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Bio-Oil Extracted of Wet Biomass of the Microalga Monoraphidiumsp. for Production of Renewable Hydrocarbons

Journal of Power and Energy Engineering 2019年第1期7卷 80-90页

作者： Yordanka R. Cruz Gisel Ch. Díaz Viviane de S. Borges Andreina Z. F. Leonett René G. Carliz Vinicius Rossa Vitor M. E. S. Silva Carolina Vieira Viegas Donato A. G. Aranda Luciano B. Oliveira greetec laboratory Federal University of Rio de Janeiro (UFRJ) Rio de Janeiro Brazil GCAT laboratory Federal University of Uberladia (UFU) Rio de Janeiro Brazil Research Company Energetic (EPE) Rio de Janeiro Brazil

Renewable hydrocarbons refer to fuels consisting of hydrocarbons of 10 to 20 carbon atoms, produced from biomass, and free of oxygen. Hydrocracking, hydrodeoxygenation and hydrotreatment processes for the production of renewable hydrocarbons are described in the literature. Microalgae have been targeted in recent years to synthesize biomass that can be used in the production of biofuels, such as renewable hydrocarbons, biodiesel or ethanol second generation. In this context the lineage Monoraphidium sp. was selected from previous ecophysiological studies and its potential to produce lipids to develop this research related with the extraction of the bio-oil of the wet biomass of Monoraphidium sp. through heat treatment. Consecutively the bio-oil was used as raw material for the production of hydrocarbons through hydrocracking and hydrodeoxygenation processes (HDO) as: decarbonylation, decarboxylation, dehydratation, with in situ production of hydrogen from liquid-phase reforming of glycerol. The reactions were carried out under two different temperature conditions, 350°C and 300°C, respectively, for 1 h and using ruthenium alumina catalyst (Ru/Al2O3). The results showed the bio-oil processing route at a temperature of 350°C promising for the production of hydrocarbons achieving a conversion of 81.54%.

关键词： Renewable Hydrocarbons Hydrotreatment Bio-Oil Monoraphidium sp.

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Hydroesterification of Nannochloropsis oculatamicroalga’s biomass to biodiesel on Al2O3supported Nb2O5catalyst

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Natural Science 2012年第4期4卷 204-210页

作者： Angel Almarales Gisel Chenard Roberto Abdala Donato A. Gomes Yordanka Reyes Neyda Om Tapanes Ecology Department University of Málaga Málaga Spain greetec laboratory Federal University of Rio de Janeiro Rio de Janeiro Brazil Materials laboratory West Zone State University Center (UEZO) Rio de Janeiro Brazil

Hydroesterification process has been presented biodiesel production from oil the green microalga Nannochloropsis oculata raw materials. Biodiesel studied in this work is the main product got from the hydroesterification of biomass the Nannochloropsis oculata and was obtained from esterification of fatty acid (product of a hydrolysis reaction) with methanol. It was used as catalyst the niobic acid pure and supported on δ-aluminum. The product was evaluated by gas chromatography and other analyses. The optimum conditions found in the conversion (%) for the hydrolysis reactions of the biomass (92.3%). Better results were observed in the algae concentration 20%, lead at 300?C with 20% of catalyst. For esterification of fatty acids of Nannochloropsis oculata (92.24%), were observed the molar ratio methanol: fat acid 3, lead at 200°C with 20% of catalyst supported.

关键词： Biodiesel Microalgae Hydrolysis Esterification Nannochloropsis oculata

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Characterization of the Lipid Components in Desmodesmusand ScenedesmusStrains: Lipid Content, Lipid Classes and Fatty Acid Profile

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American Journal of Plant Sciences 2020年第12期11卷 2103-2121页

作者： Carolina Vieira Viegas Gisel Chenard Díaz Yordanka Reyes Cruz Leonardo Brantes Bacellar Mendes greetec laboratory Federal University of Rio de Janeiro (UFRJ) Rio de Janeiro Brazil CENPES/PETROBRAS—Leopoldo Américo Miguez de Mello Research Center Rio de Janeiro Brazil

The lipid composition in terms of the amount of neutral lipids, free fatty acids and polar lipid content is of great importance to make full use possible of this fraction and to define the suitability of its application, either as a raw material for fuel production, nutraceutical purposes or feed. In addition to the fatty components present in the lipid extract, other components may be included, such as: carotenoids, pigments and sterols. The microalgae studied in this work, Scenedesmus sp. and Desmodesmus sp., were subjected to the same growth conditions and evaluated for lipid content, quantification and diversity of lipid components as well as its fatty acid profile. For lipid determination two extraction methods were compared: the J: Schmid-Bondzynski-Ratzlaff and Bligh & Dyer method. For Desmodesmus sp. 5.43% ± 0.41% and 9.18% ± 0.33% of lipids were obtained on an ash-free dry weight basis and for Scenedesmus sp. 12.46% ± 0.38% and 8.16% ± 0.42% of lipids were obtained on an ash-free dry weight basis using for both methods J:

关键词： Microalgae Desmodesmus sp. Scenedesmus sp.

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Quantification of Lipid Content and Identification of the Main Lipid Classes Present in Microalgae Extracts Scenedesmus sp. for Obtaining Fatty Compounds for Biofuel Production

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Energy and Power Engineering 2020年第6期12卷 273-287页

作者： Carolina Vieira Viegas Leonardo Brantes Bacellar Mendes Rafael Richard João Gisel Chenard Díaz Donato A. G. Aranda Yordanka Reyes Cruz greetec laboratory Federal University of Rio de Janeiro (UFRJ) Rio de Janeiro Brazil CENPES/PETROBRáS—Leopoldo Américo Miguez de Mello Research Center Rio de Janeiro Brazil

Microalgae biomass has been reported in the literature as one of the most promising sources for obtaining different products of industrial interest such as lipids, fatty acids, carotenoids, proteins and fibers. The lipid fraction of microalgae comprises neutral lipids, free fatty acids and polar lipids. It is of great importance to estimate the composition of the lipid fraction to define the potential for use, either as a raw material for the production of biofuels or for use for nutraceuticals and/or food purposes. The microalgae Scenedesmus sp. cultivated in a photobioreactor, the sky open raceway type, was evaluated for lipid content, identification and quantification of lipid components obtained from different extracts. In the quantification of the lipid content, extraction methods were proposed without chemical treatment (use of solvents only) such as chloroform:methanol (2:1 v/v)—Bligh & Dyer, Ethanol, Ethyl acetate:Hexane (1:1 v/v) and others with chemical treatment such as J-Schmid-Bondzynski-Ratzlaff (acid) and saponification (basic). For the identification of the main lipid components present in the extracts, the Thin layer chromatography (TLC) technique was used. Th

关键词： Microalgae Lipids Extraction Saponifiable Compounds Biofuels

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