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Journal of Natural Gas Chemistry 2010年第1期19卷 43-46页

作者： Lin Wang, Shunle Dong Physics department, college of Information Science and Engineering, Ocean university of china, qingdao 266100, Shandong, china [a] Physics department College of Information Science and Engineering Ocean University of China Qingdao 266100 Shandong China

INS （Inelastic Neutron Scattering） spectrum of methane hydrate was measured on MARI （a direct-geometry chopper spectrometer） at Ruther-ford Appleton Laboratory, UK. Compared with ice Ih, it is found that the whole spectrum of methane hydrate moves toward high-energy by about 1.5 meV. Using lattice dynamical （LD） technique, computer simulations of methane hydrate were carried out. In the simulations, four potential models （BE TIP3P, TIP4P, MCY） were employed to calculate the phonon density of states （PDOS）. Comparing the calculated PDOS spectrum with the experimental spectrum, it is found that BF, TIP4P, and TIP3P potential lattices give out well-separated translational and librational bands while MCY potential lattice is unstable to do so and this model is not suitable to describe hydrate system.

关键词： methane hydrate inelastic neutron scattering lattice dynamical simulation

Hepatocellular carcinoma HepG2 cell apoptosis and caspase-8 and Bcl-2 expression induced by injectable seed extract of Coix lacryma-jobi

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Hepatobiliary & Pancreatic Diseases International 2011年第3期10卷 303-307页

作者： department of general surgery (Lu Y and Zhang BY),department of Bio-Information (Jia ZX),Affiliated medical college hospital,qingdao university,qingdao 266003,china Shanghai Jiaotong university School of Medicine,Shanghai 200025,china (Wu WJ) department of Medicine,Heze medical college,Heze 274000,china (Lu ZQ) [a] department of general surgery Affiliated Medical College Hospital Qingdao University Qingdao 266003 China [b] department of Bio-Information Affiliated Medical College Hospital Qingdao University Qingdao 266003 China [c] Shanghai Jiaotong university School of Medicine Shanghai 200025 China [d] department of Medicine Heze Medical College Heze 274000 China

BACKGROUND:Many Chinese herbs,especially herbal injections,have been shown to have anti-tumor effects in recent ***,since most reports focus on the clinical effectiveness of these herbs,their mechanisms of action are not well *** this study,we assessed apoptosis in the hepatocellular carcinoma (HCC) cell line HepG2 induced by an injectable extract from the seed of Coix lacryma-jobi (Semen coicis,SC),and monitored the expression of Bcl-2 and ***:Injectable SC was applied to HepG2 cells at different concentrations and the cells were collected 12,24 and 48 hours later.5-fluorouracil was used as a positive control group,and fluorescence-activated cell-sorting cytometry was used to measure the apoptosis rate of HepG2 cells and the expression of Bcl-2 and caspase-8 ***:SC induced apoptosis in HepG2 cells in a concentration and time-dependent manner,and the expression of caspase-8 was elevated and ***,it did not significantly influence the expression of ***:Injectable SC may induce apoptosis in HCC cells by regulating the expression of caspase-8.

关键词： Semen coicis traditional Chinese medicine Bcl-2 caspase-8 HepG2 cells apoptosis

Muscarinic acetylcholine receptor M3 in proliferation and perineural invasion of cholangiocarcinoma cells

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Hepatobiliary & Pancreatic Diseases International 2012年第4期11卷 418-423页

作者： Yu-Jie Feng,Bing-Yuan Zhang,Ru-Yong Yao and Yun LuSecond department of general surgery and Central Laboratory of Molecular Biology,Affiliated medical college hospital,qingdao university,qingdao 266003,china [a] Second department of general surgery Affiliated Medical College Hospital Qingdao University Qingdao 266003 China [b] Second department of general surgery and Central Laboratory of Molecular Biology Affiliated Medical College Hospital Qingdao University Qingdao 266003 China

BACKGROUND:Cholangiocarcinoma,a type of malignant tumor,originates from epithelial cells of the bile *** invasion is common path for cholangiocarcinoma metastasis,and it is highly correlated with postoperative recurrence and poor *** has been reported that muscarinic acetylcholine receptor M3(mAChR M3) is widely expressed in digestive tract cancer,and may play an important role in the proliferation,differentiation,transformation and carcinogenesis of *** study was to explore the effect of mAChR M3 on the growth of cholangiocarcinoma cells in vitro and provide a new approach to the pathogenesis and treatment of ***:Streptavidin-biotin complex immunohistochemistry was carried out to assess the expression of mAChR M3 in surgical specimens of cholangiocarcinomas(40 cases) and normal bile duct tissues(9),as well as to investigate nerve *** cholangiocarcinoma cells were treated with different concentrations of selective M-receptor agonist pilocarpine and M-receptor blocker atropine sulfate to induce changes in cell *** experimental data were analyzed by the Chi-square ***:The strongly-positive expression rate of mAChR M3 was much higher in poorly-differentiated(69%,9/13) than in well-and moderately-differentiated cholangiocarcinomas(30%,8/27)(χ 2 =5.631,P28) was higher than that in cholangiocarcinomas from the middle and lower common bile duct(25%,3/12)(χ 2 =2.148,P2),which was much higher than those without distant metastasis(29%,8/28)(χ 2 =7.410,P<0.01).The absorbance value in the pilocarpine+atropine group was significantly higher than the corresponding value in the pilocarpine ***:The expression of mAChR M3 is influenced by the extent of differentiation,distant metastasis and the site

关键词： cholangiocarcinoma mAChR M3 immunohistochemistry perineural invasion proliferation

The extension of the first main theorem for π-blocks

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Science china Mathematics 2006年第5期49卷 620-625页

作者： HAI Jinke department of Mathematics, qingdao university, qingdao 266071, china college of mathematics ,Shandong university, Jinan 250100, china department of Mathematics Qingdao University Qingdao 266071 China college of mathematics Shandong University Jian 250100 China

Let π be a set of primes and G a π-separable group. Isaacs defines the Bπ characters, which can be viewed as the "π-modular" characters in G, such that the Bp′ characters form a set of canonical lifts for the p-modular characters. By using Isaacs' work, Slattery has developed some Brauer's ideals of p-blocks to the π-blocks of a finite π-separable group, generalizing Brauer's three main theorems to the π-blocks. In this paper, depending on Isaacs' and Slattery's work, we will extend the first main theorem for π-blocks.

关键词： π-block, π-separable group, π-regular classes, defect group.

Pre-ligation of afflicted hepatic inflow and outflow blood vessels of lesioned liver lobe during hepatectomy

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Hepatobiliary & Pancreatic Diseases International 2003年第3期2卷 358-361页

作者： Zhe-Fu Li Min Song the department of Hepatobiliary, qingdao Municipal hospital, qingdao university medical college, qingdao 266011, china department of Hepatobiliary Qingdao Municipal Hospital Qingdao University Medical College Qingdao 266011 China. lizhefu@***

OBJECTIVE: To compare the merits of hepatectomy after pre-ligation of the hepatic inflow and outflow blood vessels of the lesioned liver lobe with those of Pringle's maneuver. METHODS: A total of 68 patients were divided into two groups A and B. In the group A (n=38), Pringle's maneuver was employed, whereas in the group B (n=30), hepatectomy after pre-ligation of the hepatic inflow and outflow blood vessels of the lesioned side of the liver was used. Perioperative blood loss, postoperative bleeding and drainage, time of liver function recovery as well as incidence of postoperative complications were compared between the 2 groups. RESULTS: The mean perioperative blood loss, the mean amount of postoperative bleeding and drainage, the time of liver function recovery as well as incidence of postoperative complications were significantly higher in the group A than in the group B (P<0.01). CONCLUSION: Hepatectomy after pre-ligation of the hepatic inflow and outflow blood vessels of the lesioned side of the liver is superior to Pringle's maneuver.

关键词： hepatectomy blood flow clamping

Investigation of 'chazi'(damaged-enamels)on Chenghua doucai Porcelains

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Science china(Technological Sciences) 2009年第6期52卷 1722-1729页

作者： DU Feng1 & SU BaoRu2 1 Institute of Chemistry & Molecular Engineering,qingdao university of Science & Technology,qingdao,china 2 college of Information Science & Technology,qingdao university of Science & Technology,qingdao,china Institute of Chemistry & Molecular Engineering Qingdao University of Science & Technology Qingdao China college of Information Science & Technology Qingdao University of Science & Technology Qingdao China

At the end of the 1950s,Sun Yingzhou considered that the 'chazi'(damaged colour)on Chenghua doucai imperial porcelain as a defect was originally produced in firing process during Chenghua period(1465―1487).Researchers in china have accepted his *** any fragment with the 'chazi' has never been found in several tons of Chenghua imperial sherds excavated from Ming imperial kiln site in *** china,few scholars have questioned the formation of 'chazi',and further investigated *** researchers at the Research Laboratory in the British Museum,employing unde-structive EDXRF,have analyzed the chemical composition of the 'chazi'(damaged colour)on a Chen-ghua doucai stem cup in the museum,and they have confirmed that the 'chazi'(damaged colour)was caused by the fire of the Jianfu palace in the Forbidden City in *** on their research,the authors studied the colour chemical principle of the 'chazi's' formation *** to the ceramic technology principle,scientific reasoning for the 'chazi' was carried *** the help of the history of Qing court,the brainteaser of the 'chazi' was totally uncovered,the misunderstanding for the 'chazi' has also been *** research also suggests that employing modern science and technology is a direction to study Chinese ancient ceramic further.

关键词： Chenghua doucai porcelains court eunuchs the set on fire at the Jianfu palace ’chazi’(damaged-enamels) the British Museum colour chemical principle archaeology using science and technology

The Electrochemical Characteristics of Multilayer Assembly of Hemoglobin and Polystyrene Sulfonate at Self-assembled MonolayerSurface

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Chinese Chemical Letters 2000年第1期11卷 81-84页

作者： Hong SUN (department of Chemistry, Textile college, qingdao university, qingdao 266071) qingdao Univ Dept Chem Coll Text Qingdao 266071 Peoples R China

A multilayer film of hemoglobin (Hb) molecules and polyelectrolyte sulfonate were fabricated on a thiol self-assembled monolayers (SAMs) by electrostatic force. The Hb maintains electroactive property in the multilayer film, methylene blue (MB) incorporated into the multilayer can enhance the electron transfer rate between the Hb and the electrode surface.

关键词： multilayer film hemoglobin methylene blue

Approximately optimal tracking control for discrete time-delay systems with disturbances

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Progress in Natural Science:Materials International 2008年第2期18卷 225-231页

作者： Gongyou Tang a,,Huiying Sun b,Haiping Pang c a college of Information Science and Engineering,Ocean university of china,qingdao 266100,china b college of Information and Electrical Engineering,Shandong university of Science and Technology,qingdao 266510,china c college of Automation and Electronic Engineering,qingdao university of Science and Technology,qingdao 266042,china college of Information Science and Engineering Ocean University of China Qingdao 266100 China college of Information and Electrical Engineering Shandong University of Science and Technology Qingdao 266510 China college of Automation and Electronic Engineering Qingdao University of Science and Technology Qingdao 266042 China

Optimal tracking control (OTC) for discrete time-delay systems affected by persistent disturbances with quadratic performance index is considered. By introducing a sensitivity parameter,the original OTC problem is transformed into a series of two-point boundary value (TPBV) problems without time-advance or time-delay terms. The obtained OTC law consists of analytic feedforward and feedback terms and a compensation term which is the sum of an infinite series of adjoint vectors. The analytic feedforward and feedback terms can be found by solving a Riccati matrix equation and two Stein matrix equations. The compensation term can be obtained by using an iteration formula of the adjoint vectors. Observers are constructed to make the approximate OTC law physically realizable. A simulation example shows that the approximate approach is effective in tracking the reference input and robust with respect to exogenous persistent disturbances.

关键词： Discrete systems Time-delay systems Disturbances Optimal control Tracking control

Further study of sources of the imported cobalt-blue pigment used on Jingdezhen porcelain from late 13 to early 15 centuries

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Science china(Technological Sciences) 2008年第3期51卷 249-259页

作者： DU Feng1 & SU BaoRu2 1 Institute of Chemistry & Molecular Engineering, qingdao university of Science & Technology, qingdao 266000, china 2 college of Information Science Technology, qingdao university of Science & Technology, qingdao 266000, china Institute of Chemistry & Molecular Engineering Qingdao University of Science & Technology Qingdao 266000 China college of Information Science Technology Qingdao University of Science & Technology Qingdao 266000 China

Based on the conclusion of modern scientific analysis: the cobalt-blue pigment applied on Jingdezhen official porcelain during Yuan Dynasty and prior to Xuande reign of Ming Dynasty (1271―1425) contains high iron and low manganese con- tents, and the cobalt during Xuande and after Xuande periods (after 1426) of Ming Dynasty contains high manganese and low iron contents, in combination with the traditional archaeological method, the related historical textual records were in- vestigated and analyzed, the imported cobalt employed on Jingdezhen official porcelain was studied comprehensively, systematically and logically. In fact, 'Su Ma Li Qing' (Samarra-blue) and 'Su Bo Ni Qing' (Sumatra-blue) are definitely different cobalt ores originated in different places, because of their very similar translitera- tions in Chinese, the confusion has appeared in ancient books for more than 400 years, which considered 'Su Ma Li Qing' and 'Su Bo Ni Qing' as the same co- balt-blue pigment. In this article the mistake was corrected, the possible producing places and the approximate eras of the two pigments imported to china and used at Jingdezhen were also suggested.

关键词： imported cobalt-blue pigments employed on official blue-and-white porcelain Yuan Dynasty early Ming Dy- nasty Mn/Fe content ratio Su Ma Li Qing (Samarra-blue) Su Bo Ni Qing (Sumatra-blue) scientific archae- ological research transliteration