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Fabrication of plasmonic nanopyramidal array as flexible SERS substrate for biosensing application

Nano Research 2023年第1期16卷 1132-1140页

作者： Anindita Das Udit Pant Cuong Cao Rakesh SMoirangthem Hitesh Bhanudas Kamble Nanophotonics Lab Department of PhysicsIndian Institute of Technology(Indian School of Mines)Dhanbad-826004India Institute for Global Food Security School of Biological SciencesQueen’s University of Belfast19 Chlorine GardensBelfastBT95DLUK Material and Advanced Technologies for Healthcare Queen’s University of Belfast18-30 Malone RoadBelfastBT95BNUK IITB Nanofabrication Facility Department of Electrical EngineeringIndian Institute of TechnologyBombay-400076India

The proposed work aims to develop a sensitive surface-enhanced Raman spectroscopy(SERS)nano-biosensor.The inverted nano pyramid array on silicon substrate fabricated using electron beam lithography(EBL)was utilised as a master template and the mold was later replicated via nanoimprinting process to prepare gold-coated polymer nanopyramid three-dimensional(3D)SERS substrate.The fast and versatile replication process using nanoimprinting lithography(NIL)can produce polymer nanopyramids in a low-cost and reproducible fashion.Also,the proposed fabrication protocol can be easily upscale for large scale fabrication.The intense electric field confinement at nanotips and four edges of gold-coated polymer nanopyramid enhanced the Raman signal of probe molecules,i.e.,Rhodamine 6G with a limit of detection down to 3.277×10−9 M was achieved.This work also underlines the efficiency of gold-coated polymer nanopyramid arrays in the spectral detection of hemoglobin proteins at low concentrations.The Raman signal enhancement mechanism was further studied through the electromagnetic simulation using COMSOL Multiphysics.In addition,bending test experiments were performed to understand the effect of flexibility on SERS signal response.The fabricated gold-coated polymer nanopyramids arrays could pave the way for the development of low-cost SERS platforms for the detection of hazardous biological and chemical compounds at ultra-low concentrations in practical applications.

关键词： nanopyramids surface-enhanced Raman spectroscopy(SERS) flexible hemoglobin protein nanoimprinting replica molding

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Parallel Nanoimprint Forming of One-Dimensional Chiral Semiconductor for Strain-Engineered Optical Properties

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Nano-Micro Letters 2020年第11期12卷 242-254页

作者： Yixiu Wang Shengyu Jin Qingxiao Wang Min Wu Shukai Yao Peilin Liao Moon JKim Gary JCheng Wenzhuo Wu School of Industrial Engineering Purdue UniversityWest LafayetteIN 47907USA Flex Laboratory Purdue UniversityWest LafayetteIN 47907USA Department of Materials Science and Engineering University of Texas at DallasRichardsonTX 75080USA School of Materials Engineering Purdue UniversityWest LafayetteIN 47907USA Birck Nanotechnology Center Purdue UniversityWest LafayetteIN 47907USA Regenstrief Center for Healthcare Engineering Purdue UniversityWest LafayetteIN 47907USA

The low-dimensional,highly anisotropic geometries,and superior mechanical properties of one-dimensional(1D) nanomaterials allow the exquisite strain engineering with a broad tunability inaccessible to bulk or thin-film materials.Such capability enables unprecedented possibilities for probing intriguing physics and materials science in the 1-D limit.Among the techniques for introducing controlled strains in 1D materials,nanoimprinting with embossed substrates attracts increased attention due to its capability to parallelly form nanomaterials into wrinkled structures with controlled periodicities,amplitudes,orientations at large scale with nanoscale resolutions.Here,we systematically investigated the strain-engineered anisotropic optical properties in Te nanowires through introducing a controlled strain field using a resist-free thermally assisted nanoimprinting process.The magnitude of induced strains can be tuned by adjusting the imprinting pressure,the nanowire diameter,and the patterns on the substrates.The observed Raman spectra from the chiral-chain lattice of 1D Te reveal the strong lattice vibration response under the strain.Our results suggest the potential of 1D Te as a promising candidate for flexible electronics,deformable optoelectronics,and wearable sensors.The experimental platform can also enable the exquisite mechanical control in other nanomaterials using substrate-induced,on-demand,and controlled strains.

关键词： Chiral semiconductor Nanowires nanoimprinting Strain engineering Optical property

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Electric-driven flexible-roller nanoimprint lithography on the stress-sensitive warped wafer

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International Journal of Extreme Manufacturing 2023年第3期5卷 608-618页

作者： Yu Fan Chunhui Wang Jiaxing Sun Xiaogang Peng Hongmiao Tian Xiangming Li Xiaoliang Chen Xiaoming Chen Jinyou Shao Micro-and Nano-technology Research Center State Key Laboratory for Manufacturing Systems EngineeringXi'an Jiaotong UniversityXi’an 710049People’s Republic of China Frontier Institute of Science and Technology(FIST) Xi'an Jiaotong UniversityXi’an710049People’s Republic of China

Surface nanopatterning of semiconductor optoelectronic devices is a powerful way to improve their quality and performance.However,photoelectric devices’inherent stress sensitivity and inevitable warpage pose a huge challenge on fabricating nanostructures large-scale.Electric-driven flexible-roller nanoimprint lithography for nanopatterning the optoelectronic wafer is proposed in this study.The flexible nanoimprint template twining around a roller is continuously released and recovered,controlled by the roller’s simple motion.The electric field applied to the template and substrate provides the driving force.The contact line of the template and the substrate gradually moves with the roller to enable scanning and adapting to the entire warped substrate,under the electric field.In addition,the driving force generated from electric field is applied to the surface of substrate,so that the substrate is free from external pressure.Furthermore,liquid resist completely fills in microcavities on the template by powerful electric field force,to ensure the fidelity of the nanostructures.The proposed nanoimprint technology is validated on the prototype.Finally,nano-grating structures are fabricated on a gallium nitride light-emitting diode chip adopting the solution,achieving polarization of the light source.

关键词： nanoimprinting electric-driven flexible-roller warped stress-sensitive

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Biomimetic Moth-eye Anti-reflective Poly-(methyl methacrylate)Nanostructural Coating

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Journal of Bionic Engineering 2019年第6期16卷 1030-1038页

作者： Hongbo Xu Liuting Gong Shoucai Zhang Renping Ma Lei Pan Jiupeng Zhao Yao Li MIIT Key Laboratory of Critical Materials Technology for New Energy Conversion and Storage School of Chemistry and Chemical EngineeringHarbin Institute of TechnologyHarbin 150001China Beijing Institute of Space Mechanics and Electricity Beijing 100094China Beijing Vocational College of Labour and Social Security Beijing 102200China Center for Composite Material Harbin Institute of TechnologyHarbin 150001China

This study reports a simple imprinting method for the fabrication of biomimetic moth-eye antireflective polymethyl methacrylate(PMMA)nanostructures on the surface of the substrate.The antireflection structured silicon was obtained by Reactive Ion Etching(RIE)method.By using the antireflection structured silicon substrate as the imprinting stamp,the biomimetic moth-eye polymer structures showed tapered holes,whose depth and periodicity were around 780 nm and 580 nm,respectively.The reflectance of the resulting PMMA structures was reduced from 10% to less than 1% in the wavelength range from 300 nm to 1600 nm.This simple methodology can be scaled up via self-loading and nanoimprinting,which may have a promising application in optoelectronic devices and solar cells.

关键词： nanoimprinting sub-wavelength structure antireflective biomimetic moth-eye

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Nano-and Micro-patterned Biomaterials

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复旦学报（自然科学版） 2007年第5期46卷 706-页

作者： M.C.Lensen M.Diez V.A.Schulte P.Mela M.Mller DWI e.V.and Institute of Technical and Macromolecular Chemistry RWTH AachenGermany

1 Results Our objective is two fold: we (ⅰ) aim at the development of novel patterning methodologies in order to (ⅱ) achieve control over the positioning and alignment of living cells.The patterning of the biointerfaces is carried out both at the micro-and nanometer scale and involve (bio)chemical as well as topographic patterns.The former are relatively easily obtained by patterning techniques adapted from (conventional) soft lithography,e.***.by means of micro-contact printing (μ-CP).The topographic pat...

关键词： soft lithography hydrogels nanoimprinting UV-curing cell adhesion

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