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Integration of Electrical Properties and Polarization Loss Modulation on Atomic Fe–N‑RGO for Boosting Electromagnetic Wave Absorption

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Nano-Micro Letters 2025年第2期17卷 517-532页

作者： Kaili Zhang Yuefeng Yan Zhen Wang Guansheng Ma Dechang Jia Xiaoxiao Huang Yu Zhou State Key Laboratory of Precision welding&Joining of Materials and Structures Harbin Institute of TechnologyHarbin 150001People’s Republic of China School of Materials Science and Engineering Harbin Institute of TechnologyHarbin 150001People’s Republic of China MIIT Key Laboratory of Advanced Structural‑Functional Integration Materials&Green Manufacturing Technology Harbin Institute of TechnologyHarbin 150001People’s Republic of China

Developing effective strategies to regulate graphene’s conduction loss and polarization has become a key to expanding its application in the electromagnetic wave absorption(EMWA)*** on the unique energy band structure of graphene,regulating its bandgap and electrical properties by introducing heteroatoms is considered a feasible ***,metal-nitrogen doping reduced graphene oxide(M–N-RGO)was prepared by embedding a series of single metal atoms M–N_(4) sites(M=Mn,Fe,Co,Ni,Cu,Zn,Nb,Cd,and Sn)in RGO using an N-coordination atom-assisted *** composites had adjustable conductivity and polarization to optimize dielectric loss and impedance matching for efficient EMWA *** results showed that the minimum reflection loss(RL_(min))of Fe–N-RGO reaches−74.05 dB(2.0 mm)and the maximum effective absorption bandwidth(EAB_(max))is 7.05 GHz(1.89 mm)even with a low filler loading of only 1 wt%.Combined with X-ray absorption spectra(XAFS),atomic force microscopy,and density functional theory calculation analysis,the Fe–N_(4) can be used as the polarization center to increase dipole polarization,interface polarization and defect-induced polarization due to d-p orbital hybridization and structural ***,electron migration within the Fe further leads to conduction loss,thereby synergistically promoting energy *** study demonstrates the effectiveness of metal-nitrogen doping in regulating the graphene′s dielectric properties,which provides an important basis for further investigation of the loss mechanism.

关键词： Electromagnetic wave absorption Fe-N-RGO Dipole polarization Conduction loss Impedance matching

Equivalent Activity Coefficient Phenomenon of Cerium Reacting with Lead or Bismuth in Ag, Cu and Zn Alloy

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Journal of Rare Earths 2002年第6期20卷 626-629页

作者：薛松柏钱乙余董健 National Key Laboratory of Advanced welding Production Technology Harbin Institute of Technology Harbin welding institute Harbin 150080 China Harbin welding institute

The relation between contents of cerium and impurity lead or bismuth to their activity coefficient in Ag, Cu and Zn-base alloy was calculated and analyzed by using the ternary system Chou model. The thermodynamic calculation results show that the 'equivalent activity coefficient phenomenon' emerges among the activity coefficient of solute in a certain range of cerium (or at a certain point) for the Ce-Pb-X and Ce-Bi-X (X=Ag, Cu or Zn) ternary alloy system. Under this condition, the activity coefficient of solute has nothing to do with its own concentration. The preliminary theoretical analysis to this phenomenon was also made.

关键词： cerium thermodynamics activity coefficient

Local melting mechanism and its effects on mechanical properties of friction spot welded joint for Al-Zn-Mg-Cu alloy

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Journal of Materials Science & Technology 2018年第1期34卷 185-191页

作者： Yunqiang Zhao Chungui Wang Jizhong Li Jinhong Tan Chunlin Dong Guangdong welding institute (China-Ukraine E.O.Paton institute of welding) Guangzhou 510651 China

Local melting and the eutectic film and liquation crack formation mechanisms during friction spot weld- ing （FSpW） of Al-Zn-Mg-Cu alloy were studied by both experiment and finite element simulation. Their effects on mechanical properties of the joint were examined. When the welding heat input was high, the peak temperature in the stir zone was higher than the incipient melting temperature of the Al-Zn-Mg-Cu alloy. This resulted in local melting along the grain boundaries in this zone. In the retreating stage of the welding process, the formed liquid phase was driven by the flowing plastic material and redistributed as a ＂U-shaped＂ line in the stir zone. In the following cooling stage, this liquid phase transformed into eutectic films and liquation cracks. As a result, a new characteristic of＂U＂ line that consisted of eutectic films and liquation cracks is formed in the FSpWjoin. This ＂U＂ line was located in the high stress region when the FSpW joint was loaded, thus it was adverse to the mechanical properties of the FSpW joint. During tensile shear tests, the ＂U＂ line became a preferred crack propagation path, resulting in the occurrence of brittle fracture.

关键词： Friction spot welding Numerical simulation Local melting Liquation crack Mechanical property

Achieving superior mechanical properties in friction lap joints of copper to carbon-fiber-reinforced plastic by tool offsetting

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Journal of Materials Science & Technology 2018年第9期34卷 1628-1637页

作者： L.H.Wu K.Nagatsuka K.Nakata Joining and welding Research institute Osaka University

It is a challenge to achieve a sound welded metal/carbon-fiber-reinforced thermoplastic（CFRTP） joint with high strength and few bubbles. In this study, sound lap joints of Cu and CFRTP were obtained by friction lap joining（FLJ） directly at rotation rates of 600-2000 rpm, with the welding tool at the joint center and offsetting the tool 7 mm away from the center toward the retreating side, respectively. Tool offsetting reduced the non-uniform temperature distribution in the lap joints resulting from the high conductivity of Cu, which not only enhanced the tensile shear force from 0.89-2.25 kN to 1.71-3.54 kN,with the maximum increasing rate of 135%, but also reduced the bubble area to only 19% of the original level of 2000 rpm. It is the first time to report a high-quality Cu/CFRTP joint with a high strength and few bubbles. The large increase of the strength after tool offsetting was attributed to the increase of the joining area, the decrease of bubbles and the decrease of the CFRTP degradation. The details on the generation,quantitative distribution and expulsion of the bubbles in the FLJ joints were discussed.

关键词： Hybrid joining Plastic Metal Carbon-fiber-reinforced plastic Properties

Numerical Analysis of welding Residual Stress and Distortion in Laser+GMAW Hybrid welding of Aluminum Alloy T-Joint

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Acta Metallurgica Sinica(English Letters) 2013年第3期26卷 352-360页

作者： Guoxiang XU Chuansong WU Xuezhou MA Xuyou WANG Key Laboratory of Advanced welding Technology of Jiangsu Province Jiangsu Univeristy of Science and Technology institute of Advanced welding Technology Shandong University Harbin welding institute China Academy of Machinery Science & Technology

A 3-D finite element model is developed to predict the temperature field and thermally induced residual stress and distortion in laser＋GMAW hybrid welding of 6061-T6 aluminum alloy T-joint. And the characteristics of residual stress distribution and deformation are numerically investigated. In the simulation, the heat source model takes into account the effect of joint geometric shape and welding torch slant on the heat flux distribution and a sequentially coupled thermo-mechanical method is used. The calculated results show that higher residual stress is distributed in and surround the weld zone. Its peak value is very close to the yield strength of base metal. Besides, a large deformation appears in the middle and rear part of the weldment.

关键词： Hybrid welding Residual stress welding distortion Aluminum alloy T-joint Numerical simulation

Indirect Measurement of Material Thermal and Mechanical Properties during welding

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Journal of Materials Science & Technology 2003年第Z1期19卷 173-175页

作者： Dongqing LI Jun TAO Qingguo Meng Hongyuan FANG State Key Laboratory of welding Harbin Institute of Technology 150001 Chins State Key Laboratory of Welding Harbin Institute of Technology 150001 Chins State Key Laboratory of Welding Harbin Institute of Technology 150001 Chins State Key Laboratory of Welding Harbin Institute of Technology 150001 Chins

By means of a newly developed non-contact detecting method, electronic speckle pattern interferometry (ESPI), a method of determining material property data during welding is studied. A TIG fixed-point welding process is modeled in which some achievements of simulation, such as the effect of welding pool on temperature field and nonlinear relation between convection coefficient and temperature, are all considered. In addition, by taking into account effect of heating rate, the workpiece is divided into near-weld zone and far-weld zone, which will be treated with different property values. When the displacement field computed with original property data is compared and matched with the experimental displacement field, which is measured by ESPI, these original data are adjusted properly. A group of raw properties are obtained and are corrected by statistical regression before they enter the simulation process *** such a loop of "simulation-comparison-modification", a set of property data that best satisfy the real condition are achieved finally. In such a way, a new method for measuring material properties during welding is found.

关键词： Material properties, welding displacement field, Numerical simulation, ESPI

Self-adjusting dynamic characteristics of pulsed MIG welding for aluminum alloys

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中国有色金属学会会刊：英文版 2004年第1期14卷 111-115页

作者：包晔峰周昀吴毅雄楼松年 welding Engineering institute Shanghai Jiaotong University

Pulsed MIG welding is suitable for aluminum alloys welding, because spray transfer and excellent profile can be arrived during whole welding current range, and the energy of droplet can be controlled to overcome losing of alloy elements with lower melting and steam point by controlling pulse current and pulse time. Because of the special physic properties of aluminum alloys, there are different requirements for pulsed MIG welding between starting arc short circuit and drop transfer short circuit, pulse period and base period. In order to satisfy the need of aluminum alloys MIG welding, self adjusting dynamic characteristics are designed to output different dynamic characteristics in different welding startes. The self adjusting dynamic characteristics of pulsed MIG welding are achieved through a short circuit controller and a dynamic electronic inductor. The welding machine(AL MIG 350) with self adjusting dynamic characteristics has a high rate of successfully starting arc up to 96%, and the short circuit time during transfer is less than 1 ms, in the mean time, the arc is stiffness, spatter is low and weld appearance is good.

关键词： MIG焊铝合金动力学气体保护焊自调节动力特征

Microstructure Evolution and Tensile Properties of Ti_3Al/Ni-based Superalloy Welded Joint

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Journal of Materials Science & Technology 2014年第7期30卷 715-721页

作者： Bingqing Chen Huaping Xiong Bingbing Sun Siyi Tang Shaoqing Guo Xuejun Zhang Laboratory of welding and Forging Beijing Institute of Aeronautical Materials

In the present work, the dissimilar joining of a Ti3Al-based alloy to a Ni-based superalloy was attempted by gas tungsten arc （GTA） welding technology. Sound joints were successfully achieved by using a Cu-Ni alloy as filler material. According to X-ray energy dispersive spectroscopy and X-ray diffraction analysis results three transitional layers at the weld/Ti3Al interface were verified as follows： Ti2AlNb phase dissolved with Cu and Ni; Al（Cu,Ni）2Ti, （Cu,Ni）2Ti and （Nb, Ti） solid solution; Cu-rich phase and a complex multi-element phase. The In718/weld interface is characterized by solid solutions of Ni, Cu, Cr, Fe and Nb. The average tensile strength of the as-welded joints at room temperature is 163 MPa, and after a post-weld heat treatment it is increased slightly to 177 MPa. The fracture occurred at the surfacial layer of the joined Ti3Al base alloy, indicating that the Ti2AINb layer dissolved with Cu and Ni is the weak link of the Ti3Al/In718 joint.

关键词： Ti3Al-based alloy Ni-base superalloys welding Interface Microstructure Tensile properties

FEM SIMULATION FOR LASER FORMING PROCESSING

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Acta Metallurgica Sinica(English Letters) 2004年第3期17卷 317-322页

作者： L.Q.Li Y.B.Chen X.Y Wang S.Y Lin State Key Laboratory of Advanced welding Production Technology Harbin Institute of Technology Harbin 150001 China Harbin Research Institute of Welding Harbin 150001 ChinaState Key Laboratory of Advanced Welding Production Technology Harbin Institute of Technology Harbin 150001 China Harbin Research Institute of Welding Harbin 150001 ChinaHarbin Research Institute of Welding Harbin 150001 ChinaHarbin Research Institute of Welding Harbin 150001 China

Laser forming involves heating sheet metal workpiece along a certain path with adefocused laser beam directed irradiate to the surface. During laser forming, a tran-sient temperature fields is caused by the irradiation and travelling of a laser beam.Consequently, thermal expansion and contraction take place, and allows the thermal-mechanical forming of complex shapes. This is a new manufacturing technique thatforming metal sheet only by thermal stress. Therefore, the analysis of temperaturefields and stress fields are very useful for studying the forming mechanism and con-trolling the accuracy of laser forming. The non--liner finite element solver, MARC, isemployed to solve the thermal--mechanical analysis. Using this model, the stress andstrain distribution of pure aluminum plate with different thickness are analyzed. Theinfluence of scanning speed on temperature fields and plastic strain of metal sheet un-der the condition of constant line energy are also presented. Numerical results agreewell with the experimental results.

关键词： laser forming FEM simulation temperature fields stress distributton