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Effects of Corrosion Inhibitors on Lubrication Performance of Rolling Oil for copper foil

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China Petroleum Processing & Petrochemical Technology 2014年第2期16卷 71-78页

作者： Xiong Sang Sun Jianlin Zeng Yingfeng Xu Yang School of Materials Science and Engineering University of Science and Technology Beijing Research Institute of Petroleum Processing Sinopec Corp.

The 2,5-bis（ethyldisulfanyl）-l,3,4-thiadiazole （T561）, benzotriazole （BTA）,1-N, N-bis （2-ethylhexyl） aminomethyl-4-methyl-lh-benzotriazole （IRGAMET39） and I-IN, N-bis （2-ethylhexyl） aminomethyl] methyl benzotriazole （TT- LX） have been evaluated as corrosion inhibitors used in rolling oil for cold rolling of copper foil. The MRS-10A four-ball friction and wear tests have been carried out to compare their tribological properties, and the lubricating performance of rolling oils has been studied through rolling experiments. The oil sample containing IRGAMET 39 has the same PB value as that one containing T561, with the coefficient of friction increased by 35.6% and wear scar diameter decreased by 4%. The minimum rolling gauge has been studied after rolling lubrication, but the results show that inhibitors have no effect on it. Scanning electron microscopy （SEM） and energy dispersive spectrometry （EDS） analyses have indicated that the inhibitor is adsorbed on the copper surface to prevent copper from being corroded easily. In addition, the LEXT OLS4000 laser confocal microscopy has been used to observe the foil surface which shows that the streaks of foil surface are clear, the scratches are shallow and the surface failure is improved effectively.

关键词： copper foil corrosion inhibitor cold rolling surface topography lubrication

Purification of copper foils driven by single crystallization

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Chinese Physics B 2024年第2期33卷 506-511页

作者：寇金宗赵孟泽李兴光何梦林杨方友刘科海成庆秋任云龙刘灿付莹吴慕鸿刘开辉王恩哥 Songshan Lake Materials Laboratory Dongguan 523808China Beijing National Laboratory for Condensed Matter Physics Institute of PhysicsChinese Academy of SciencesBeijing 100190China Guangdong Provincial Key Laboratory of Quantum Engineering and Quantum Materials School of PhysicsSouth China Normal UniversityGuangzhou 510006China Guangdong–Hong Kong Joint Laboratory of Quantum Matter Frontier Research Institute for PhysicsSouth China Normal UniversityGuangzhou 510006China State Key Laboratory for Mesoscopic Physics Frontiers Science Center for Nano-optoelectronicsSchool of PhysicsPeking UniversityBeijing 100871China Key Laboratory of Quantum State Construction and Manipulation(Ministry of Education) Department of PhysicsRenmin University of ChinaBeijing 100872China International Center for Quantum Materials Collaborative Innovation Center of Quantum MatterPeking UniversityBeijing 100871China School of Physics Liaoning UniversityShenyang 110036China

High-purity copper(Cu) with excellent thermal and electrical conductivity, is crucial in modern technological applications, including heat exchangers, integrated circuits, and superconducting magnets. The current purification process is mainly based on the zone/electrolytic refining or anion exchange, however, which excessively relies on specific integrated equipment with ultra-high vacuum or chemical solution environment, and is also bothered by external contaminants and energy consumption. Here we report a simple approach to purify the Cu foils from 99.9%(3N) to 99.99%(4N) by a temperature-gradient thermal annealing technique, accompanied by the kinetic evolution of single crystallization of *** success of purification mainly relies on(i) the segregation of elements with low effective distribution coefficient driven by grain-boundary movements and(ii) the high-temperature evaporation of elements with high saturated vapor *** purified Cu foils display higher flexibility(elongation of 70%) and electrical conductivity(104% IACS) than that of the original commercial rolled Cu foils(elongation of 10%, electrical conductivity of ~ 100% IACS). Our results provide an effective strategy to optimize the as-produced metal medium, and therefore will facilitate the potential applications of Cu foils in precision electronic products and high-frequency printed circuit boards.

关键词： purification copper foil thermal annealing technique single crystallization

Growth of large-area aligned pentagonal graphene domains on high-index copper surfaces

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Nano Research 2016年第7期9卷 2182-2189页

作者： Kailun Xia Vasilii I. Artyukhov Lifei Sun Jingying Zheng Liying Jiao Boris I. Yakobson Yingying Zhang Department of Chemistry Tsinghua University Beijing 100084 China Center for Nano and Micro Mechanics Tsinghua University Beijing 100084 China Department of Materials Science and Nano Engineering Rice University Houston TX 77005 USA

Single-crystal graphene domains grown by chemical vapor deposition （CVD） intrinsically tend to have a six-fold symmetry; however, several factors can influence the growth kinetics, which can in turn lead to the formation of graphene with different shapes. Here we report the growth of oriented large-area pentagonal single-crystal graphene domains on Cu foils by CVD. We found that high-index Cu planes contributed selectively to the formation of pentagonal graphene. Our results indicated that lattice steps present on the crystalline surface of the underlying Cu promoted graphene growth in the direction perpendicular to the steps and finally led to the disappearance of one of the edges forming a pentagon. In addition, hydrogen promoted the formation of pentagonal domains. This work provides new insights into the mechanism of graphene growth.

关键词： pentagonal graphene copper foil high index plane chemical vapor deposition large area

Preparation of graphene on Cu foils by ion implantation with negative carbon clusters

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Chinese Physics B 2015年第1期24卷 528-530页

作者：李慧尚艳霞张早娣王泽松张瑞付德君 School of Physics and Technology and Key Laboratory of Artificial Micro- and Nano-Materials of Ministry of Education Wuhan University

We report on few-layer graphene synthesized on Cu foils by ion implantation using negative carbon cluster ions,followed by annealing at 950？C in vacuum. Raman spectroscopy reveals IG/I2 Dvalues varying from 1.55 to 2.38 depending on energy and dose of the cluster ions, indicating formation of multilayer graphene. The measurements show that the samples with more graphene layers have fewer defects. This is interpreted by graphene growth seeded by the first layers formed via outward diffusion of C from the Cu foil, though nonlinear damage and smoothing effects also play a role. Cluster ion implantation overcomes the solubility limit of carbon in Cu, providing a technique for multilayer graphene synthesis.

关键词： ion implantation carbon clusters graphene copper foil

High efficiency graphene nanoplates derivative nitrogen-doped graphene/copper composite film for thermal conductivity film

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High efficiency graphene nanoplates derivative nitrogen-dope...