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Nano Research 2024年第8期17卷 7020-7026页

作者： Jinhua He Chenhui Wang Mingrui Liu Muhammad Ramzan Zhiwei Long xian-gang wu Yu Chen Haizheng Zhong MIIT Key Laboratory for Low-Dimensional Quantum Structure and Devices School of Materials Science and EngineeringBeijing Institute of TechnologyBeijing 100081China Beijing Engineering Research Center for Mixed Reality and Advanced Display Technology School of Optics and PhotonicsBeijing Institute of TechnologyBeijing 100081China

The potential use of large-size ZnSe quantum dots as blue emitters for display applications has greatly inspired the colloidal ***,we report the negative effects of side reactions of large-size ZnSe quantum *** side reactions between oleic acid and oleylamine generated amidation products and H_(2)O,which led to the hydrolysis of Zn(OA)2 to Zn(OH)2 and the subsequent formation of zinc oxide(ZnO)and zinc bis[diphenylphosphinate](Zn(DPPA)2)*** side reactions resulted in the formation of a defective surface including a Se-rich surface and oxygen-related *** negative effects can be overcome by adopting an etching strategy using potassium fluoride and myristic acid in *** overcoating a ZnS shell,blue emissive ZnSe/ZnS quantum dots with a maximum photoluminescence quantum yield of up to 91%were *** further fabricated ZnSe quantum dots-based blue light-emitting diodes with an emission peak at 456 *** device showed a turn-on voltage of 2.7 V with a maximum external quantum efficiency of 4.2%and a maximum luminance of 1223 cd·m^(−2).

关键词： quantum dots ZnSe side reactions surface etching light-emitting diodes

Enhanced piezo-response in copper halide perovskites based PVDF composite films

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Science Bulletin 2018年第19期63卷 1254-1259页

作者： Sheng Huang gang Tang Hailong Huang xian-gang wu Puming Zhou Lin Zou Lei Xie Jianming Deng Xueyun Wang Haizheng Zhong Jiawang Hong Beijing Key Laboratory of Nanophotonics and Ultrafine Optoelectronic Systems School of Materials Science & Engineering Beijing Institute of Technology Beijing 100081. China School of Aerospace Engineering Beijing Institute of Technology Beijing 100081 China The 48th Research Institute China Electronics Technology Group Corporation Changsha 410111 China Key Laboratory of Neutron Physics and Institute of Nuclear Physics and Chemistry China Academy of Engineering Physics Mianyang 621999 China

ln-situ fabricated perovskite nanocrystals in polymeric matrix provide new generation composite mate- rials for plenty of cutting edge technology. In this work, we report the in-situ fabrication of copper halide perovskite （MA_2CuCI_4, MA：CH_3NH＋3） embedded poly（vinylidene fluoride）（PVDF） composite films. The optimized MA_2CuCI_4/PVDF composite films exhibit greatly enhanced piezo-response in comparasion with pure PVDF films. The enhancements were invesitgated and explained by applying piezo-response force microscopy （PFM） measurements and density functional theory （DFT） caculations. We proposed that the high piezoelectric properties of MA_2CuCI_4/PVDF composite films could be related to the large Cu off-centering displacement, the strong interactions between MA_2CuCI_4 and PVDF as well as large stress concentration around the MA_2CuCI_4 particles in the films. These piezoelectric composite films are expected to be suitable functional materials for flexible and/or wearable niezoelectrics.

关键词： Perovskite Piezoelectric Composite films MA_2CuCI_4

Revealing the vertical structure of in-situ fabricated perovskite nanocrystals films toward efficient pure red light-emitting diodes

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Fundamental Research 2024年第2期4卷 362-368页

作者： xian-gang wu Shipei Sun Tinglu Song Xin Zhang Chenhui Wang Yingguo Yang Shuangpeng Wang Haizheng Zhong MIIT Key Laboratory for Low-Dimensional Quantum Structure and Devices School of Materials Science&EngineeringBeijing Institute of TechnologyBeijing 100081China Experimental Center of Advanced Materials School of Materials Science&EngineeringBeijing Institute of TechnologyBeijing 100081China Shanghai Synchrotron Radiation Facility(SSRF) Shanghai Institute of Applied PhysicsChinese Academy of SciencesShanghai 201204China Institute of Applied Physics and Materials Engineering University of MacaoMacao 999078China

The development of efficient perovskite light-emitting diodes(PeLEDs)relies strongly on the fabrication of perovskite films with rationally designed structures(grain size,composition,surface,etc.).Therefore,an understanding of structure-performance relationships is of vital importance for developing high-performance perovskite devices,particularly for devices with in-situ fabricated perovskite nanocrystal *** this study,we reveal the vertical structure of an in-situ fabricated quasi-two-dimensional perovskite *** combining time-of-flight secondary ion mass spectrometry,energy dispersive spectroscopy,grazing incidence wide-angle X-ray scattering(GIWAXS),and low-temperature photoluminescence spectra,we illustrate that the resulting in-situ fabricated DPPA_(2)Cs_(n-1)Pb_(n)(Br_(0.3)I_(0.7))_(3n+1)(DPPA^(+):3,3-diphenylpropylammonium)film has a gradient structure with a very thin layer of ligands on the surface,predominantly small-n domains at the top,and predominantly large-n domains at the bottom owing to the solubility difference of the *** addition,GIWAXS measurements show that the domain of n=2 on the top layer has an ordered in-plane *** on the understanding of the film structure,we developed an in-situ fabrication process with ligand exchange to achieve efficient pure red PeLEDs at 638 nm with an average external quantum efficiency(EQE)of 7.4%.The optimized device had a maximum luminance of 623 cd/m^(2) with a peak EQE of 9.7%.

关键词： Light-emitting diodes Perovskite TOF-SIMS Vertical structure in-situ fabrication

Insights into spinal muscular atrophy from molecular biomarkers

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Neural Regeneration Research 2025年第7期20卷 1849-1863页

作者： Xiaodong Xing Xinzhu Liu xiandeng Li Mi Li xian wu Xiaohui Huang Ajing Xu Yan Liu Jian Zhang Department of Clinical Pharmacy Xinhua HospitalShanghai Jiao Tong University School of MedicineShanghaiChina College of Pharmacy Chongqing Medical UniversityChongqingChina

Spinal muscular atrophy is a devastating motor neuron disease characterized by severe cases of fatal muscle *** is one of the most common genetic causes of mortality among infants aged less than 2 *** research is currently receiving more attention,and new candidate biomarkers are constantly being *** review initially discusses the evaluation methods commonly used in clinical practice while briefly outlining their respective pros and *** also describe recent advancements in research and the clinical significance of molecular biomarkers for spinal muscular atrophy,which are classified as either specific or non-specific *** review provides new insights into the pathogenesis of spinal muscular atrophy,the mechanism of biomarkers in response to drug-modified therapies,the selection of biomarker candidates,and would promote the development of future ***,the successful utilization of biomarkers may facilitate the implementation of gene-targeting treatments for patients with spinal muscular atrophy.

关键词： biomarkers disease progression gene-targeting therapy neurofilaments Nusinersen spinal muscular atrophy(SMA) survival motor neuron therapeutic evaluation treatment outcomes

Reduction of NO_(x)emission based on optimized proportions of mill scale and coke breeze in sintering process

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International Journal of Minerals,Metallurgy and Materials 2021年第9期28卷 1453-1461页

作者： Zhi-gang Que xian-bin Ai Sheng-li wu Institute of Energy Research Jiangxi Academy of ScienceNanchang 330096China School of Metallurgical and Ecological Engineering University of Science and Technology BeijingBeijing 100083China

Reducing NO_(x) emission of iron ore sintering process in a cost effective manner is a challenge for the iron and steel industry at *** of the proportion of mill scale and coke breeze on the NO_(x) emission,strength of sinter,and sinter indexes were studied by com-bustion and sinter pot *** showed that the peak value of NO concentration,total of NO emission,and fuel-N conversion rate gradu-ally decreased as the proportions of the mill scale increased because NO was reduced to N_(2) by Fe_(3)O_(4),FeO,and Fe in the mill *** strength of sinter reached the highest value at 8.0wt%mill scale due to the formation of minerals with low melting *** fuel-N conver-sion rate slightly fluctuated and total NO_(x) emission significantly decreased with the decreased proportions of coke breeze because CO forma-tion and content of N element in the sintered mixture ***,the sinter strength also decreased due to the decrease in the amount of the melting ***,results of the sinter pot tests indicated that NO_(x) emission *** sinter indexes performed well when the proportions of mill scale and coke breeze were 8.0wt%and 3.70wt%respectively in the sintered mixture.

关键词： iron ore sinter NO_(x)emission mill scale coke breeze proportion optimization

Stability and Determination of Metamizole Sodium by Capillary Electrophoresis Analysis Combined with Infra-red Spectroscopy

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Chemical Research in Chinese Universities 2007年第6期23卷 654-658页

作者： xianG Qian NIU gang wu xian-hua CHEN gang Department of Applied Chemistry Changchun Institute of Technology Changchun 130022 P. R. China Key Laboratory of Automobile Materials of Ministry of Education College of Materials Science and Engineering Jilin University Changchun 130012 P. R. China

Metamizole sodium was chosen as a representative of unstable analytes for investigation by discussing the effects of oxygen and solvent on its degradation reaction using the capillary electmphoresis technique. A possible degradation mechanism was deduced from the observed behavior and was confirmed by infra-red spectroscopic study. The degradation reaction could be inhibited obviously by methanol instead of water as the solvent of analyte. Under the optimized conditions： separation voltage of 20 kV, and 5 mmol/L disodium hydrogen phosphate and 5 mmol/L borax with 10% methanol（pH 9. 12） as the running buffer, the standard curve of metamizole sodium was linear in a range of 3.77- 74. 07 mg/L. A satisfactory result was achieved when the technique was used to detect metamizole sodium in tablet.

关键词： Capillary electmphoresis Metamizole sodium Stability

Spectrophotometric Determination of Trace Chromium(VI) in Mass Chromium(III)

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Chinese Chemical Letters 2001年第7期12卷 635-636页

作者： Zi gang XU xian Hong WEN Qing Zhou wu Center of Analysis&Testing Zhejiang UniversityHangzhou 310027

The method for the sepration and determination of trace Cr(VI) exiting in mass Cr(III) has been researched. The method is highly sensitive and less interference, but is simple and useful for analysis trace Cr(VI).

关键词： Spectrophotometric Cr(VI) Cr(III) diphenyl carbazide(DPC) 4-methyl-benzene sulfonic acid

Permeability measurement of the fracture-matrix system with 3D embedded discrete fracture model

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Petroleum Science 2022年第4期19卷 1757-1765页

作者： Bao Jia Cheng-gang xian State Key Laboratory of Petroleum Resources and Prospecting China University of Petroleum(Bejing)Beijing 102249China Unconventional Petroleum Research Institute China University of Petroleum(Bejing)Bejing 102249China

In this work, we performed the pulse-decay experiment on a fractured shale core and applied the 3 D embedded discrete fracture model(EDFM) to simulate the experiment process. The irregularly rough fracture surface was depicted in detail using a 3 D scanner. Then the fracture surface profile was imported in the discrete fracture network model to simulate the flow process in the fracture-matrix system realistically. History matching was efficiently performed to simultaneously obtain porosity and permeability for the matrix and fracture. Gas properties after applying nanopore confinement were obtained by modifying Sutton's viscosity correlation with sensitivity analysis on the pore diameter ranging from 2 to50 nm. Nanopore confinement results in low matched permeability due to viscosity reduction in the matrix-only porous media. The fracture-matrix system complicates the interpretation of nanopore confinement impact on flow behavior in shale reservoirs. Different scenarios of the highly fractured and matrix-dominated systems were discussed in detail by constructing the digital twin model.

关键词： Permeability Fracture Pulse-decay Shale Viscosity

CO_2-sensitive Amphiphilic Triblock Copolymer Self-assembly Morphology Transition and Accelerating Drug Release from Polymeric Vesicle

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Chinese Journal of Polymer Science 2018年第1期36卷 18-24页

作者： xian-wu Jing Zhi-Yu Huang Hong-Sheng Lu Bao-gang Wang College of Chemistry and Chemical Engineering Southwest Petroleum University Engineering Research Center of Oilfield Chemistry Ministry of Education

A series of triblock copolymers, containing a CO_2-switchable block poly（2-（dimethylamino）ethyl methacrylate）（PDM） block and two symmetrical hydrophilic blocks polyacrylamide（PAM）, were synthesized using atom transfer radical polymerization（ATRP） method. The p H and conductivity tests showed that the triblock copolymer exhibited switchable responsiveness to CO_2, i.e. a relatively low conductivity of solution could be switched on and off by bubbling and removing of CO_2, and the triblock copolymer aqueous solution displayed a CO_2-switchable viscosity variation. The changes were all attributed to protonation of tertiary amine groups in PDM blocks and proven by 1 H-NMR. Cryogenic transmission electron microscopy and dynamic light scattering characterization demonstrated that the viscosity variation was the result of a unilamellar vesicle-network aggregate structure transition. The release of rhodamine B from the vesicles with and without CO_2 stimuli showed the potential application in drug delivery domains; after CO_2 bubbling, the drug release rate could be accelerated. Finally, reasonable mechanism of CO_2-switchable morphology changes and CO_2-induced drug release was proposed.

关键词： ATRP CO_2-sensitive Polymeric vesicles Drug release

人口流动对我国高等教育资源配置的影响及对策研究

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黑龙江高教研究 2025年第1期43卷 31-37页

作者：陈茂建吴刚龙福建教育学院福建福州350001 黎明职业大学福建泉州362000

基于2013一2022年31个省份面板数据,使用固定效应模型实证检验人口流动对我国高等教育资源配置的影响。结果发现:第一,人口流动对高等教育资源配置具有显著影响作用,人口净流入地区和净流出地区分别对高等教育资源配置产生负向影响和正... 详细信息

基于2013一2022年31个省份面板数据,使用固定效应模型实证检验人口流动对我国高等教育资源配置的影响。结果发现:第一,人口流动对高等教育资源配置具有显著影响作用,人口净流入地区和净流出地区分别对高等教育资源配置产生负向影响和正向影响;第二,人口流动对高等教育资源配置的影响因地区经济发展水平、城镇化水平以及人口结构的不同而存在差异,东部地区、城镇化水平为中等的地区、中等文化水平程度在人口流动对高等教育资源配置的影响方面均最显著。基于研究结果一,提出以下对策:一是加强人口流入地区的高等教育资源配置;二是优化人口流出地区的高等教育资源配置。基于研究结果二,提出以下对策:一是加强东部地区的高等教育资源配置;二是注重城镇化水平中等地区的高等教育资源配置;三是加强教育普及程度相对均衡地区的高等教育资源配置。

关键词：人口流动高等教育资源配置对策