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Journal of Materials Science & Technology 2024年第2期169卷 235-242页

作者： h.X.Lu h.Liu z.z.Fu Y.Y.Chen h.Q.Dai z.hu W.L.zhang R.Q.Guo Institute for Electric Light Sources School of Information Science and TechnologyFudan UniversityShanghai 200433China Institute of Future Lighting Academy for Engineering and TechnologyFudan UniversityShanghai 200433China Yiwu Research Institute of Fudan University YiwuZhejiang 322000China zhongshan-Fudan Joint Innovation Center Zhongshan 528437China

In this study,a two-step method was used to synthesize highly luminescent AgGaS/znS/znS quantum dots(QDs).In the first step,an inner znS shell was formed via a one-pot method,which resulted in a smaller lattice mismatch between the AgGaS core and the outer znS shell,thereby facilitating the formation of a thick outer *** the two-step shelling process,the synthesized AgGaS/znS/znS QDs showed an excellent photoluminescence quantum yield(PLQY)of 96.4%with a peak wavelength of 508 nm,repre-senting the highest PLQY reported thus far for AgGaS ***,the effect of halogen ions in zn precursors on the shelling process was *** was proposed that the capacity of halogen ions to coordinate with the QDs influenced the balance between zn cation diffusion and znS shelling ***,the znS shelling reaction was dominant when znCl_(2)was employed,while zn cation diffusion was the dominant process under the I^(−)-rich *** work provides insights into the interfacial restructuring during the znS shelling and offers a clear map for the tailored synthesis of core/shell QDs.

关键词： AgGaS Quantum dots Photoluminescence Core/shell Alloyed core/shell interface

Precipitation of multi-type nano-quasicrystals in a Mg-zn-Y alloy

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Journal of Magnesium and Alloys 2024年第3期12卷 997-1008页

作者： W.z.Wang X.z.zhou L.F.zhang h.Q.Ye z.Q.Yang Shenyang National Laboratory for Materials Science Institute of Metal ResearchChinese Academy of ScienceShenyang 110016China Ji hua Laboratory Foshan 528251China Foshan University Foshan 528231China

Mg-6zn-1Y(at.%)ribbons with strengthening precipitates of multi-type nanoquasicrystals were prepared by melt-spinning followed by aging *** evolution of the rapidly solidified ribbons during isothermal aging was comprehensively studied using various electron microscopy *** new kinds of decagonal quasicrystals were formed in aged ribbons,in addition to precipitation of nanometer icosahedral ***-resolution observations reveal that both decagonal quasicrystals can be modeled by quasiperiodic tiling with decagonal clusters of 2.5 nm in diameter,but overlap of neighboring clusters in both decagonal quasicrystals is different from the Gummelt model observed in other quasicrystals.A shell composed of complex Laves Mg-zn domains was formed surrounding each decagonal quasicrystal precipitate upon prolonged *** addition,all kinds of nanoprecipitates exhibit excellent structure and size stability at 573 *** findings may have implications for not only fundamental studies about quasicrystals,but also microstructural manipulation of high-performance Mg alloys.

关键词： Quasicrystal Mg alloys Rapid solidification Scanning-transmission electron microscopy.

Microstructure evolution and shape memory behaviors of Ni_(47)Ti_(44)Nb_(9)alloy subjected to multistep thermomechanical loading with different prestrain levels

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Journal of Materials Science & Technology 2024年第4期171卷 80-93页

作者： Y.h.zhang h.Li z.W.Yang X.Liu Q.F.Gu State Key Laboratory of Solidification Processing School of Materials Science and EngineeringNorthwestern Polytechnical UniversityXi’an 710072China Shaanxi Key Laboratory of high-Performance Precision Forming Technology and Equipment Northwestern Polytechnical UniversityXi’an 710072China

Ni_(47)Ti_(44)Nb_(9)shape memory alloy(SMA)is a promising material in the aerospace field due to its wide transformation *** application of shape memory effect depends on multistep thermomechan-ical loading,viz.,low-temperature deformation and subsequent heating to ***-temperature deformation prestrain plays a pivotal role in shape memory properties tailoring of SMA ***,microstructure evolution and deformation mechanisms of Ni_(47)Ti_(44)Nb_(9)SMA subjected to vari-ous prestrain levels are still *** this end,microstructure evolution and shape memory behaviors of Ni_(47)Ti_(44)Nb_(9)alloy subjected to multistep thermomechanical loading with prestrain levels of 8%-16%at-28℃(M_(s)+30℃)were *** results demonstrate that the stress-strain curve of the specimen exhibits four distinct stages at a maximal prestrain of 16%.Whereas stageⅡand stageⅢend at prestrains of∼8%and∼12%,*** stageⅡ,the stress-induced martensitic transformation is accompanied by the dislocation slip of the NiTi matrix andβ-Nb *** stageⅢ,in addition to the higher density of dislocations and further growth of stress-induced martensite variants(SIMVs),(001)compound twins are introduced as a result of the(001)deformation twinning in stress-induced ***{20-1}martensite twins are gradually introduced in stageⅣ.Correspondingly,after subsequent unloading and heating,a higher density of{114}austenite twins form in the specimen with a larger prestrain of 16%.With increasing prestrain from 8%to 16%,the recoverable strainε_(re)^(T)upon heating increases first and then ***ε_(re)^(T)obtains a maximum of 7.03%at 10%prestrain and de-creases to 6.17%at 16%*** increase ofε_(re)^(T)can be attributed to the formation of new SIMVs,the further growth of existing SIMVs,and the recoverable(001)compound *** the decrease ofε_(re)^(T)is mainly associated with the irrecoverable strain by{20−1}martensite *** effe

关键词： Ni_(47)Ti_(44)Nb_(9)shape memory alloy Wide transformation hysteresis Thermomechanical loading Microstructure evolution Shape memory behaviors Stress-induced martensitic transformation Deformation twinning

Exploring Variability in Sea Level at a Tide Gauge Station through Control Charts

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Journal of Environmental & Earth Sciences 2024年第1期6卷 11-18页

作者： h.Bâkiİz Independent Scholar Boca Raton Florida33496USA

Monitoring temporal changes in sea level is important in assessing coastal *** level anomalies at a tide gauge station,if kinematically conceived,include systematic variations such as trend,acceleration,periodic oscillations,and random *** them,the non-stationary nature of the random sea level variations of known or unknown origin at coastal regions has been long recognized by the sea level *** study proposes the analyses of subgroups of random residual statistics of a rigorously formulated kinematic model solution of tide gauge variations using X-bar and S control *** approach is demonstrated using Key West,Florida tide gauge *** mean and standard errors of 5-year-long subgroups of the residuals revealed that sea level changes at this location have been progressively intensifying from 1913 to the *** oscillations in sea level at this locality may be attributed partly to the thermal expansion of seawater with increasing temperatures causing larger buoyancy-related sea level fluctuations as well as the intensification of atmospheric events including wind patterns and the impact of changes in inverted barometer effects that will alter coastal risk assessments for the future.

关键词： Climate change Sea level variance X-bar S control charts

Construction of 2D/2D Ti_(3)C_(2)T_(x)MXene/CdS heterojunction with photothermal effect for efficient photocatalytic hydrogen production

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Journal of Materials Science & Technology 2024年第4期171卷 1-9页

作者： T.Y.huang z.Yang S.Y.Yang z.h.Dai Y.J.Liu J.h.Liao G.Y.zhong z.J.Xie Y.P.Fang S.S.zhang Key Laboratory for Biobased Materials and Energy of Ministry of Education Guangdong Laboratory for Lingnan Modern AgricultureCollege of Materials and EnergySouth China Agricultural UniversityGuangzhou 510643China School of Physics and Optoelectronics South China University of TechnologyGuangzhou 510640China School of Chemical Engineering and Energy Technology Guangdong Provincial Key Laboratory of Distributed Energy SystemsDongguan University of TechnologyDongguan 523808China

The insensitivity of semiconductors to visible and infrared light is a key constraint on the utilization of light energy in photocatalytic *** photocatalysts with full-spectrum absorption through surface engineering is an effective approach to fully harnessing light energy in semiconductor ***,a novel stable Ti_(3)C_(2)T_(x)MXene/CdS heterojunction catalyst is obtained by in-situ epitaxial growth of two-dimensional(2D)CdS nanosheets on 2D MXene interface via a solvothermal *** exceptional light absorption properties of MXene confer outstanding full-spectrum driven photocat-alytic hydrogen evolution capability upon the heterogeneous *** unique 2D/2D structure effectively mitigated the recombination of photogenerated carriers,enhancing the photocatalytic performance of the ***,the composite catalyst exhibits a significantly higher surface temperature of 80.4℃under visible light irradiation at an intensity of 0.1 W/cm^(2),which is 1.84 times higher than that of *** irradiation of visible and near infrared light,the composite catalyst with photothermal ef-fect demonstrates a remarkable hydrogen evolution rate of 65.4 mmol g^(-1)h^(-1),which is 7.2 times higher than that of CdS *** study introduces a novel approach for constructing full-spectrum absorption catalysts and expands the application of the photothermal effect in photocatalytic hydrogen evolution research.

关键词： Two-dimensional structure heterostructure Photothermal effect Photocatalyst hydrogen evolution

Dedicated SiPM array for GRD of GECAM

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Radiation Detection Technology and Methods 2022年第1期6卷 63-69页

作者： D.L.zhang X.L.Sun z.h.an X.Q.Li X.Y.Wen K.Gong C.Cai z.Chang G.Chen C.Chen Y.Y.Du M.Gao R.Gao D.Y.Guo J.J.he D.J.hou Y.G.Li C.Y.Li G.Li L.Li X.F.Li M.S.Li X.h.Liang X.J.Liu Y.Q.Liu F.J.Lu h.Lu B.Meng W.X.Peng F.Shi h.Wang J.z.Wang Y.S.Wang h.z.Wang X.Wen S.Xiao S.L.Xiong Y.B.Xu Y.P.Xu S.Yang1 X.zhou J.W.Yang Fan zhang S.N.zhang C.Y.zhang C.M.zhang Fei zhang X.Y.zhao Institute of high Energy Physics CASBeijing 100049China State Key Laboratory of Particle Detection and Electronics Beijing 100049China

Purpose The discovery of gravitational waves and gamma-ray bursts heralds the era of multi-messenger *** the adoption of two small satellites to achieve the all-sky monitoring of gamma-ray bursts,the gravitational wave highenergy electromagnetic counterpart all-sky monitor(GECAM)possesses a quasi-real-time early warning ability and plays an important role in positioning the sources of gravitational waves and in subsequent *** satellite of GECAM was fitted with 253-inch-diameter gamma-ray detectors(GRD),covering an energy range of 8–2 *** have adopted silicon photomultiplier tubes(SiPM)in lieu of photomultiplier tubes(PMT)to adapt to the dimensional limitations of *** A unique 3-inch circular SiPM array was *** this design,646×6 mm chips were arranged evenly in a circular manner with the seams filled with reflecting films,thus achieving satisfactory uniformity of light *** integrated pre-amplifier circuit on the back of the SiPM array adopted two-level grouping and summing;further,it achieved a satisfactory signal-to-noise *** high-gain and low-gain channels were adopted to achieve a large dynamic range,and two independent power supply units were used,where each unit can be closed separately,thus improving *** Performance studies show that this SiPM array meets the requirements of *** A 3-inch SiPM array have been developed that uses grouped summation,reflective films,a circular arrangement,two groups of independent power supplies,high-and low-gain signals,differential signal output technologies,*** solution can be used not only for GECAM,but also as a general solution for SiPM-based scintillation detectors.

关键词： SiPM GECAM Gamma-ray Signal-to-noise ratio Reflecting film Pre-amplifier

The data acquisition algorithm designed for the SiPM-based detectors of GECAM satellite

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Radiation Detection Technology and Methods 2022年第1期6卷 70-77页

作者： Y.Q.Liu K.Gong X.Q.Li X.Y.Wen z.h.an C.Cai z.Chang G.Chen C.Chen Y.Y.Du M.Gao R.Gao D.Y.Guo J.J.he D.J.hou Y.G.Li C.Y.Li G.Li L.Li X.F.Li M.S.Li X.h.Liang X.J.Liu F.J.Lu h.Lu B.Meng W.X.Peng F.Shi X.L.Sun h.Wang J.z.Wang Y.S.Wang h.z.Wang X.Wen S.Xiao S.L.Xiong Y.B.Xu Y.P.Xu S.Yang J.W.Yang Q.B.Yi Fan zhang D.L.zhang S.N.zhang C.Y.zhang C.M.zhang Fei zhang X.Y.zhao Y.zhao X.zhou Key Laboratory of Particle Astrophysics Institute of High Energy PhysicsChinese Academy of SciencesBeijing 100049China University of Chinese Academy of Sciences Chinese Academy of SciencesBeijing 100049China Physics and Space Science College China West Normal UniversityNanchong 637002China

Background The Gravitational Wave high-energy Electromagnetic Counterpart All-sky Monitor(GECAM)consists of 2 microsatellites,each of which contains 25 GRD(LaBr3)detectors and 8 CPD(plastic scintillator)*** silicon photomultiplier(SiPM)array is used to read each *** output signal of these detectors with SiPM array is very special and challenging to *** this study,a novel data acquisition(DAQ)algorithm for these detectors is designed and implemented,and the content of the output event packet is *** and Conclusion The performances,including the event acquisition efficiency of this DAQ algorithm,are extensively verified through experimental *** the on-ground and in-flight tests,this algorithm has excellent performance despite the very limited resources and short development time of GECAM mission.

关键词： Silicon photomultiplier Digital waveform processing Data acquisition

The design and performance of charged particle detector onboard the GECAM mission

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Radiation Detection Technology and Methods 2022年第1期6卷 53-62页

作者： Y.B.Xu X.Q.Li X.L.Sun S.Yang h.Wang W.X.Peng X.h.Liang K.Gong Y.Q.Liu D.Y.Guo X.Y.zhao C.Y.Li z.h.an J.J.he X.J.Liu X.Y.Wen S.L.Xiong Fan zhang D.L.zhang C.Y.zhang C.Cai z.Chang G.Chen C.Chen Y.Y.Du M.Gao R.Gao D.J.hou Y.G.Li G.Li L.Li X.F.Li M.S.Li F.J.Lu h.Lu B.Meng F.Shi J.z.Wang Y.S.Wang h.z.Wang X.Wen S.Xiao Y.P.Xu J.W.Yang Q.B.Yi S.N.zhang C.M.zhang F.zhang Y.zhao X.zhou Key Laboratory of Particle Astrophysics Institute of High Energy PhysicsChinese Academy of SciencesBeijing 100049China

Background The Gravitational wave highly energetic Electromagnetic Counterpart All-sky Monitor(GECAM)is dedicated to detecting gravitational wave gamma-ray *** is capable of all-sky monitoring over and discovering gamma-ray bursts and new radiation *** consists of two microsatellites,each equipped with 8 charged particle detectors(CPDs)and 25 gamma-ray detectors(GRDs).Purpose The CPD is used to measure charged particles in the space environment,monitor energy and flow intensity changes,and identify between gamma-ray bursts and space charged particle events in conjunction with *** CPD uses plastic scintillator as the sensitive material for detection,silicon photomultiplier array as the optically readable device,and the inlaid Am-241 radioactive source as the onboard calibration *** In this paper,we will present the working principle,physical design,functional implementation and preliminary performance test results of the *** a result,the energy range of electron,gamma-ray detection efficiency and dead time are tested to be better than the indexes required through the ground calibration experiment.

关键词： GECAM CPD SiPM

Quality assurance test and failure analysis of SiPM arrays of GECAM satellites

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Radiation Detection Technology and Methods 2022年第1期6卷 35-42页

作者： D.L.zhang M.Gao X.L.Sun X.Q.Li z.h.an X.Y.Wen C.Cai z.Chang G.Chen C.Chen Y.Y.Du R.Gao K.Gong D.Y.Guo J.J.he D.J.hou Y.G.Li C.Y.Li G.Li L.Li X.F.Li M.S.Li X.h.Liang X.J.Liu Y.Q.Liu F.J.Lu h.Lu B.Meng W.X.Peng F.Shi h.Wang J.z.Wang Y.S.Wang h.z.Wang X.Wen S.Xiao S.L.Xiong Y.B.Xu Y.P.Xu S.Yang J.W.Yang Fan.zhang S.N.zhang C.Y.zhang C.M.zhang Fei zhang X.Y.zhao X.zhou Institute of high Energy Physics CASBeijing 100049People’s Republic of China

Background The Gravitational wave high-energy Electromagnetic Counterpart All-sky Monitor(GECAM)satellite developed a SiPM-based gamma-ray detector to monitor the gravitational wave-related GRBs and guide subsequent observations in other wavelengths of *** As all the available SiPM devices belong to commercial grade,quality assurance tests need to be performed in accordance with the aerospace *** In the SiPM application of GECAM,quality assurance experiments were *** mechanism of the failure of SiPM devices was analyzed during the development *** Based on the quality assurance test results,the fnal pass rate of SiPM array was 95%.Based on the failure analysis,it was found that a piece of SiPM had a leakage channel after longtime operation due to device *** According to the accumulated experience,in the reliability test of SiPM,it is necessary to pay special attention to test the impedance of each pin of SiPM to ground and confrm that the power switch state of SiPM is controllable.

关键词： Gravitational waves Gamma-ray detectors Silicon photomultipliers Quality assurance test Failure analysis

The design and performance of GRD onboard the GECAM satellite

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Radiation Detection Technology and Methods 2022年第1期6卷 43-52页

作者： z.h.an X.L.Sun D.L.zhang S.Yang X.Q.Li X.Y.Wen K.Gong X.h.Liang X.J.Liu Y.Q.Liu Y.G.Li S.L.Xiong Y.B.Xu Fan zhang X.Y.zhao C.Cai z.Chang G.Chen C.Chen Y.Y.Du P.Y.Feng M.Gao R.Gao D.Y.Guo J.J.he D.J.hou C.Y.Li G.Li L.Li X.F.Li M.S.Li F.J.Lu h.Lu B.Meng W.X.Peng F.Shi h.Wang J.z.Wang Y.S.Wang h.z.Wang X.Wen S.Xiao Y.P.Xu J.W.Yang Q.B.Yi S.N.zhang C.Y.zhang C.M.zhang Fei zhang Y.zhao X.zhou CAS Institute of High Energy PhysicsBeijing 100049China State Key Laboratory of Particle Detection and Electronics Beijing 100049China 3 Xiangtan UniversityXiangtan 411105China 4 Beijing Normal UniversityBeijing 110875China Xiangtan University Xiangtan 411105China Beijing Normal University Beijing 110875China

Background Each GECAM satellite payload contains 25 gamma-ray detectors(GRDs),which can detect gamma-rays and particles and can roughly localize the Gamma-Ray Bursts(GRBs).GRD was designed using lanthanum bromide(LaBr3)crystal as the sensitive material with the rear end coupled with silicon photomultiplier(SiPM)array for *** In aerospace engineering design of GRD,there are many key points to be *** this paper,we present the specific design scheme of GRD,the assembly and the performance test results of *** Based on Monte Carlo simulation and experimental test results,the specific schematic design and assembling process of GRD were *** being fully assembled,the GRDs were conducted performance tests by using radioactive source and also conducted random vibration *** and conclusion The test results show that all satellite-borne GRDs have energy resolutionhows that GRD can maintain in a stable performance,which meets the requirement of spatial application.

关键词： Lanthanum bromide scintillator SiPM array GECAM Gamma-ray detector Energy resolution