3 (18 BZ), ZnO/ 33%BaTiO3 (33 BZ) and ZnO/48%BaTiO3 (48 BZ) under UV light. After the exposure time of 420 min, about 99.57% and 97.87% of OTC was degraded using ZnO and 3 BZ respectively. Further, increasing the amount of BaTiO3 in ZnO prolongs the degradation time. Therefore, faster efficiency was found using ZnO nanoparticles. The observed reaction rate constant using ZnO was 0.00933 min-1 which decreased to 0.00532 min-1 using 48 BZ, indicating the decrease of reaction rate for increasing the amount of BaTiO3. Hence, the use of ZnO photocatalyst is anticipated to be a promising technique for the photocatalytic degradation of contaminated wastewater with oxytetracycline antibiotics using UV light.

关键词： Advanced Oxidation Process (AOP) Antibiotics Zinc Oxide (ZnO) and Barium Titanate (BaTiO3)

The Temperature Dependence of the Density of States in Semiconductors

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World Journal of Condensed Matter Physics 2013年第4期3卷 216-220页

作者： gafur Gulyamov Nosir Yusupjanovich Sharibaev Ulugbek Inoyatillaevich Erkaboev Namangan Engineering Pedagogical Institute Namangan Uzbekistan Namangan Engineering Pedagogical Institute Namangan Uzbekistan Namangan Engineering Institute of Technology Namangan Uzbekistan

The temperature dependence of the density of energy states in semiconductors is considered. With the help of mathematical modeling of the thermal broadening of the energy levels, the temperature dependence of the band gap of semiconductors is studied. In view of the non-parabolic and the temperature dependence of the effective mass of the density of states in the allowed bands, graphs of temperature dependence of the band gap are obtained. The theoretical results of mathematical modeling are compared with experimental data for Si, InAs and solid solutions of p-Bi2-xSbxTe3-ySey. The theoretical results satisfactorily explain the experimental results for Si and InAs. The new approach is investigated by the temperature dependence of the band gap of semiconductors.

关键词： Band Gap The Effective Mass Density of States The Energy Spectrum The Numerical Simulation and Experiment