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mgO-attached graphene nanosheet(mgO@GNs)reinforced magnesium matrix nanocomposite with superior mechanical,corrosion and biological performance

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International Journal of minerals,metallurgy and materials 2024年第9期31卷 2062-2076页

作者： s.Abazari A.shamsipur H.R.Bakhsheshi-Rad m.s.soheilirad F.Khorashadizade s.s.mirhosseini Department of materials and metallurgical engineering Amirkabir University of TechnologyTehran ***Iran Iranian National standards Organization of Hormozgan HormozganIran Advanced materials Research Center Department of Materials EngineeringNajafabad BranchIslamic Azad UniversityNajafabadIran Department of materials and metallurgical engineering Iran University of Science and TechnologyTehranIran

magnesium(mg)alloys are gaining great consideration as body implant materials due to their high biodegradability and ***,they suffer from low corrosion resistance and antibacterial *** this research,semi-powder metallurgy followed by hot extrusion was utilized to produce the magnesium oxide@graphene nanosheets/magnesium(mgO@GNs/mg)composite to improve mechanical,corrosion and cytocompatibility *** have revealed that the incorporation of mgO@GNs nanohybrids into mg-based composite enhanced microhardness and compressive *** vitro,osteoblast cell culture tests show that using mgO@GNs nanohybrid fillers enhances osteoblast adhesion and apatite *** presence of mgO@GNs nanoparticles in the composites decreased the opening defects,micro-cracks and micro-pores of the composites thus preventing the penetration of the corrosive solution into the *** demonstrated that the mgO@GNs/mg composite possesses excellent antibacterial properties because of the combination of the release of mgO and physical damage to bacterium membranes caused by the sharp edges of graphene nanosheets that can effectively damage the cell wall thereby facilitating penetration into the bacterial lipid ***,the mgO@GNs/mg composite with high mechanical strength,antibacterial activity and corrosion resistance is considered to be a promising material for load-bearing implant applications.

关键词： metal matrix composites mgO@GNs nanohybrid strengthening mechanisms antibacterial activity biocompatibility

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Descriptors-based machine-learning prediction of cetane number using quantitative structure–property relationship

Energy and AI

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energy and AI 2024年第3期17卷 168-178页

作者： Rodolfo s.m.Freitas Xi Jiang school of engineering and materials science Queen Mary University of LondonMile End RoadLondonE14NSUK

The physicochemical properties of liquid alternative fuels are important but difficult to measure/predict, especially when complex surrogate fuels are concerned. In the present work, machine learning is used to develop quantitative structure–property relationship models. The fuel chemical structure is represented by molecular descriptors, allowing the linking of important features of the fuel composition and key properties of fuel utilization. Feature selection is employed to select the most relevant features that describe the chemical structure of the fuel and several machine learning algorithms are tested to construct interpretable models. The effectiveness of the methodology is demonstrated through the development of accurate and interpretable predictive models for cetane numbers, with a focus on understanding the link between molecular structure and fuel properties. In this context, matrix-based descriptors and descriptors related to the number of atoms in the molecule are directly linked with the cetane number of hydrocarbons. Furthermore, the results showed that molecular connectivity indices play a role in the cetane number for aromatic molecules. Also, the methodology is extended to predict the cetane number of ester and ether molecules, leveraging the design of alternative fuels towards fully sustainable fuel utilization.

关键词： Chemical descriptors Quantitative structure-property relationship machine learning Cetane number Fuel design

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Comparative studies on Y(Ⅲ)and Dy(Ⅲ)extraction from hydrochloric and nitric acids by Cyanex 572 as a novel extractant

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Journal of Rare earths 2018年第12期36卷 1342-1350页

作者： N.e.el-Hefny m.s.Gasser sh.sh.emam W.H.mahmoud H.F.Aly Hot Laboratories Centre Atomic Energy Authority Faculty of science Ain Shams University

extraction of Y(III) and Dy(III) from hydrochloric and nitric acids by Cy-572 in kerosene was studied. The factors affecting the extraction were separately investigated. The stoichiometry of the extracted species was deduced on the basis of slope analysis method. evaluation of extraction equilibrium and stripping investigation was studied as well as saponification effect of Cy-572. The composition of the extracted metal species in the organic phase was found to be [mA·(HA)] for Y(III) or Dy(III) in both media.1.0 mol/L HCI is the best stripping agent for each metal ion from the studied acidic media in one *** Cy-572 does not exhibit any selectivity towards the extraction of Y(III) or Dy(III) from both HCI and HNOsolutions. Based on the obtained results, the data were compared and the separation feasibility between lanthanides and Y(III) in the two media was discussed.

关键词： extraction Cyanex-572 Yttrium Lanthanides separation factor saponification

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enhancing high-temperature oxidation resistance(at 1000 °C) of nickel superalloy obtained by laser powder bed fusion via reactive electric spark treatment

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Transactions of Nonferrous metals society of China 2024年

作者： s.K.mUKANOV m.I.PeTRZHIK A.e.KUDRYAshOV e.A.NAUmOVA F.A.BAsKOV P.A.LOGINOV e.A.LeVAshOV National University of science and Technology mIsIs

The high-temperature oxidation resistance of the nickel superalloy grown by the Laser Powder Bed Fusion (LPBF) has been significantly increased as a result of in-situ formation of a thermal barrier layer (α-Al2O3+ CamoO4) during oxidative annealing of surface layers modified by electric spark treatment (esT). The reactive esT of the LPBF-built items based on nickel eP741NP alloy was carried out with low-melting Al-12%si， Al-6%Ca-0.6%si and Al-7%Ca-1%mn electrodes. It was found that at esT done by Al-7%Ca-1%mn electrode an intermetallic (β-NiAl + γ’-Ni3Al) 15 microns thick layer reinforced by spherical oxide (Came)O nanoparticles was formed. Formation of that structure increases the wear resistance of LPBF nickel superalloy by 4.5 times. Further oxidative annealing at 1000 °C lead to a formation of continuous two-layered coating with an inner layer of α-Al2O3and an outer layer of CamoO4， which together act as an effective barrier preventing the diffusion of oxygen into the volume of the superalloy.

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In vivo and in vitro study of resorbable magnesium wires for medical implants:mg purity,surface quality,Zn alloying and polymer coating

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Journal of magnesium and Alloys 2024年第6期12卷 2472-2488页

作者： K.Tesar J.Luňácková m.Jex m.Žaloudková R.Vrbová m.Bartoš P.Klein L.Vištejnová J.Dušková e.Filová Z.sucharda m.steinerová s.Habr K.Balík A.singh Department of materials Faculty of Nuclear Sciences and Physical EngineeringCzech Technical University in PragueTrojanova 13Prague 12000Czech Republic Institute of Physics Czech Academy of SciencesNa Slovance 2Prague 18221Czech Republic Institute of Dental medicine First Faculty of MedicineCharles University and General University Hospital in PragueKaterinská32Prague 12801Czech Republic Department of Physics Faculty of Nuclear Sciences and Physical EngineeringCzech Technical University in PragueBrehová7Prague 11519Czech Republic Department of Composites and Carbon materials Institute of Rock Structure and MechanicsCzech Academy of SciencesV Holešovickách 41Prague 18209Czech Republic Institute of Anatomy First Faculty of MedicineCharles UniversityU Nemocnice 3Prague 12800Czech Republic Biomedical Center Faculty of Medicine in PilsenCharles UniversityAlej Svobody 76Pilsen 32300Czech Republic Department of Pathological Physiology Faculty of Medicine in PilsenCharles UniversityAlej Svobody 7632300 PilsenCzech Republic Department of Histology and embryology Faculty of Medicine in PilsenCharles UniversityAlej Svobody 7632300 PilsenCzech Republic Institute of Pathology First Faculty of MedicineCharles University and General University Hospital in PragueStudnickova 2Prague 12800Czech Republic Department of Biomaterials and Tissue engineering Institute of PhysiologyCzech Academy of SciencesVidenska 1083Prague 14200Czech Republic Research Center for structural materials National Institute for Materials Science1-2-1 SengenTsukuba 305-0047Japan

magnesium is an excellent material in terms of biocompatibility and its corrosion products can serve as an active source for new bone ***,localized corrosion and H_(2)generation limit the potential of mg-based *** low-alloyed mg-Zn wires can strongly reduce problems with large H_(2)bubbles and improve the mechanical properties considerably while maintaining excellent long-term *** pickling and a polymer coating can be effectively used to lower the rate of in vivo *** this work,microstructural,mechanical,and in vitro characterization of 250μm and 300μm extruded wires made from ultra-pure mg,commercially pure mg,mg-0.15Zn,mg-0.4Zn and mg-1Zn was ***,mg-0.4Zn wires together with a variant coated with a copolymer of L-lactide andε-caprolactone were tested in vivo on artificially damaged Wistar rat *** on the observed mg-induced osteogenesis,polymer-coated mg wires with a small addition of Zn are a perspective material for bone-support applications,such as cerclage and fixation wires.

关键词： magnesium Resorbable mg wire mg-Zn implant degradation Biocompatibility study Zn grain boundary segregation

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structural effects induced by dialysis-based purification of carbon nanomaterials

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Nano materials science 2024年第4期6卷 475-483页

作者： A.D.Veloso A.m.Ferraria A.m.Botelho do Rego A.s.Viana A.J.s.Fernandes A.J.Fielding R.A.Videira m.C.Oliveira CQ-VR and Chemistry Department University of Trás-os-Montes e Alto Douro BsIRG iBB-Institute for Bioengineering and BiosciencesDepartment of Chemical Engineeringand Associate Laboratory i4HB-Institute for Health and BioeconomyInstituto Superior TécnicoUniversidade de Lisboa Centro de Química estrutural Institute of Molecular SciencesDepartamento de Química e BioquímicaFaculdade de CiênciasUniversidade de Lisboa I3N and Physics Department University of AveiroCampus de Santiago Faculty of science Pharmacy and Biomolecular SchoolLiverpool John Moores University ReQUImTe/LAQV Laborat orio de FarmacognosiaDepartamento de QuímicaFaculdade de Farm aciaUniversidade do Porto

Dialysis plays a crucial role in the purification of nanomaterials but its impact on the structural properties of carbon nanomaterials was never ***,a carbon-based nanomaterial generated electrochemically in potassium phosphate buffer,was characterized before and after dialysis against pure *** is shown that dialysis affects the size of the carbon domains,structural organization,surface functionalization,oxidation degree of carbon,and grade of ***,dialysis drives the nanomaterial organization from discrete roundish carbon domains,with sizes ranging from 70 to 160 nm,towards linear stacking structures of small nanoparticles （m）.In parallel,alcohol and ether （epoxide） surface groups evolve into more oxidized carbon groups （e.g.,ketone and ester groups）.Investigation of the as-prepared nanomaterial by electron paramagnetic resonance （ePR） revealed a resonance signal consistent with carbon-oxygen centred ***,this study brings to light the selective affinity of the carbon nanomaterial under study to capture Na+ions,a property greatly enhanced by the dialysis process,and its high ability to trap oxygen,particularly before *** findings open new perspectives for the application of carbon-based nanomaterials and raise awareness of the importance of structural changes that can occur during the purification of carbon-based nanomaterials.

关键词： Nanocarbon surface functionalization NmR XPs Hydrophilic carbon Paramagnetic

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Large magnetocaloric effect and magnetic properties of euRhO3

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Journal of Rare earths 2024年第9期42卷 1724-1729页

作者： m.Lassri m.sajieddine A.elouafi A.el Hachmi s.el Ouahbi R.moubah Laboratory of energy and materials engineering (LGem) University of Sultan Moulay SlimaneFaculty of Science and Technology (FST) Institute of Applied Physics (IAP)-school of Industrial management (emINes) Mohammed Ⅵ Polytechnic University National school of Applied sciences (eNsA) University of Sultan Moulay Slimane Laboratory of mechanics Production and Industrial Engineering (LMPGI)Higher School of Technology of Casablanca (ESTC)University of Hassan Ⅱ Casablanca Laboratory of Radiation on matter and Instrumentation (LRmI) Faculty of Science and Technology (FST) SettatHassan Ⅰ University Laboatory of Physics of Advanced materials and Thermic (LPmAT) Faculty of Science Ain Chock (FSAC)University of Hassan Ⅱ Casablanca

We report on the structural,magnetic,and magnetocaloric properties of *** oxidation states of eu and Rh ions were studied using X-ray photoelectron spectroscopy（XPs）.It is found that the eu ions are mainly in the divalent oxidation state while the Rh ions have+4 ***3powders are found to be antiferromagnetic with a second order magnetic transition at Neel temperature（TN=2.9 K）.Analysis of the magnetic susceptibility versus temperature data in terms of the Curie=Weiss law:(χ=C/（T-θW）) for T>TN,yields θW=-3.1 K and effective magne tic moment ■,which is close to the theoretical value ■.The magnetic entropy change(-Δsm),was determined by em ploying the thermodynam ic maxwell's *** μ0H=5 T and near TN,■ and relative cooling power（RCP） exhibit large values of 33.7 J/（kg·K） and 238 J/kg,*** large magnitude of-Δsmand RCP show that the euRhO3compound could be a potential candidate to be used in cryogenic magnetic refrigeration.

关键词： Cryogenic magnetic refrigeration magnetic properties magnetocaloric effect Rare earths X-ray photoelectron spectroscopy

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Computational Fluid Dynamics Approach for Predicting Pipeline Response to Various Blast scenarios: A Numerical modeling study

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Computer modeling in engineering & sciences 2024年第9期140卷 2747-2777页

作者： Farman saifi mohd Javaid Abid Haleem s.m.Anas Department of mechanical engineering Jamia Millia Islamia(A Central University)New Delhi110025India Department of Civil engineering Jamia Millia Islamia(A Central University)New Delhi110025India

Recent industrial explosions globally have intensified the focus in mechanical engineering on designing infras-tructure systems and networks capable of withstanding blast *** centered on high-profile facilities such as embassies and petrochemical plants,this concern now extends to a wider array of infrastructures and *** and scholars increasingly prioritize structural safety against explosions,particularly to prevent disproportionate collapse and damage to nearby *** has further amplified the reliance on oil and gas pipelines,making them vital for urban life and prime targets for terrorist ***,there is a growing imperative for computational engineering solutions to tackle blast loading on pipelines and mitigate associated risks to avert *** this study,an empty pipe model was successfully validated under contact blast conditions using Abaqus software,a powerful tool in mechanical engineering for simulating blast effects on buried *** a eulerian-Lagrangian computational fluid dynamics approach,the investigation extended to above-surface and below-surface blasts at standoff distances of 25 and 50 *** descriptions in the numerical model relied on Abaqus’default mechanical *** analysis revealed varying pipe performance,with deformation decreasing as explosion-to-pipe distance *** explosion’s location relative to the pipe surface notably influenced deformation levels,a key finding highlighted in the ***,quantitative findings indicated varying ratios of plastic dissipation energy(PDe)for different blast scenarios compared to the contact blast(P0).specifically,P1(25 mm subsurface blast)and P2(50 mm subsurface blast)showed approximately 24.07%and 14.77%of P0’s PDe,respectively,while P3(25 mm above-surface blast)and P4(50 mm above-surface blast)exhibited lower PDe values,accounting for about 18.08%and 9.67%of P0’s PDe,***

关键词： Blast loading computational fluid dynamics computer modeling pipe networks response prediction structural safety

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Credit Card Fraud Detection Using Improved Deep Learning models

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Computers, materials & Continua 2024年第1期78卷 1049-1069页

作者： sumaya s.sulaiman Ibraheem Nadher sarab m.Hameed Computer science Department Al-Mustansiriya UniversityBaghdad10001Iraq Computer science Department University of BaghdadBaghdad10001Iraq Faculty of Basic education Al-Mustansiriya UniversityBaghdad10001Iraq

Fraud of credit cards is a major issue for financial organizations and *** fraudulent actions become more complex,a demand for better fraud detection systems is *** learning approaches have shown promise in several fields,including detecting credit card ***,the efficacy of these models is heavily dependent on the careful selection of appropriate *** paper introduces models that integrate deep learning models with hyperparameter tuning techniques to learn the patterns and relationships within credit card transaction data,thereby improving fraud *** deep learning models:Autoencoder(Ae),Convolution Neural Network(CNN),and Long short-Term memory(LsTm)are proposed to investigate how hyperparameter adjustment impacts the efficacy of deep learning models used to identify credit card *** experiments conducted on a european credit card fraud dataset using different hyperparameters and three deep learning models demonstrate that the proposed models achieve a tradeoff between detection rate and precision,leading these models to be effective in accurately predicting credit card *** results demonstrate that LsTm significantly outperformed Ae and CNN in terms of accuracy(99.2%),detection rate(93.3%),and area under the curve(96.3%).These proposed models have surpassed those of existing studies and are expected to make a significant contribution to the field of credit card fraud detection.

关键词： Card fraud detection hyperparameter tuning deep learning autoencoder convolution neural network long short-term memory resampling

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In search of a pan-coronavirus vaccine:next-generation vaccine design and immune mechanisms

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Cellular & molecular Immunology 2024年第2期21卷 103-118页

作者： s.Cankat m.U.Demael L.swadling Division of Infection and Immunity Institute of Immunity and TransplantationUniversity College LondonPears BuildingLondon NW32PPUK

members of the coronaviridae family are endemic to human populations and have caused several epidemics and pandemics in recent *** this review,we will discuss the feasibility of and progress toward the ultimate goal of creating a pan-coronavirus vaccine that can protect against infection and disease by all members of the coronavirus *** will detail the unmet clinical need associated with the continued transmission of sARs-CoV-2,meRs-CoV and the four seasonal coronaviruses(HCoV-OC43,NL63,HKU1 and 229e)in humans and the potential for future zoonotic *** will highlight how first-generation sARs-CoV-2 vaccines and natural history studies have greatly increased our understanding of effective antiviral immunity to coronaviruses and have informed next-generation vaccine *** will then consider the ideal properties of a pan-coronavirus vaccine and propose a blueprint for the type of immunity that may offer ***,we will describe a subset of the diverse technologies and novel approaches being pursued with the goal of developing broadly or universally protective vaccines for coronaviruses.

关键词： Vaccine Coronavirus Cross-reactive immunity Cross-protection Universal

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