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Determination of Young's modulus by nanoindentation

Science China(Technological Sciences) 2004年第4期47卷 398-408页

作者： MA Dejun1, Chung Wo Ong2, LIU Jianmin1 & HE Jiawen3 1. Surface Engineering Research Institute, CMES, Beijing 100072, China 2. Department of Applied Physics and Materials Research Center, The Hong Kong Polytechnic University, Hong Kong, China 3. State Key Laboratory for Mechanical Behavior of Materials, Xian Jiaotong University, Xian 710049, China Surface Engineering Research Institute CMES Beijing China Department of Applied Physics and Materials Research Center The Hong Kong Polytechnic University Hong Kong China State Key Laboratory for Mechanical Behavior of Materials Xi’an Jiaotong University Xi’an China

A methodology for determining Youngs modulus of materials by non-ideally sharp indentation has been developed. According to the principle of the same area-to-depth ratio, a non-ideally pyramidal indenter like a Berkovich one can be approximated by a non-ideally conical indenter with a spherical cap at the tip. By applying dimensional and finite element analysis to the non-ideally conical indentation, a set of approximate one-to-one relationships between the ratio of nominal hardness/reduced Youngs modulus and the ratio of elastic work/total work, which correspond to different tip bluntness, have been revealed. The nominal hardness is defined as the maximum indentation load divided by the cross-section area of the conical indenter specified at the maximum indentation depth. As a consequence, Youngs modulus can be determined from a nanoindentation test only using the maximum indentation load and depth, and the work done during loading and unloading processes. The new method for determining Youngs modulus is referred to as pure energy method. The validity of the method was examined by performing indentation tests on five materials. The experimental results and the standard reference values are in good agreement, indicating that the proposed pure energy method is a promising substitution for the most widely used analysis models at present.

关键词： Young's modulus, nanoindentation, nominal hardness, indentation work.

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Structural and mechanical properties of nano-crystal TiN coatings

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Science China(Physics,Mechanics & Astronomy) 2004年第Z1期47卷 1-7页

作者： ZHANG Chenhui PAN Guoshun LUO Jianbin LI Wenzhi CHEN Darong State Key Laboratory of Tribology Tsinghua University Beijing 100084 China State Key Laboratory of Tribology Tsinghua University Beijing 100084 China State Key Laboratory of Tribology Tsinghua University Beijing 100084 China State Key Laboratory of Tribology Tsinghua University Beijing 100084 China State Key Laboratory of Tribology Tsinghua University Beijing 100084 China

The structural and mechanical properties of TiN coatings prepared by ion beam assisted deposition (IBAD) were studied. The coatings have a polycrystal structure with grain size of ～10 nm or less. The hardness of the coatings increases with increasing grain size of TiN crystallites. The coating with grain size of 10.3 nm even has a superhardness of 44.7GPa. The relationship between the hardness and the grain size in the nano-crystalline coatings was discussed on the basis of grain-boundary triple junctions.

关键词： TiN, nano-crystal, microstructure, hardness, grain-boundary triple junctions.

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