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Large-scale synthesis of fluorine-free carbonyl iron-organic silicon hydrophobic absorbers with long term corrosion protection property

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Nano Research 2022年第10期15卷 9479-9491页

作者： Wei Tian Jinyao Li Yifan Liu Longjiang Deng Yang Guo xian Jian National Engineering Researching Centre of Electromagnetic Radiation Control Materials Key Laboratory of Multi-Spectral Absorbing Materials and Structures of Ministry of EducationState Key Laboratory of Electronic Thin Films and Integrated DevicesSchool of Electronic Science and EngineeringUniversity of Electronic Science and Technology of ChinaChengdu 611731China The Yangtze Delta Region Institute(Huzhou)&School of Electronic Science and Engineering University of Electronic Science and Technology of ChinaHuzhou 313001China School of Materials and Energy University of Electronic Science and Technology of ChinaChengdu 611731China School of Electrical and Information Engineering Panzhihua UniversityPanzhihua 617000China

Environmentally-friendly magnetic metallic absorbers with high-performing antioxidant property,thermal stability,and anticorrosion capability have attracted great attention in real-world applications.A surface modification technology of magnetic metallic absorbers with dense and inert materials has been an effective strategy to solve the aforesaid problem.Herein,fluorinefree core–shell carbonyl iron-organic silicon absorbers(CI@SiO_(2)/1,1,1,3,3,3-hexamethyl disilazane(HMDS))were fabricated via a facile one-pot synthesis using tetraethyl orthosilicate(TEOS)and HMDS as the precursor of protective layer(SiO_(2)/HMDS),and CI@SiO_(2)/HMDS hybrid reveals its long-term corrosion resistance and excellent microwave absorption performance with a minimum reflection loss value of−44.3 dB and an effective absorption bandwidth of 5.3 GHz at a thin thickness of 2.0 mm after immersion in 5.0 wt.%NaCl acidic solutions for 2,160 h.Meanwhile,CI@SiO_(2)/HMDS hybrid can still achieve the maximum radar cross-sectional(RCS)reduction values about 16.5 dB·m^(2) at the detectionθof 0°.The exceptional microwave absorption performance and structural stability are largely due to the extraordinary wave-transparent property and shielding ability against corrosive medium of SiO_(2)/HMDS hydrophobic protective layer with a contact angle of 132.5°.The research paves the way for the large-scale and batch production of high-performance magnetic metallic absorbers and increases their survivability and reliability in the harsh environments.

关键词： microwave absorption long-term corrosion resistance carbonyl iron(CI)@SiO_(2)/1 1 1 3 3 3-hexamethyl disilazane(HMDS)hybrid core-shell radar cross-sectional simulation

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Dynamic p-y curves for vertical and batter pile groups in liquefied sand

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Earthquake Engineering and Engineering Vibration 2022年第3期21卷 605-616页

作者： Zhang jian Li Yurun Rong xian Liang Yan School of Civil and Transportation Engineering Hebei University of TechnologyTianjin 300401China Campus Construction and Management Hebei University of TechnologyTianjin 300401China

In this study,centrifuge model tests of vertical and batter pile groups in liquefied sand were conducted on a centrifuge shaking table.The dynamic p-y curves for these pile groups before and during sand liquefaction were obtained from calculations based on test data.The results confirm that liquefaction contributes to a reduction in the energy consumption of pile foundations,with the degradation effect being more pronounced for batter pile groups.At shallow depths,the difference in the backbone gradients of the p-y curves after liquefaction for vertical and batter pile groups indicates that the lateral stiffness of a batter pile group is greater than that of a vertical pile group.As shaking intensity increases,the lateral stiffness of a vertical pile group increases with depth during the late stage of sand liquefaction.However,the lateral stiffness of a batter pile group during liquefaction does not vary with depth.The results of this study provide a reference for the seismic design of vertical and batter pile groups in liquefied soil.

关键词： soil liquefaction pile-soil interaction p-y curve centrifuge shaking table

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Plasma-enhanced interfacial engineering of FeSiAl@PUA@SiO_(2)hybrid for efficient microwave absorption and anti-corrosion

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Nano Research 2023年第1期16卷 645-653页

作者： Hongyan Zhang Feng Cao Hui Xu Wei Tian Ying Pan Nasir Mahmood xian Jian School of Materials and Energy University of Electronic Science and Technology of ChinaChengdu 611731China Yangtze Delta Region Institute(Huzhou) University of Electronic Science and Technology of ChinaHuzhou 313001China Department of Engineering Technology Huzhou CollegeHuzhou 313000China School of Science RMIT UniversityMelbourneVIC 3001Australia

Microwave absorption materials are prone to degradation in extremely humid and salty environments,and it is still challenging to develop a dense and firm interface to protect microwave absorbers.Herein,a robust FeSiAl@PUA@SiO2(PUA:acrylic polyurethane)gradient hybrid was prepared through plasma-enhanced chemical vapor deposition(PECVD)to achieve efficient microwave absorption and anti-corrosion properties.The organic/inorganic dual coat of PUA/SiO2 not only facilitated the interface polarization but also effectively reduced the dielectric constant and optimized impedance matching.Owing to the unique hybrid structure,the(PECVD-FeSiAl@PUA)@SiO_(2) exhibited highly efficient microwave absorbing performance in frequency bands covering almost the entire Ku-bands(12-18 GHz)with a minimum reflection loss(RLmin)of−47 dB with a matching thickness of 2.3 mm.The organic/inorganic dual protection effectively shields against the corrosive medium,as the corrosion potential and the polarization resistance increased from−0.167 to−0.047 V and 8,064 to 16,273Ω·cm^(2),respectively.While the corrosion current decreased from 3.04×10^(−6) to 2.16×10^(−6) A/cm^(2).Hence,the plasma-enhanced densification of PUA created a strong bridge to integrate FeSiAl and organic/inorganic components acquiring dual-function of efficient microwave absorption and anticorrosion,which opened a promising platform for potential practical absorbers.

关键词： FeSiAl polyurethane acrylic inorganic/organic interface microwave absorption anti-corrosion

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Sustainable Polyamides Enabled by Controlled Ring-opening Polymerization of 4-Hydroxyproline-derived Lactams

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Chinese Journal of Polymer Science 2023年第5期41卷 728-734,I0008页

作者： jian-Qun Wang xian-Hong Wang You-Hua Tao Key Laboratory of Polymer Ecomaterials Changchun Institute of Applied ChemistryChinese Academy of SciencesChangchun 130022China University of Science and Technology of China Hefei 230026China

Aliphatic polyamides have been considered as eco-friendly materials,useful for a wide range of applications.However,it still presents obstacle to produce sustainable aliphatic polyamides from abundant renewable sources.Herein,we describe that 4-hydroxyproline(4-HYP),a renewable resource,was readily converted to its corresponding bicyclic bridged lactam monomers bearing pendant Boc-protected secondary amino group,and oligo-ethylene glycol group.Lithium hexamethyldisilazide(LiHMDS)-mediated polymerization of the resulting monomers exhibited a controlled feature,affording sustainable aliphatic polyamides with number-average molecular weight up to 73 kg/mol and a low molecular weight distribution?<1.28.Overall,this work can lead to a novel kind of functional and sustainable polyamides with potential applications,including degradable plastics,and drug delivery.

关键词： Polyamides Renewable Ring-opening polymerization 4-Hydroxyproline

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Flexible carbon fiber-based composites for electromagnetic interference shielding

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Rare Metals 2022年第11期41卷 3612-3629页

作者： Hong-Yan Zhang Jin-Yao Li Ying Pan Yi-Fan Liu Nasir Mahmood xian Jian School of Materials and Energy University of Electronic Science and Technology of ChinaChengdu611731China Yangtze Delta Region Institute(Huzhou) University of Electronic Science and Technology of ChinaHuzhou 313001China RMIT University School of EngineeringMelbourneVic3001Australia

With the rapid development of electronic information technology,the waste electromagnetic radiation generated by the wireless and various other electronic devices has caused serious harm to human health.The development of high-efficiency flexible electromagnetic interference(EMI)shielding materials has become one of the most effective ways to mitigate the increasingly serious problem of electromagnetic pollution.Flexible carbon fiber composites possess most of the physical requirements needed for EMI shielding applications,including high electrical conductivity,large specific surface area,light weight,flexibility,porous structure,and adjustable physical and chemical properties,and various morphology of carbon fibers-based composites applied EMI.In this review,the primary EMI shielding mechanism of carbonfiber-based materials is presented.Since carbon fiber suffers from a low absorption efficiency when used for EMI shielding by itself,it is usually combined with additional EMI filling materials.Therefore,the methods of adding EMI filler materials to the carbon fiber framework and the influence of different fillers on the EMI shielding performance are also discussed.In addition,the novel structural designs of flexible carbon fiber-based EMI shielding materials,including fiber orientation,core-shell structure,and multilayer heterostructure,are summarized in terms of their classification,which includes composites with metal,polymer,nano-carbon,and MXenes.The review concludes with a brief discussion of the challenges,research directions,and future prospects of carbon-fiber-based EMI shielding materials.

关键词： Carbon fibers Electromagnetic interference shielding Flexible Composites

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MAFLD vs.NAFLD:shared features and potential changes in epidemiology,pathophysiology,diagnosis,and pharmacotherapy

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Chinese Medical Journal 2021年第1期134卷 8-19页

作者： Ying-Xin xian jian-Ping Weng Fen Xu Department of Endocrinology and Metabolism The Third Affiliated Hospital of Sun Yat-sen UniversityGuangzhouGuangdong 510630China Guangdong Provincial Key Laboratory of Diabetology GuangzhouGuangdong 510630China Department of Endocrinology of the First Affiliated Hospital Division of Life Sciences and MedicineUniversity of Science and Technology of ChinaHefeiAnhui 230001China

Nonalcoholic fatty liver disease(NAFLD)is the most common chronic liver disease worldwide,placing an increasing burden on human health.NAFLD is a complex multifactorial disease involving genetic,metabolic,and environmental factors.It is closely associated with metabolic syndrome,obesity,and type 2 diabetes,of which insulin resistance is the main pathophysiological mechanism.Over the past few decades,investigation of the pathogenesis,diagnosis,and treatments has revealed different aspects of NAFLD,challenging the accuracy of definition and therapeutic strategy for the clinical practice.Recently,experts reach a consensus that NAFLD does not reflect the current knowledge,and metabolic(dysfunction)associated fatty liver disease(MAFLD)is suggested as a more appropriate term.The new definition puts increased emphasis on the important role of metabolic dysfunction in it.Herein,the shared features and potential changes in epidemiology,pathophysiology,diagnosis,and pharmacotherapy of the newly defined MAFLD,as compared with the formerly defined NAFLD,are reviewed for updating our understanding.

关键词： Nonalcoholic fatty liver disease Metabolic(dysfunction)associated fatty liver disease Epidemiology Pathophysiology Diagnosis Pharmacotherapy

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A Framework of Convergence Analysis of Mini-batch Stochastic Projected Gradient Methods

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Journal of the Operations Research Society of China 2023年第2期11卷 347-369页

作者： jian Gu xian-Tao Xiao School of Sciences Dalian Ocean UniversityDalian 116023China School of Mathematical Sciences Dalian University of TechnologyDalian 116023China

In this paper,we establish a unified framework to study the almost sure global convergence and the expected convergencerates of a class ofmini-batch stochastic(projected)gradient(SG)methods,including two popular types of SG:stepsize diminished SG and batch size increased SG.We also show that the standard variance uniformly bounded assumption,which is frequently used in the literature to investigate the convergence of SG,is actually not required when the gradient of the objective function is Lipschitz continuous.Finally,we show that our framework can also be used for analyzing the convergence of a mini-batch stochastic extragradient method for stochastic variational inequality.

关键词： Stochastic projected gradient method Variance uniformly bounded Convergence analysis

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Convergence of Bregman Peaceman–Rachford Splitting Method for Nonconvex Nonseparable Optimization

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Journal of the Operations Research Society of China 2023年第4期11卷 707-733页

作者： Peng-Jie Liu Jin-Bao jian Bo He xian-Zhen jiang College of Mathematics and Physics Guangxi Key Laboratory of Hybrid Computation and IC Design AnalysisCenter for Applied Mathematics and Artificial IntelligenceGuangxi University for NationalitiesNanning530006GuangxiChina College of Mathematics and Information Science Guangxi UniversityNanning530004GuangxiChina School of Mathematics China University of Mining and TechnologyXuzhou221116JiangsuChina

This work is about a splitting method for solving a nonconvex nonseparable optimization problem with linear constraints,where the objective function consists of two separable functions and a coupled term.First,based on the ideas from Bregman distance and Peaceman–Rachford splitting method,the Bregman Peaceman–Rachford splitting method with different relaxation factors for the multiplier is proposed.Second,the global and strong convergence of the proposed algorithm are proved under general conditions including the region of the two relaxation factors as well as the crucial Kurdyka–Łojasiewicz property.Third,when the associated Kurdyka–Łojasiewicz property function has a special structure,the sublinear and linear convergence rates of the proposed algorithm are guaranteed.Furthermore,some preliminary numerical results are shown to indicate the effectiveness of the proposed algorithm.

关键词： Nonconvex nonseparable optimization Peaceman-Rachford splitting method Bregman distance Kurdyka-Łojasiewicz inequality Convergence rate

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Laparoscopic pancreaticoduodenectomy with portal or superior mesenteric vein resection and reconstruction for pancreatic cancer:A single-center experience

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Hepatobiliary & Pancreatic Diseases International 2023年第2期22卷 147-153页

作者： Ming-jian Ma He Cheng Yu-Sheng Chen xian-Jun Yu Chen Liu Department of Pancreatic Surgery Fudan University Shanghai Cancer CenterShanghai 200032China Department of Oncology Shanghai Medical CollegeFudan UniversityShanghai 200032China Shanghai Pancreatic Cancer Institute Shanghai 200032China Pancreatic Cancer Institute Fudan UniversityShanghai 200032China

Background: Open pancreaticoduodenectomy(OPD) with portal or superior mesenteric vein resection and reconstruction has been applied in pancreatic cancer patients with tumor infiltration or adherence. However, it is controversial whether laparoscopic pancreaticoduodenectomy(LPD) with major vascular resection and reconstruction is feasible. This study aimed to evaluate the safety and feasibility of LPD with major vascular resection compared with OPD with major vascular resection. Methods: We reviewed data for all pancreatic cancer patients undergoing LPD or OPD with vascular resection at Department of Pancreatic Surgery, Fudan University Shanghai Cancer Center, between February 2018 and May 2022. We compared the preoperative, intraoperative, and postoperative clinicopathological data of the two groups to conduct a comprehensive evaluation of LPD with major vascular resection. Results: A total of 63 patients underwent pancreaticoduodenectomy(PD) with portal or superior mesenteric vein resection and reconstruction, including 25 LPDs and 38 OPDs. The LPD group had less intraoperative blood loss(200 vs. 400 m L, P < 0.001), lower proportion of intraoperative blood transfusion(16.0% vs. 39.5%, P = 0.047), longer operation time(390 vs. 334 min, P = 0.004) and shorter postoperative hospital stay(11 vs. 14 days, P = 0.005). There was no perioperative death in all patients. There was no significant difference in the incidence of total postoperative complications, grade B/C postoperative pancreatic fistula, delayed gastric emptying and abdominal infection between the two groups. No postpancreatectomy hemorrhage nor bile leakage occurred during perioperative period. There was no significant difference in R0 resection rate and number of lymph nodes harvested between the two groups. Patency of reconstructed vessels in the two groups were 96.0% and 92.1%, respectively( P = 0.927). Conclusions: LPD with portal or superior mesenteric vein resection and reconstruction was safe, feasible and oncologically acceptable for selected pat

关键词： Laparoscopy Pancreaticoduodenectomy Whipple procedure Mesenteric veins Portal vein Pancreatic neoplasms

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Atomic-Scale Layer-by-Layer Deposition of Fe SiAl@ZnO@Al_(2)O_(3) Hybrid with Threshold Anti-Corrosion and Ultra-High Microwave Absorption Properties in Low-Frequency Bands

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Nano-Micro Letters 2021年第10期13卷 308-321页

作者： Wei Tian Jinyao Li Yifan Liu Rashad Ali Yang Guo Longjiang Deng Nasir Mahmood xian Jian National Engineering Researching Centre of Electromagnetic Radiation Control Materials Key Laboratory of Multi-Spectral Absorbing Materials and Structures of Ministry of EducationState Key Laboratory of Electronic Thin Films and Integrated DevicesSchool of Electronic Science and EngineeringUniversity of Electronic Science and Technology of ChinaChengdu 611731People’s Republic of China School of Electronic Science and Engineering The Yangtze Delta Region Institute HuzhouUniversity of Electronic Science and Technology of ChinaHuzhou 313001People’s Republic of China School of Materials and Energy University of Electronic Science and Technology of ChinaChengdu 611731People’s Republic of China School of Electrical and Information Engineering Panzhihua UniversityPanzhihua 617000People’s Republic of China School of Engineering RMIT UniversityMelbourneVictoria 3001Australia

Developing highly efficient magnetic microwave absorb-ers(MAs)is crucial,and yet challenging for anti-corrosion properties in extremely humid and salt-induced foggy environments.Herein,a dual-oxide shell of ZnO/Al_(2)O_(3) as a robust barrier to FeSiAl core is introduced to mitigate corrosion resistance.The FeSiAl@ZnO@Al_(2)O_(3) layer by layer hybrid structure is realized with atomic-scale precision through the atomic layer deposition technique.Owing to the unique hybrid structure,the FeSiAl@ZnO@Al_(2)O_(3) exhibits record-high micro-wave absorbing performance in low-frequency bands covering L and S bands with a minimum reflection loss(RLmin)of-50.6 dB at 3.4 GHz.Compared with pure FeSiAl(RLmin of-13.5 dB,a bandwidth of 0.5 GHz),the RLmin value and effective bandwidth of this designed novel absorber increased up to~3.7 and~3 times,respectively.Fur-thermore,the inert ceramic dual-shells have improved 9.0 times the anti-corrosion property of FeSiAl core by multistage barriers towards corrosive medium and obstruction of the electric circuit.This is attributed to the large charge transfer resistance,increased impedance modulus|Z|0.01 Hz,and frequency time constant of FeSiAl@ZnO@Al_(2)O_(3).The research demonstrates a promising platform toward the design of next-generation MAs with improved anti-corrosion properties.

关键词： Atomic layer deposition Magnetic alloy Dual-oxide-shells Microwave absorption Anti-corrosion

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