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Power characteristics of multiple inductively coupled RF discharges inside a metallic chamber

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Plasma Science and Technology 2022年第1期24卷 70-76页

作者： Dane LOJEN Rok ZAPLOTNIK Miran MOZETIC Alenka VESEL Gregor PRIMC Department of Surface Engineering Jozef Stefan InstituteJamova cesta 391000 LjubljanaSlovenia jozef stefan international postgraduate school Jamova cesta 391000 LjubljanaSlovenia Plasmadis Ltd. Teslova ulica 301000 LjubljanaSloven

The characteristics of an innovative configuration of multiple radiofrequency(RF)coils immersed in a large metallic chamber are ***-cooled copper coils were mounted within the slits of double-walled glass tubes,which were immersed into a stainless-steel *** coils were connected in parallel to a gamma-type matching network,powered by an RF generator operating at industrial *** leads enabled optimisation of the line impedances and thus uniformly distributed RF power across the four *** from E-to H-mode and vice versa were measured for all coils at various oxygen pressures between 5 and 25 Pa.A uniform plasma was sustained in H-mode at the absorbed power threshold,which increased monotonously with increasing pressure in the metallic *** coils exhibit the same E-to H-mode transition hysteresis and need the same amount of power for transitioning from E-to *** setup enables maintaining uniform plasma in virtually any number of coils at high power without the risk of arcing and without the dead volume typical for a classical configuration with coils mounted outside the metallic chamber.

关键词： inductively coupled plasma large-area plasma E-to H-mode transition high power

Advancing Li-ion storage performance with hybrid vertical carbon/Ni_(3)S_(2)-based electrodes

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Journal of Energy Chemistry 2022年第4期31卷 8-18页

作者： Neelakandan M.Santhosh Nitheesha Shaji d Petra Stražar Gregor Filipič Janez Zavašnik Chang Won Ho Murugan Nanthagopal Chang Woo Lee UrošCvelbar Department of Gaseous Electronics(F6) Jožef Stefan InstituteJamova cesta 39SI-1000 LjubljanaEUSlovenia Jožef stefan international postgraduate school Jamova cesta 39SI-1000 LjubljanaEUSlovenia Faculty of Mathematics and Physics University of LjubljanaJadranska cesta 19SI-1000 LjubljanaEUSlovenia Department of Chemical Engineering(Integrated Engineering) College of EngineeringKyung Hee University1732 Deogyeong-daeroGiheungYonginGyeonggi 17104South Korea Center for the SMART Energy Platform College of EngineeringKyung Hee University1732 Deogyeong-daeroGiheungYonginGyeonggi 17104South Korea

Conversion-reaction induced charge storage mechanisms of transition metal sulphides have received considerable interest in designing high-capacity electrodes for electrochemical energy storage ***,their low conductivity and structural degradation during cycling limit their applications as energy storage devices.A combination of different nickel sulphide phases tailored with carbon nanostructures is suggested to address these ***,a facile,two-step approach is demonstrated for fabricating a hybrid electrode,consisting of trinickel disulphide(Ni_(3)S_(2))formed on a metallic Ni nanoparticle supported by vertical carbon nanotubes(VCN)backbone in the form Ni_(3)S_(2)/Ni@***_(3)S_(2)/Ni@VCN electrodes were tested as anode for lithium-ion batteries,and the electrode featured outstanding lithiumstorage capabilities with a high reversible capacity(1113 m Ah g^(-1) after 100 cycles at 100 m A g^(-1)),excellent long-term cycling stability(770 m Ah g^(-1) after 500 cycles at 200 m A g^(-1)),and good rate *** resulting electrode performance is one of the best Li-ion storage capabilities in the Ni_(3)S_(2)-type anode materials described.A unique “broccoli-like”structure of polycrystalline Ni_(3)S_(2)capped on conductive VCN backbone helps the interface storage process and boosts lithium storage performance.

关键词： Ni_(3)S_(2) Vertical carbon nanostructures Hierarchical structures Binder-free electrode Lithium-ion batteries

Particle size dependent sinterability and magnetic properties of recycled HDDR Nd-Fe-B powders consolidated with spark plasma sintering

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Journal of Rare Earths 2020年第1期38卷 90-99页

作者： Awais Ikram Farhan Mehmood Richard Stuart Sheridan Muhammad Awais Allan Walton Anas Eldosouky Saso Sturm Spomenka Kobe Kristina Zuzek Rozman Department for Nanostructured Materials Jozef Stefan InstituteJamova 39SI-1000 LjubljanaSlovenia jozef stefan international postgraduate school Jamova 39SI-1000 LjubljanaSlovenia school of Metallurgy and Materials University of BirminghamEdgbastonBirminghamB152TTUnited Kingdom Magneti Ljubljana d.d.Stegne 37SI-1000 LjubljanaSlovenia

The dependence of the magnetic properties on the particle size of recycled HDDR Nd-Fe-B powders was investigated,with the aim to assess the reprocessing potential of the end-of-life scrap magnets via spark plasma sintering(SPS).The as received recycled HDDR powder has coercivity(Hci)=830 kA/m and particles in the range from 30 to 700 μm(average 220 μm).After burr milling,the average particle size is reduced to 120 μm and subsequently the Hci of fine(milled) powder was 595 kA/*** plasma sintering was exploited to consolidate the nanograined HDDR powders and limit the abnormal grain *** optimal SPS-ing of coarse HDDR powder at 750℃for 1 min produces fully dense magnets with Hci=950±100 kA/m which further increases to 1200 kA/m via thermal treatment at 750℃for 15 *** burr milled fine HDDR powder under similar SPS conditions and after thermal treatment results in Hci=940 kA/*** fine powder is further sieved down from 630 to less than 50 μm mesh size,to evaluate the possible reduction in Hci in relation to the particle *** gain in oxygen content doubles for 200 μm).The XRD analysis for fractionated powder indicates an increase in Nd2O3 phase peaks in the finer(200 μm) to 460 kA/m in the fine sized particles(200 μm) is higher than 930 kA/m and it falls abruptly to just 70 kA/m for the fine sized particles(1000 kA/m only up to 100 μm sized fractions with>90% sintered *** full densification(>99%) is observed only in the coarse *** loss of coercivity and lack of sinterability in the fine sized particles(<100 μm) are attributed to a very high oxygen *** implies that durin

关键词： Reprocessing end-of life scrap Rare earth permanent magnets HDDR Nd2Fe14B Recycling Spark plasma sintering

Stable dielectric response in lead-free relaxor K_(0.5)Na_(0.5)NbO_(3)-SrTiO_(3) thin films

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Journal of Advanced Dielectrics 2014年第2期4卷 41-45页

作者： A.Eršte A.Kupec B.Kmet B.Malič V.Bobnar Condensed Matter Physics Department Jozef Stefan Institute Jamova cesta 39SI-1000 LjubljanaSlovenia Electronic Ceramics Department Jozef Stefan Institute Jamova cesta 39SI-1000 LjubljanaSlovenia jozef stefan international postgraduate school jamova cesta 39 SI-1000 LjubljanaSlovenia

K_(0.5)Na_(0.5)NbO_(3)-SrTiO_(3)(KNN-STO)thin films of different compositions were prepared by the chemical solution deposition *** structural investigations confirmed the formation of perovskite solid solution in all developed films,dieletric experiments revealed a relaxor broad dispersive maximum in the sample with 15 mol%of STO,exhibiting for a thin film high ε′~330 at~*** history-dependent effects of this relaxor sample were compared to those of KNN STO ceramics and,furthermore,shown to be much weaker than in widely used lead-based ferroelectric and relaxor(Pb,L a)(Zr,Ti)O_(3) ceramics:While fatigue endurance results revealed a slight drop in polarization after 3 × 10^(5) switching cycles,the results of aging of the dielectric constant revealed no notable decrease in its values after 10^(6)s.

关键词： Lead-free ceramic thin films relaxor ferroelectrics electrical fatigue and aging

N-Graphene Nanowalls via Plasma Nitrogen Incorporation and Substitution: The Experimental Evidence

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Nano-Micro Letters 2020年第4期12卷 92-108页

作者： Neelakandan MSanthosh Gregor Filipič Eva Kovacevic Andrea Jagodar Johannes Berndt Thomas Strunskus Hiroki Kondo Masaru Hori Elena Tatarova UrošCvelbar Jožef stefan Institute Jamova cesta 391000 LjubljanaSlovenia Jožef stefan international postgraduate school Jamova cesta 391000 LjubljanaSlovenia GREMI CNRS-University of Orleans 14 rue d’Issoudun45067 Orleans Cedex 2France Institute for Materials Science Christian Albrechts University KielKaiserstr224143 KielGermany Department of Electrical Engineering and Computer Science University of NagoyaFuro‑cho Chikusa‑kuNagoyaAichi 464‑8603Japan Instituto de Plasmas e Fusão Nuclear Instituto Superior TécnicoUniversidade de Lisboa1049 LisbonPortugal

Incorporating nitrogen(N)atom in graphene is considered a key technique for tuning its electrical ***,this is still a great challenge,and it is unclear how to build N-graphene with desired nitrogen *** is a lack of experimental evidence to explain the influence and mechanism of structural defects for nitrogen incorporation into graphene compared to the derived DFT ***,this gap is bridged through a systematic study of different nitrogen-containing gaseous plasma post-treatments on graphene nanowalls(CNWs)to produce N-CNWs with incorporated and substituted *** structural and morphological analyses describe a remarkable difference in the plasma–surface interaction,nitrogen concentration and nitrogen incorporation mechanism in CNWs by using different nitrogen-containing *** conductivity measurements revealed that the conductivity of the N-graphene is strongly influenced by the position and concentration of C–N bonding *** findings open up a new pathway for the synthesis of N-graphene using plasma post-treatment to control the concentration and configuration of incorporated nitrogen for application-specific properties.

关键词： Graphene Graphene nanowalls Plasma post-treatment Nitrogen incorporation Raman spectroscopy Vacancy defects

Plasma-enabled sensing of urea and related amides on polyaniline

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Frontiers of Chemical Science and Engineering 2016年第2期10卷 265-272页

作者： Harinarayanan Puliyalil Petr Slobodian Michal Sedlacik Ruhan Benlikaya Pavel Riha Kostya (Ken) Ostrikov Uros Cvelbar jozef stefan Institute (F4) Jamova cesta 39 1000 Ljubjana Slovenia jozef stefan international postgraduate school Jamova cesta 39 1000 Ljubjana Slovenia Centre of Polymer Systems University Institute Tomas Bata University Trida T. Bati 5678 76001 Zlin Czech Republic Department of Secondary Science and Mathematics Education Faculty of Necatibey Education Balikesir University 10100 Balikesir Turkey Institute of Hydrodynamics Academy of Sciences Pod Patankou 5 166 12 Prague 6 Czech Republic Institute for Future Environments and Institute for Health and Biomedical Innovation School of ChemistryPhysics and Mechanical Engineering Queensland University of Technology Brisbane Queensland 4000 Australia CSIRO-QUT Joint Sustainable Materials and Devices Laboratory Commonwealth Scientific and Industrial Research Organization New South Wales 2070 Australia school of Physics The University of Sydney Sydney New South Wales 2006 Australia

The atmospheric pressure plasma jet （APPJ） was used to enhance the sensitivity of industrially important polyaniline （PANI） for detection of organic vapors from amides. The gas sensing mechanism of PANI is operating on the basis of reversible protonation or deprotonation, whereas the driving force to improve the sensitivity after plasma modifications is unknown. Herein we manage to solve this problem and investigate the sensing mechanism of atmospheric plasma treated PANI for vapor detection of amides using urea as a model. The results from various analytical techniques indicate that the plausible mechanism responsible for the improved sensi- tivity after plasma treatment is operating through a cyclic transition state formed between the functional groups introduced by plasma treatment and urea. This transition state improved the sensitivity of PANI towards 15 ppm of urea by a factor of 2.4 times PANI. This plasma treated compared to the non-treated PANI is promising for the improvement of the sensitivity and selectivity towards other toxic and carcinogenic amide analytes for gas sensing applications such as improving material proces- sing and controlling food quality.

关键词： gas sensing urea PANI amides plasma