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Thermogravimetric,kinetic study and gas emissions analysis of the thermal decomposition of waste-derived fuels

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Journal of Environmental Sciences 2024年第3期137卷 155-171页

作者： Vadim V.Dorokhov Galina S.Nyashina Pavel A.Strizhak Heat and Mass Transfer Laboratory National Research Tomsk Polytechnic University30 Lenin AvenueTomsk 634050Russia

A wide range of wastes can potentially be used to generate thermal and electrical *** co-combustion of several types of waste as part of water-containing waste-derived fuels is a promising method for their *** this research,we use thermogravimetric analysis and differential scanning calorimetry to study the thermal behavior and kinetics of coal slime,biomass,waste oils,and blends on their *** also analyze the concentrations of gaseous *** results show that biomass,oils,and coal slime significantly affect each other in the course of their co-combustion when added to slurry *** preparation of coal-water slurry based on slime and water reduced the ignition and burnout temperature by up to 16%.Adding biomass and waste oils additionally stimulated the slurry ignition and burnout,which occurred at lower *** to dry coal slime,threshold ignition temperatures and burnout temperatures decreased by 6%–9%and 17%–25%,***,the use of biomass and waste oils as part of slurries inhibited NOхand SO_(2)emission by 2.75 *** to the kinetic analysis,added biomass and waste turbine oil provide a 28%–51%reduction in the activation energy as compared to a coal-water slurry without additives.

关键词： Coal-water slurry Water-containing composite fuels Combustion Emission Kinetic TGA-DSC

A comparative study of the pore characteristics and phenol adsorption performance of activated carbons prepared from oil-palm shell wastes by steam and combined steam-chemical activation

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Green Chemical Engineering 2024年第1期5卷 85-96页

作者： Aik Chong Lua School of Mechanical and Aerospace Engineering Nanyang Technological University50 Nanyang AvenueSingapore639798Republic of Singapore

Oil-palm shell wastes were successfully converted into useful activated carbons in a systematic and novel approach by optimizing the pyrolysis conditions and subsequent steam activation conditions to maximize the BET surface *** optimal activation conditions were a steam flow rate of 1.13 kg/h,hold time of 1.5 h and temperature of 950℃,yielding BET areas of 1432.94 and 1382.95 m^(2)/g for nitrogen-pyrolyzed and vacuumpyrolyzed chars,*** steam-chemical activation,one-step activation of oil-palm shell in steam with potassium carbonate(K_(2)CO_(3)),sodium carbonate(Na_(2)CO_(3))or potassium chloride(KCl)was conducted,resulting in BET area output order of shell/K_(2)CO_(3)(710.56 m^(2)/g)>shell/KCl(498.55 m^(2)/g)>shell(366.7 m^(2)/g)>shell/Na_(2)CO_(3)(326.62 m^(2)/g).This study reported the first use of KCl and Na_(2)CO_(3)as chemical reagents in one-step steam-chemical activation of ***-activated carbon exhibited retardation of tar formation property,resulting in better pore development than pure steam activated *** adsorption of activated carbon is not only a function of the BET surface area but also the type of pyrolysis used prior to physical *** carbon(BET area of 1192.29 m^(2)/g)pyrolyzed under vacuum could adsorb 87%more phenol than that pyrolyzed in nitrogen flow which had a higher BET area of 1432.94 m^(2)/*** adsorption capacities of activated carbons are:shell pyrolyzed under vacuum(275.5 mg/g)>shell pyrolyzed in N_(2)flow(147.1 mg/g)>shell/K_(2)CO_(3)(145.7 mg/g)>shell without pyrolysis(12.1 mg/g).These activated carbons would be highly suitable in industry processes to remove phenolic contaminants.

关键词： Pore surface area Oil-palm shell Activated carbon Steam activation Phenol adsorption

Synthetic polymers:A review of applications in drilling fluids

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Petroleum Science 2024年第1期21卷 475-518页

作者： Shadfar Davoodi Mohammed Al-Shargabi David A.Wood Valeriy S.Rukavishnikov Konstantin M.Minaev School of Earth Sciences&Engineering Tomsk Polytechnic UniversityLenin AvenueTomskRussia DWA Energy Limited LincolnUnited Kingdom

With the growth of deep drilling and the complexity of the well profile,the requirements for a more complete and efficient exploitation of productive formations increase,which increases the risk of various ***,reagents based on modified natural polymers(which are naturally occurring compounds)and synthetic polymers(SPs)which are polymeric compounds created industrially,are widely used to prevent emerging complications in the drilling ***,compared to modified natural polymers,SPs form a family of high-molecular-weight compounds that are fully synthesized by undergoing chemical polymerization *** provide substantial flexibility in their ***,their size and chemical composition can be adjusted to provide properties for nearly all the functional objectives of drilling *** can be classified based on chemical ingredients,type of reaction,and their responses to ***,some of SPs,due to their structural characteristics,have a high cost,a poor temperature and salt resistance in drilling fluids,and degradation begins when the temperature reaches 130℃.These drawbacks prevent SP use in some medium and deep ***,this review addresses the historical development,the characteristics,manufacturing methods,classification,and the applications of SPs in drilling *** contributions of SPs as additives to drilling fluids to enhance rheology,filtrate generation,carrying of cuttings,fluid lubricity,and clay/shale stability are explained in *** mechanisms,impacts,and advances achieved when SPs are added to drilling fluids are also *** typical challenges encountered by SPs when deployed in drilling fluids and their advantages and drawbacks are also *** issues also impact the applications of SPs in drilling ***,the cost of the most relevant SPs,and the monomers used in their synthesis,are *** impacts of SPs when deployed in drilling fluids,and t

关键词： Synthetic versus natural polymers Nanopolymers Drilling fluid additives Lubricity Clay swelling Hole cleaning

Surface Metallization of Glass Fiber(GF)/Polyetheretherketone(PEEK) Composite with Cu Coatings Deposited by Magnetron Sputtering and Electroplating

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Journal of Wuhan University of Technology(Materials Science) 2024年第1期39卷 213-220页

作者：钟利金凡亚朱剑豪 TONG Honghui DAN Min Southwest Institute of Physics Chengdu 610000China City University of Hong Kong Tat Chee AvenueKowloonHong Kong 999077China

Surface metallization of glass fiber(GF)/polyetheretherketone(PEEK)[GF/PEEK] is conducted by coating copper using electroplating and magnetron sputtering and the properties are determined by X-ray diffraction(XRD), scanning electron microscopy(SEM), and electron backscatter diffraction(EBSD).The coating bonding strength is assessed by pull-out tests and scribing in accordance with GB/T *** results show that the Cu coating with a thickness of 30 μm deposited on GF/PEEK by magnetron sputtering has lower roughness, finer grain size, higher crystallinity, as well as better macroscopic compressive stress,bonding strength, and electrical conductivity than the Cu coating deposited by electroplating.

关键词： surface metallization Cu coating magnetron sputtering electroplating

Chemical Synthesis of a Key Precursor Relevant to the Tetrasaccharide Repeating Unit from Treponema medium ATCC 700293

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Chinese Journal of Chemistry 2024年第14期42卷 1615-1622页

作者： Wenbin Sun Guangzong Tian Meiru Ding Chunjun Qin Xiaopeng Zou Jing Hu Jian Yin Key Laboratory of Carbohydrate Chemistry and Biotechnology Ministry of EducationSchool of Biotechnology&School of Life Sciences and Health EngineeringJiangnan UniversityLihu Avenue 1800WuxiJiangsu214122 China Wuxi School of Medicine Jiangnan UniversityLihu Avenue 1800WuxiJiangsu214122 China

Treponema is a Gram-negative anaerobic bacterium,among which the pathogenic Treponema can cause various diseases,such as venereal syphilis(Treponema pallidum),yaws(Treponema carateum),and oral diseases(Treponema denticola and Treponema medium).Although different from conventional lipopolysaccharides,the extracellular glycoconjugate of Treponema may still be a potential antigen and provide a candidate for vaccine ***,we completed the first chemical synthesis of Treponema medium ATCC 700293 tetrasaccharide precursor containing L-ornithine(L-Orn)and D-aspartic acid(D-Asp)*** efficiency of non-reducing end disaccharide formation has been improved by optimizing the assembly of the protecting groups in the donors and ***[3+1]glycosylation strategy attempted to reduce the length of the acceptor to increase the nucleophilicity of the hydroxyl group,thereby improving the efficiency of synthesizing the target *** L-Orn derivative was introduced at the final stage due to its influence on the glycosylation stereospecificity and ***,the successful introduction of two amino acid derivatives and the synthesis of a tetrasaccharide precursor with complex functional-group modifications have provided valuable insights for synthesizing other complex bacterial glycans.

关键词： Glycosylation Total synthesis Treponema medium ATCC 700293 Tetrasaccharide precursor Protecting group Oligosaccharides Regioselectivity Neighboring-group effects

Topological Dirac-vortex microcavity laser for robust on-chip optoelectronics

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Light(Science & Applications) 2024年第4期13卷 591-592页

作者： Yuanpeng Wu Zetian Mi Department of Electrical Engineering and Computer Science University of Michigan1301 Beal AvenueAnn ArborMI 48109USA

Dirac-vortex microcavity laser based on InAs/InGaAs quantum dots have been experimentally realized on silicon *** topological laser features a large spectral range and high robustness against variations such as cavity... 详细信息

关键词： laser optoelectronics cavity

Endoscopic treatment of biliopancreatic pathology in patients with Whipple's pancreaticoduodenectomy surgical variants: Lessons learned from single-balloon enteroscopy-assisted ERCP

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Hepatobiliary & Pancreatic Diseases International 2024年第5期23卷 509-514页

作者： Rodrigo Garcés-Durán Laurent Monino Pierre H Deprez Hubert Piessevaux Tom G Moreels Department of Gastroenterology and Hepatology Universitécatholique de LouvainCliniques Universitaires Saint-LucAvenue Hippocrates 101200 BrusselsBelgium

Background: Endoscopic treatment of biliopancreatic pathology is challenging due to surgically altered anatomy after Whipple's pancreaticoduodenectomy. This study aimed to evaluate the feasibility and safety of single-balloon enteroscopy-assisted endoscopic retrograde cholangiopancreatography(SBE-ERCP) to treat biliopancreatic pathology in patients with Whipple's pancreaticoduodenectomy surgical variants. Methods: We retrospectively analyzed 106 SBE-ERCP procedures in 46 patients with Whipple's variants. Technical and clinical success rates and adverse events were evaluated. Results: Biliary SBE-ERCP was performed in 34 patients and pancreatic SBE-ERCP in 17, including 5 with both indications. From a total of 106 SBE-ERCP procedures, 76 were biliary indication with technical success rate of 68/76(90%) procedures and clinical success rate of 30/34(88%) patients. Mild adverse event rate was 8/76(11%), without serious adverse events. From a total of 106 SBE-ERCP procedures, 30 were pancreatic indication with technical success rate of 24/30(80%) procedures( P = 0.194 vs. biliary SBEERCP) and clinical success rate of 11/17(65%) patients( P = 0.016 vs. biliary SBE-ERCP). Mild adverse event rate was 6/30(20%)( P = 0.194 vs. biliary SBE-ERCP), without serious adverse events. After SBE-ERCP failure, endoscopic ultrasound-guided drainage, percutaneous drainage and redo surgery were alternative therapeutic options. Conclusions: Biliopancreatic pathology after Whipple's pancreaticoduodenectomy variants can be treated using SBE-ERCP without serious adverse events. Technical and clinical success rates are high for biliary indications, whereas clinical success rate of pancreatic indications is significantly lower. SBE-ERCP can be considered as first-line treatment option in this patient group with surgically altered anatomy.

关键词： Enteroscopy Endoscopic retrograde cholangiopancreatography Pancreaticoduodenectomy Surgically altered anatomy Whipple’s procedure

Efficient fidelity estimation:alternative derivation and related applications

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Communications in Theoretical Physics 2024年第9期76卷 16-20页

作者： Diego S Starke Marcos L W Basso Jonas Maziero Physics Department Center for Natural and Exact SciencesFederal University of Santa MariaRoraima Avenue 1000Santa MariaRS97105-900Brazil Center for Natural and Human Sciences Federal University of ABCAvenue of the StatesSanto AndréSão Paulo09210-580Brazil

In[***.A 107012427(2023)],Baldwin and Jones prove that Uhlmann–Jozsa’s fidelity between two quantum statesρandσ,i.e.,F(ρ,σ)=(Tr√√ρσ√ρ)^(2),can be written in a simplified form as F(ρ,σ)=(Tr√ρσ)^(2).In this article,we give an alternative proof of this result,using a function power series expansion and the properties of the trace *** approach not only reinforces the validity of the simplified expression but also facilitates the exploration of novel dissimilarity functions for quantum states and more complex trace functions of density operators.

关键词： Ulhmann–Jozsa fidelity Rényi entropy efficient fidelity estimation Chebyshev polynomials

Impact of the Brink-Axel hypothesis on unique first-forbiddenβ-transitions for r-process nuclei

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Chinese Physics C 2024年第3期48卷 148-168页

作者： Fakeha Farooq Jameel-Un Nabi Ramoona Shehzadi Department of Physics University of the PunjabQuaid-e-Azam Campus 54590LahorePakistan University of Wah Quaid AvenueWah Cantt 47040PunjabPakistan

Key nuclear inputs for the astrophysical r-process simulations are the weak interaction ***,the accuracy of these inputs directly affects the reliability of nucleosynthesis *** majority of the stellar rates,used in simulation studies are calculated by invoking the Brink-Axel(BA)*** BA hypothesis assumes that the strength functions of all parent excited states are the same as for the ground state,only shifted in ***,the BA hypothesis has to be tested against microscopically calculated state-by-state *** this project,we study the impact of the BA hypothesis on calculated stellarβ^(-)-decay and electron capture *** investigation include both unique first forbidden(U1F)and allowed transitions for 106 neutron-rich trans-iron nuclei([27,77]≤[Z,A]≤[82,208]).The calculations were performed using the deformed proton-neutron quasiparticle random-phase approximation(pn-QRPA)model with a simple plus quadrupole separable and schematic ***-point and several key r-process nuclei lie within the considered mass region of the nuclear *** computed electron capture andβ^(-)-decay rates using two different prescriptions for strength *** was based on invoking the BA hypothesis and the other was the state-by-state calculation of strength functions,under stellar density and temperature conditions([10,1]≤[ρYe(g/cm^(3)),T(GK)]≤[10^(11),30]).Our results show that the BA hypothesis invoked U1Fβ^(-)rates are overestimated by 4–5 orders of magnitude as compared to microscopic *** capture rates,more than two orders of magnitude differences were noted when applying the BA *** was concluded that the BA hypothesis is not a reliable approximation,especially forβ^(-)-decay forbidden transitions.

关键词： Brink-Axel hypothesis pn-QRPA model unique first forbiddenβ-transitions GT strength functions trans-iron nuclei r-process