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Effect of titanium on the sticking of pellets based on hydrogen metallurgy shaft furnace:Behavior analysis and mechanism evolution

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International Journal of Minerals,Metallurgy and Materials 2024年第2期31卷 282-291页

作者： Jinge Feng Jue Tang Zichuan Zhao Mansheng Chu Aijun Zheng Xiaobing Li Xiao’ai Wang School of Metallurgy Northeastern UniversityShenyang 110819China Institute for Frontier Technologies of Low-carbon Steelmaking Northeastern UniversityShenyang 110819China Liaoning Low-carbon Steelmaking Technology Engineering Research Center Northeastern UniversityShenyang 110819China Engineering Research Center of Frontier Technologies for Low-carbon Steelmaking(Ministry of Education Shenyang 110819China Zhang Xuan Technology of HBIS group co. Ltd.Shijiazhuang 050000China Xuanhua Iron and Steel group co. Ltd.Shijiazhuang 050000China Iron and Steel Research Institute of HBIS group co. Ltd.Shijiazhuang 050000China

Direct reduction based on hydrogen metallurgical gas-based shaft furnace is a promising technology for the efficient and low-carbon smelting of vanadium-titanium ***,in this process,the sticking of pellets occurs due to the aggregation of metal-lic iron between the co.tact surfaces of adjacent pellets and has a serious negative effect on the co.tinuous *** paper presents a detailed experimental study of the effect of TiO2 on the sticking behavior of pellets during direct reduction under different *** showed that the sticking index(SI)decreased linearly with the increasing TiO2 *** phenomenon can be attributed to the increase in unreduced FeTiO3 during reduction,leading to a decrease in the number and strength of metallic iron interco.nections at the sticking *** the TiO2 addition amount was raised from 0 to 15wt%at 1100°C,the SI also increased from 0.71%to 59.91%.The co.nection of the slag phase co.ld be attributed to the sticking at a low reduction temperature,co.responding to the low sticking ***,the interco.nection of metallic iron became the dominant factor,and the SI increased sharply with the increase in re-duction ***2 had a greater effect on SI at a high reduction temperature than at a low reduction temperature.

关键词： titanium sticking index hydrogen metallurgy direct reduction pellets

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Effect of Heat Treatment on Gradient Microstructure and Tensile Property of Laser Powder Bed Fusion Fabricated 15-5 Precipitation Hardening Stainless Steel

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Acta Metallurgica Sinica(English Letters) 2024年第1期37卷 181-195页

作者： Sheng Cao Hongyu Liu Jin Jiang Ke He Binghua Lv Hao Zhang Lujie Zhang Jingrong Meng Hao Deng Xiaodong Niu Department of Mechanical Engineering College of EngineeringShantou UniversityShantou515063China China State Shipbuilding co. Ltd.Huangpu Wenchong Shipbuilding Company Ltd.Guangzhou510715China Faculty of Materials and Manufacturing Beijing University of TechnologyBeijing100080China Shantou Ruixiang Mould co. Ltd.Shantou515041China Military Representative Office X of Unit 93147 Deyang618000China China National Erzhong group co. Deyang Wanhang Die Forging Co.Ltd.Deyang618013China

This work investigated the gradient microstructure evolution and tensile property of LPBF fabricated 15-5 precipitation hardening stainless steel in post-process direct ageing(DA)and solution treating&ageing(STA).The varied microstructures for austenite and small-sized oxide inclusions at different sample heights in the as-built(AB)co.dition was generally preserved after DA ***,austenite was almost disappeared,and oxide particle grew significantly after the STA *** a result,the tensile property differences in sample top and bottom for AB and DA co.ditions did not occur in the STA *** the influence of post-process heat treatment,the STA co.dition had the highest yield strength due to the highest volume fraction of nano-sized Cu ***,the DA specimen had the highest ultimate tensile strength and elongation owing to the co.siderable amount of austenite phase and associated transformation induced plasticity effect.

关键词： 15-5 PH stainless steel Laser powder bed fusion Heat treatment Gradient microstructures Tensile properties

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Effect of slow shot speed on externally solidified crystal,porosity and tensile property in a newly developed high-pressure die-cast Al-Si alloy

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China Foundry 2024年第1期21卷 11-19页

作者： Wen-ning Liu Wei Zhang Peng-yue Wang Yi-xian Liu Xiang-yi Jiao Ao-xiang Wan Cheng-gang Wang Guo-dong Tong Shou-mei Xiong School of Materials Science and Engineering Tsinghua UniversityBeijing 100084China Key Laboratory for Advanced Materials Processing Technology Tsinghua UniversityBeijing 100084Beijing China FAW group co. Ltd.Changchun 130013China China FAW Foundry co. Ltd.Changchun 130013China

The effect of slow shot speed on externally solidified crystal(ESC),porosity and tensile property in a newly developed high-pressure die-cast Al-Si alloy was investigated by optical microsco.y(OM),scanning electron microsco.y(SEM)and laboratory co.puted tomography(CT).Results showed that the newly developed AlSi9MnMoV alloy exhibited improved mechanical properties when co.pared to the AlSi10MnMg *** AlSi9MnMoV alloy,which was designed with trace multico.ponent additions,displays a notable grain refining effect in co.parison to the AlSi10MnMg *** elements Ti,Zr,V,Nb,B promote heterogeneous nucleation and reduce the grain size of primaryα-*** a lower slow shot speed,the large ESCs are easier to form and gather,developing into the dendrite net and *** an increase in slow shot speed,the size and number of ESCs and porosities significantly *** addition,the distribution of ESCs is more dispersed and the net-shrinkage *** tensile property is greatly improved by adopting a higher slow shot *** ultimate tensile strength is enhanced from 260.31 MPa to 290.31 MPa(increased by 11.52%),and the elongation is enhanced from 3.72%to 6.34%(increased by 70.52%).

关键词： hypoeutectic Al-Si alloy high pressure die casting porosity externally solidified crystal tensile property

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Dissolution behavior of Al_(2)O_(3)inclusions into CaO-MgO-SiO_(2)-Al_(2)O_(3)-TiO_(2)system ladle slags

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International Journal of Minerals,Metallurgy and Materials 2024年第5期31卷 977-987页

作者： Zhiyin Deng Xiaomeng Zhang Guangyu Hao Chunxin Wei Miaoyong Zhu Key Laboratory for Eco.ogical Metallurgy of Multimetallic Mineral(Ministry of Education) Northeastern UniversityShenyang 110819China School of Metallurgy Northeastern UniversityShenyang 110819China TBEA Shenyang Transformer group co. Ltd.Shenyang 110141China Angang Steel co. Ltd.Anshan 114021China

To investigate the dissolution behaviors of Al_(2)O_(3)inclusions in CaO-5wt%MgO-SiO_(2)-30wt%Al_(2)O_(3)-TiO_(2)system ladle slags,co.focal scanning laser microsco.y was co.ducted on the slags with different TiO_(2)co.tents(0-10wt%),and scanning electron microsco.y was performed to study the interfacial reaction between Al_(2)O_(3)and this slag *** results disclose that the dissolution of Al_(2)O_(3)inclusions does not result in the formation of new phases at the boundary between the slag and the *** TiO_(2)-bearing and TiO_(2)-free ladle slags,there is no difference in the dissolution mechanism of Al_(2)O_(3)inclusions at steelmaking *** layer diffusion is found as the co.trolling step of the dissolution of Al_(2)O_(3),and the diffusion co.fficient is in the range of 4.18×10^(-10)to 2.18×10^(-9)m^(2)/s at 1450-1500℃.co.pared with the solubility of Al_(2)O_(3)in the slags,slag visco.ity and temperature play a more profound role in the dissolution of Al_(2)O_(3)inclusions.A lower visco.ity and a lower melting point of the slags are beneficial for the *** addition of TiO_(2)(e.g.,5wt%)in ladle slags can enhance the dissolution of Al_(2)O_(3)inclusions because of the low visco.ity and melting point of the slags,while excessive addition of TiO_(2)(e.g.,10wt%)shows the opposite trend.

关键词： inclusions dissolution ladle refining slag titanium dioxide co.focal scanning laser microsco.y

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Prediction for permeability index of blast furnace based on VMD-PSO-BP model

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Journal of Iron and Steel Research International 2024年第3期31卷 573-583页

作者： Xiao-jie Liu Yu-jie Zhang Xin Li Zhi-feng Zhang Hong-yang Li Ran Liu Shu-jun Chen School of Metallurgy and Energy North China University of Science and TechnologyTangshan 063210HebeiChina Chengde Branch HBIS Group Co.Ltd.Chengde 067000HebeiChina

The permeability index is one of the important production indicators to monitor the operation of blast *** is crucial to grasp the trends of changes in the new permeability index in *** the co.plex vibration spectrum of the permeability index,a prediction model of the permeability index based on the VMD-PSO-BP(variational mode deco.position-particle swarm optimization-back propagation)method was ***,the key factors that affect the permeability index of blast furnace were studied from multiple ***,the permeability index was divided into multiple sub-modes based on the difference of frequency bands by the VMD algorithm,and a PSO-BP prediction model was established for each ***,the prediction results of each sub-mode were summed to obtain the final *** results show that the co.posite prediction accuracy by using the VMD algorithm is 3%higher than that of the traditional prediction method,which has better applicability.

关键词： Big data-Blast furnace Air permeability Variational mode deco.position Particle swarm optimization Back propagation Model prediction

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Diffusion and reaction mechanism of limestone and quartz in fluxed iron ore pellet roasting process

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International Journal of Minerals,Metallurgy and Materials 2024年第3期31卷 485-497页

作者： Yufeng Guo Jinlai Zhang Shuai Wang Jianjun Fan Haokun Li Feng Chen Kuo Liu Lingzhi Yang School of Minerals Processing and Bioengineering Central South UniversityChangsha 410083China Technology Center Taiyuan Iron Steel(Group)Co.Ltd.(TISCO)Taiyuan 030003China

The increase to the proportion of fluxed pellets in the blast furnace burden is a useful way to reduce the carbon emissions in the ironmaking *** this study,the interaction between calcium carbonate and iron ore powder and the mineralization mechanism of fluxed iron ore pellet in the roasting process were investigated through diffusion co.ple *** electron microsco.y with energy dispersive spectrosco.y was used to study the elements’diffusion and phase transformation during the roasting *** results indicated that limestone deco.posed into calcium oxide,and magnetite was oxidized to hematite at the early stage of *** the increase in roasting temperature,the diffusion rate of Fe and Ca was obviously accelerated,while the diffusion rate of Si was relatively *** order of magnitude of interdiffusion co.fficient of Fe_(2)O_(3)-CaO diffusion co.ple was 10^(−10) m^(2)·s^(−1) at a roasting temperature of 1200℃for 9 ***_(2)Fe_(2)O_(5) was the initial product in the Fe_(2)O_(3)-CaO-SiO_(2) diffusion interface,and then Ca_(2)Fe_(2)O_(5) co.tinued to react with Fe_(2)O_(3) to form CaFe_(2)O_(4).With the expansion of the diffusion region,the sillico.ferrite of calcium liquid phase was produced due to the melting of SiO_(2) into CaFe_(2)O_(4),which can strengthen the co.solidation of fluxed ***,andradite would be formed around a small part of quartz particles,which is also co.ducive to the co.solidation of fluxed *** addition,the principle diagram of limestone and quartz diffusion reaction in the process of fluxed pellet roasting was discussed.

关键词： fluxed iron ore pellet limestone hematite quartz diffusion reaction

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Properties and microstructure of co.per–titanium alloys with magnesium additions

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Rare Metals 2024年第5期43卷 2290-2299页

作者： Lue Huang Li-Jun Peng Jiang Li Xu-Jun Mi Gang Zhao Guo-Jie Huang Hao-Feng Xie Yi-Cheng Cao Wen-Jing Zhang Zhen Yang State Key Laboratory of Nonferrous Metals and Processes GRINM Group Co.Ltd.Beijing 100088China GRIMAT Engineering Institute co. LtdBejing 101407China School of Materials Science and Engineering Northeastern UniversityShenyang110000China General Research Institute for Nonferrous Metals Beijing 100088China China Academy of Space Technology Beijing 100094China China Nonferrous Metals Mining group(Tianjin)co.Ltd Tianjin 3001llChina

The volume fractions and morphology of precipitates in precipitation-strengthened Cu-Ti alloys,which precipitate mainly as co.tinuous and disco.tinuous precipitates,are important for the application of the *** study employed hardness and electrical co.ductivity tests transmission electron microsco.y(TEM),atom probe tomography(APT),and first-principles calculations to demonstrate that the addition of Mg is effective for accelerating nanosized co.tinuousβ'-Cu_(4)Ti precipitation as well as for suppressing the precipitation of co.rse lamellar disco.tinuousβ-Cu_(4)Ti precipitates along the grain boundaries,resulting in Cu-Ti alloys with high yield strength and good electrical *** results showed that the co.tinuous precipitation ofβ'-Cu_(4)Ti was accelerated by the Mg additions,which reduced the supersaturation of the matrix,thereby reducing the chemical driving force for the disco.tinuous *** the other hand,Mg additions increased the mismatch between the disco.tinuousβ-Cu_(4)Ti precipitates and matrix decreased the nucleation rate of the disco.tinuous precipitates,and increased the spacing of the disco.tinuous precipitation layer,resulting in a lower growth rate of the disco.tinuous ***,the addition of Mg to Cu-Ti alloys enhances the strength and improves the resistance to over-ageing.

关键词： Cu-Ti-Mg alloy Precipitation hardening Disco.tinuous precipitation co.tinuous precipitation Microstructure formation mechanism

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Changes in microstructure and properties of weld heat-affected zone of high-strength low-alloy steel

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Journal of Iron and Steel Research International 2024年第8期31卷 2041-2052页

作者： Shu-jun Jia Qi-lin Ma Yu Hou Ba Li He-song Zhang Qing-you Liu Central Iron and Steel Research Institute co. Ltd.Beijing 100081China co.laborative Innovation Center for Steel co.monality University of Science and Technology BeijingBeijing 100083China co.struction Project Management Branch of China National Petroleum Pipeline Network group co. Ltd.Langfang 065000HebeiChina

The evolution of the microstructure and toughness of APL5L X80 pipeline steel after thermal welding simulation was investigated by X-ray diffraction,electron backscatter diffraction,and transmission electron *** results indicated that primary heat-affected zones can be divided into weld,co.rse-grained,fine-grained,intercritical,and sub-critical *** microstructure of the weld zone is mainly co.posed of bainitic ferrite and a small amount of granular bainite;however,the original austenite grains are distributed in the co.umnar *** structure of the co.rse-grained zone is similar to that of the weld zone,but the original austenite grains are *** co.trast,the microstructure in the fine-grained zone is dominated by fine granular bainite,and the effective grain size is only 8.15μm,thus providing the highest toughness in the entire heat-affected *** intercritical and subcritical zones were brittle valley regions,and the microstructure was dominated by granular ***,the martensite-austenite(M/A)co.stituents are present in island chains along the grain boundaries,and the co.rse size of the M/A co.stituents seriously reduces the *** results of the crack propagation analyzes revealed that high-angle grain boundaries can significantly slow down crack growth and change the crack direction,thereby increasing the material *** impact toughness of the low-temperature tempering zone was equivalent to that of the co.umnar grain zone,and the impact toughness was between those of the critical and fine-grained zones.

关键词： Welding thermal simulation Impact toughness Crack propagation Martensite-austenite co.stituent High-strength low-alloy steel weld Heat-affected zone

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Development and engineering application of integrated safety monitoring systems for China’s high-speed trains

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Transportation Safety and Environment 2024年第2期6卷 36-44页

作者： Yan Zhu Tiantian Wang Ruiyuan Shen Jingsong Xie Jingsong Yang Guoqin Zhang Hongqi Tian Xifeng Liang School of Traffic and Transportation Engineering Central South UniversityChangsha 410075HunanChina CRRC Changchun Railway Vehicles co. LtdChangchun 130062JilinChina China State Railway group co. Ltd.Beijing 100084China

With the improvement of the running speed of China’s high-speed trains,the demands for running status monitoring and security assurance of High-speed Electric Multiple Units(EMU)have increased ***,the current safety monitoring systems are independent,which is not co.ducive to the co.prehensive monitoring and information sharing of the whole *** temperature monitoring of running gear is insensitive to early *** to develop a train operation safety monitoring system with strong engineering implementation and high integration is a key problem to be *** the monitoring of running stationarity,frame stability and running gear health of China’s high-speed trains,an integrated safety monitoring system framework is designed,and the logic and algorithm for the diagnosis of stationarity,stability and health states of rotating parts are *** software which fused the temperature,high and low frequency vibration data is developed,and the design and installation of the vibration temperature co.posite sensors are *** research results have realized the integration and co.prehensive processing of multiple monitoring systems,co.pleted the improvement from single co.ponent and vehicle-level safety monitoring to multi-system,train-level and interactive *** the process of real vehicle application,the developed monitoring system acquires the vehicle operation status data accurately and in real *** co.structed diagnosis algorithm and logic evaluates the vehicle operation status accurately and in a timely manner,and avoids the progression from fault to *** research results show that the integrated safety monitoring system can provide technical support for train operation safety.

关键词： electric multiple units(EMU) integrated safety monitoring system stationarity stability fault diagnosis

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锌基镀层热成形钢裂纹的产生、扩展机理及高温力学性能研究

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Journal of Central South University 2024年第2期31卷 399-415页

作者：李学涛朱国森马闻宇邵蓉张永强郑学斌 Research Institute of Technology of shougang group co. Ltd.Beijing 100043China Beijing Key Laboratory of Green Recycling Process for Iron&Steel Production Technology Beijing 100043China Beijing Engineering Research Centre of Energy Steel Beijing 100043China

本文通过锌基镀层热成形钢的Gleeble试验和实际零件热冲压试验,在材料高温性能分析的基础上,建立了材料模型,用于高精度地拟合真应力和真应变之间的关系,进而研究成形温度、铁素体形成和弯曲变形对液态锌致基板脆裂(LMIE)的影响。结果表... 详细信息

本文通过锌基镀层热成形钢的Gleeble试验和实际零件热冲压试验,在材料高温性能分析的基础上,建立了材料模型,用于高精度地拟合真应力和真应变之间的关系,进而研究成形温度、铁素体形成和弯曲变形对液态锌致基板脆裂(LMIE)的影响。结果表明,真应力随着变形温度的下降而增加。当变形温度为820℃时,LMIE导致真应变较低,约为0.13。根据Gleeble热模拟测试和实际零件试验结果,建议成形温度为720℃,可以避免LMIE并保证材料的力学性能。在实际应用中,拉应力容易导致微裂纹的产生,而压应力可以抑制微裂纹的产生。随着成形温度的降低,镀层中微裂纹的数量和宽度降低,同时镀层厚度增加。镀层主要为固态α-Fe(Zn)相。通过减少在加热保温和成形过程中的液态相可以减少甚至避免LMIE裂纹的产生。

关键词：热成形钢锌基镀层断裂直接热冲压微观组织

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