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Correlation between microstructure and impact toughness of weld heat-affected zone in 5 wt.% manganese steels

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Journal of Iron and Steel research International 2019年第7期26卷 761-770页

作者： Jun-hui Li Hong-hong Wang Qiang Luo Li Li Chao Sun r.d.k. misra The State key Laboratory of refractories and Metallurgy Wuhan University of Science and Technology Wuhan 430081 Hubei China research Institute of Nanjing Iron and Steel Co. Ltd. Nanjing 210035 Jiangsu China Laboratory for Excellence in Advanced Steel research Department of Metallurgical Materials and Biomedical Engineering University of Texas at El Paso El Paso TX 7996& USA

The microstructure in welding heat-affected zones of 5 wt.% manganese steels was studied, and its effect on impact toughness was analyzed. The simulated coarse-grained heat-affected zone (CGHAZ) had the lowest impact toughness of ~39 J at — 40℃ because of coarse-grained structure and least volume fraction of retained austenite (rA) of 1.2 vol.%. The impact toughness of simulated intercritical heat-affected zone (ICHAZ) and fine-grained heat-affected zone (FGHAZ) were ~165 and ~45 J, respectively, at — 40℃. The effective grain size of simulated FGHAZ was smaller than that of the simulated ICHAZ. Furthermore, microstructural investigation revealed that the simulated FGHAZ and ICHAZ had similarity in volume fraction and stability of rA. However, tempered martensite was present in ICHAZ and absent in FGHAZ. It is proposed that the presence of tempered martensite contributed to good impact toughness in simulated ICHAZ.

关键词： 5 wt.% manganese steel Welding heat-affected zone retained austenite Tempered martensite Impact toughness

Nanoscale deformation of multiaxially forged ultrafine-grained Mg-2Zn-2Gd alloy with high strength-high ductility combination and comparison with the coarse-grained counterpart

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Journal of Materials Science & Technology 2018年第2期34卷 311-316页

作者： k. Li V.S.Y.Injeti P. Trivedi L.E. Murr r.d.k. misra department of Metallurgical Materials and Biomedical Engineering University of Texas at El Paso 500 W. University Avenue El Paso TX 79968-0521 USA

Cold processing of magnesium （Mg） alloys is a challenge because Mg has a hexagonal close-packed （HCP） lattice with limited slip systems, which makes it difficult to plastically deform at low temperature. To address this challenge, a combination of annealing of as-cast alloy and multi-axial forging was adopted ro obtain isotropic ultrafine-grained （UFG） structure in a lean Mg-2Zn-2Gd alloy with high strength （yield strength： ~227 MPa）-high ductility （% elongation：～30%） combination. This combination of strength and ductility is excellent for the lean alloy, enabling an understanding of deformation processes in a formable high strength Mg-rare earth alloy. The nanoscale deformation behavior was studied via nanoindentation and electron microscopy, and the behavior was compared with its low strength （yield strength：～46 MPa） - low ductility （% elongation：～7%） coarse-grained （CG） counterpart. In the UFG alloy, extensive dislocation slip was an active deformation mechanism, while in the CG alloy, mechanical twinning occurred. The differences in the deformation mechanisms of UFG and CG alloys were reflected in the discrete burst in the load-displacement plots. The deformation of Mg-2Zn-2Gd alloys was significantly influenced by the grain structure, such that there was change in the deformation mechanism from dislocation slip （non-basal slip） to nanoscale twins in the CG structure. The high plasticity ofUFG Mg alloy involved high dislocation activity and change in activation volume.

关键词： Magnesium alloy Ultrafine-grained Nanoscale deformation

Effect of Nb on corrosion behavior of inner bottom plate of cargo oil tankers

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Journal of Iron and Steel research International 2019年第6期26卷 611-620页

作者： Xiang-yu Xu Long Tian Yun Zhou Ming-yu Sun Xue-min Wang Cheng-jia Shang r.d.k. misra Collaborative Innovation Center of Steel Technology University of Science and Technology Beijing Beijing 100083 China Tianjin Long March Launch Vehicle Manufacturing Co. Ltd. Tianjin 300462 China Institute of research of Iron and Steel (IrIS) Sha-steel Zhangjiagang 215625 Jiangsu China Center for Structural and Functional Materials research and Innovation Department of Metallurgical and Materials Engineering University of Texas at El Paso El Paso TX 7996& USA

The effect of Nb on the corrosion resistance of steels in simulating an oil-corrosion environment was investigated by means of microstructure observation, electrochemical test, dissolved Nb content measurement and Nb segregation observation. The results show that the microstructure of the experimental steels is mainly ferrite with a little pearlite. The dissolved Nb contents of the experimental steels are 0.0235 and 0.0458 wt.%, respectively, while the undissolved Nb content is nearly the same. In addition to enhancing mechanical properties of the steel, dissolved Nb improves the corrosion resistance by enriching Nb in the rust layer. Nb oxides in the rust layer cause a decrease in the corrosion rate due to a decrease in the anodic reaction kinetics. The segregation of Nb at the grain boundaries suppresses the corrosion. Moreover, Nb is enriched at the bottom of the corrosion pit and prevents any further corrosion.

关键词： Low-alloy steel Acid corrosion Pitting corrosion Electrochemical impedance spectroscopy segregation

Signifcant impact of cold-rolling deformation and annealing on damping capacity of Fe-Mn-Cr alloy

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Journal of Iron and Steel research International 2020年第5期27卷 566-576页

作者： Bo Xia Xiao-ming Zhang r.d.k.misra Ming-ming Pan Yu-qian Wang State key Laboratory of rolling and Automation Northeastern UniversityShenyang 110819LiaoningChina Laboratory for Excellence in Advanced Steel research Department of MetallurgicalMaterials and Biomedical EngineeringUniversity of Texas at El PasoEl PasoTX 79668USA

The infuences of cold-rolling deformation and annealing on the damping capacity of Fe-19Mn-8Cr alloy were *** was observed that the cold-rolled Fe-19Mn-8Cr alloy with a reduction of 10%showed the relatively excellent damping capacity because of the relatively moreε-martensite and lower dislocation density,and the reduction of slopes of diferent damping curves increased along with increasing the cold-rolling ***,the subsequent annealing process can further enhance the damping *** 70%cold-rolling deformation,the austenite grain would grow up with the increase in the annealing temperature,which resulted in a signifcant change in the content and morphology ofε-martensite infuencing the damping capacity of the experimental *** damping capacity was optimum when annealed at 800°C for 30 min,displaying that the size ofε-martensite has a vital infuence on the damping capacity of the experimental *** study may enrich the fundamental knowledge about how to ameliorate the damping capacity of Fe-Mn-Cr damping steels.

关键词： damping capacity Fe-19Mn-8Cr damping alloy ε-martensite α′-martensite Cold rolling

Uncovering Microstructure-Property relationship in Ni-Alloyed Fe-Mn-Al-C Low-density Steel Treated by Hot-rolling and Air-Cooling Process

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Acta Metallurgica Sinica(English Letters) 2024年第4期37卷 713-725页

作者： Xiaoliang Jia Guhui Gao Xiaolu Gui Chun Feng r.d.k.misra Bingzhe Bai School of Mechanical Electronicand Control EngineeringBeijing Jiaotong UniversityBeijing100044China CNPC Tubular Goods research Institute Xi’an710077China Laboratory for Excellence in Advanced Steel research University of Texas at El PasoEl PasoTX79968-0521USA School of Material Science and Engineering Key Laboratory of Advanced Materials of Ministry of EducationTsinghua UniversityBeijing100084China

This paper focuses on the relationship between the microstructure and tensile properties of Fe-Mn-Al-C low-density high-strength steel processes by hot-rolling and air-cooling process. The microstructure analysis reveals that the combination of hot-rolling and air-cooling results in the formation of heterogeneous structures comprising different-sized γ and B_(2) phases in the low-density steel with the addition of nickel (Ni). The addition of Ni promotes the formation of the B_(2) phase and induces the pinning of B_(2) phase particles at the γ grain boundaries. This pinning effect effectively hinders the growth of the γ grains, leading to grain refinement. The tensile test results demonstrate that LdS-5Ni (low-density steel, LdS) exhibits excellent high strength and ductility combination, e.g., a tensile strength of 1535 MPa, yield strength of 1482 MPa, and elongation of 23.3%. These remarkable mechanical properties are primarily attributed to the combined strengthening contributions of grain refinement and duplex nano-sized second-phase precipitation hardening.

关键词： Low-density steel Microstructure B_(2)phase κ-Carbide Tensile properties

Influence of Component Size on the Corrosion Behavior of Ti6Al4V Alloy Fabricated by Electron Beam Powder Bed Fusion

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Acta Metallurgica Sinica(English Letters) 2024年第1期37卷 159-168页

作者： Hongyu Zheng Xin Gai Yun Bai Wentao Hou Shujun Li Yulin Hao r.d.k.misra rui Yang Institute of Metal research Chinese Academy of SciencesShenyang110016China School of Materials Science and Engineering University of Science and Technology of ChinaShenyang110016China Nuclear Power Institute of China Chengdu610213China department of Metallurgical Materialsand Biomedical EngineeringThe University of Texas at El Paso500WUniversity AvenueEl PasoTX79968USA

The electrochemical behavior of Ti-6Al-4V with 1 mm and 16 mm thickness prepared by electron beam powder bed fusion(EB-PBF)was investigated in phosphate buffered *** results showed that EB-PBF Ti-6Al-4V with a larger component size was more resistant to corrosion compared to the smaller component,because of less acicularαʹphase content and moreβphase *** a non-equilibrium phase in the“high-energy state”,αʹphase has a greater susceptibility to corrode and reduces the corrosion resistance of the material,whileβphase improves corrosion resistance of titanium *** results show that the phase composition has a more significant effect on the corrosion performance than the grain size.

关键词： Electron beam powder bed fusion Ti6Al4V alloy Corrosion resistance Component size Polarisation

Effect of La on the Corrosion Behavior and Mechanism of 3Ni Weathering Steel in a Simulated Marine Atmospheric Environment

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Acta Metallurgica Sinica(English Letters) 2024年第2期37卷 308-324页

作者： Gang Niu rui Yuan r.d.k.misra Na Gong Zhi-Hui Zhang Hao-Xiu Chen Hui-Bin Wu Cheng-Jia Shang Xin-Ping Mao Collaborative Innovation Center of Steel Technology University of Science and Technology BeijingBeijing100083China Laboratory for Excellence in Advanced Steel research Department of MetallurgicalMaterials and Biomedical EngineeringUniversity of Texas at El PasoEl PasoTX79968USA Institute of Materials research and Engineering Agency for ScienceTechnologyand ResearchSingapore138634Singapore department of Materials Science and Engineering University of TorontoTorontoONM5S 3E4Canada

The corrosion behavior and mechanism of 3Ni weathering steel in a simulated oceanic atmospheric environment are investigated in order to comprehend the impacts of La,as determined through electrochemical analysis and rust layer *** results of this study demonstrate that the addition of La enhances the corrosion resistance of 3Ni weathering steel in the marine atmospheric environment,thereby reducing the corrosion rate and improving the protection of the rust *** influence of La on corrosion resistance can be attributed to two primary ***,La functions as a grain refiner,minimizing the potential difference of the micro-regions on the substrate surface,thereby significantly reducing the corrosion of bare steel in the marine ***,La inhibits the process of Fe_(3)O_(4) oxidation back toγ-FeOOH during corrosion at the local site,thus decreasing the formation ofγ-FeOOH and enhancing the charge transfer *** research work may serve as a reference for expanding the application of rare earth elements in the field of weathering steel.

关键词： Weathering steel rare earth rust layer Corrosion behavior Corrosion resistance

Flavonoid Myricetin as Potent Anticancer Agent: A Possibility towards development of Potential Anticancer Nutraceuticals

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Chinese Journal of Integrative Medicine 2024年第1期30卷 75-84页

作者： Anchal Trivedi Adria Hasan rumana Ahmad Sahabjada Siddiqui Aditi Srivastava Aparna misra Snober S.Mir department of Biochemistry Era's Lucknow Medical College&HospitalEra UniversityLucknow(226003)India Molecular Cell Biology Laboratory Integral Information and Research Centre-4(IIRC-4)Department of BioengineeringFaculty of EngineeringIntegral UniversityLucknow(226026)India department of Biotechnology Era's Lucknow Medical College&HospitalEra UniversityLucknow(226003)India department of Biosciences Faculty of ScienceIntegral UniversityLucknow(226026)India

Good nutrition plays a crucial role in maintaining a balanced lifestyle. The beneficial effects of nutrition have been found to counteract nutritional disturbances with the expanded use of nutraceuticals to treat and manage cardiovascular diseases, cancer, and other developmental defects over the last decade. Flavonoids are found abundantly in plant-derived foods such as fruits, vegetables, tea, cocoa, and wine. Fruits and vegetables contain phytochemicals like flavonoids, phenolics, alkaloids, saponins, and terpenoids. Flavonoids can act as anti-inflammatory, anti-allergic, anti-microbial(antibacterial, antifungal, and antiviral) antioxidant, anti-cancer, and anti-diarrheal agents. Flavonoids are also reported to upregulate apoptotic activity in several cancers such as hepatic, pancreatic, breast, esophageal, and colon. Myricetin is a flavonol which is naturally present in fruits and vegetables and has shown possible nutraceutical value. Myricetin has been portrayed as a potent nutraceutical that may protect against cancer. The focus of the present review is to present an updated account of studies demonstrating the anticancer potential of myricetin and the molecular mechanisms involved therein. A better understanding of the molecular mechanism(s) underlying its anticancer activity would eventually help in its development as a novel anticancer nutraceutical having minimal side effects.

关键词： myricetin flavonoids anticancer nutraceuticals Chinese medicine Ayurveda complementary and alternative medicine

Highly ductile hypereutectic Al-Si alloys fabricated by selective laser melting

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Journal of Materials Science & Technology 2022年第15期110卷 84-95页

作者： Yafeng Yang kang Geng Shaofu Li Michael Bermingham r.d.k.misra State key Laboratory of Multiphase Complex Systems Institute of Process EngineeringChinese Academy of SciencesBeijing 100190China University of Chinese Academy of Sciences Beijing 100049China School of Mechanical and Mining Engineering University of QueenslandSaint LuciaQueensland 4072Australia department of Metallurgical Materials and Biomedical EngineeringUniversity of Texas at El Paso500 W University AvenueEl PasoTX 79968USA

In the endeavor to maximize the refinement effect of primary Si and alleviate the inherent brittleness of hypereutectic Al-Si alloy,the approach of coating P as a modifier on powder was *** ultimate aim was to create more heterogeneous fine Al P nucleus and enhance the nucleation efficiency of primary Si on Al P to refine the coarse primary Si to nano-scale during 3d *** the combination of large undercooling and high density of nucleation sites,the size of primary Si was successfully refined to 200–300 nm and the divorced eutectic was also induced to modify the microstructure of *** the presence of nano-scale primary Si,the melting pool boundary(MPB)feature disappeared and the fracture mechanism also changed from load transfer to interfacial *** with the pristine alloy,the ductility was increased four times without significantly changing the ultimate tensile strength(UTS)and wear *** improvement of ductility is attributed to the refinement of primary Si,the disappearance of MPB features and the formation of divorced *** optimal tensile properties were:UTS-482 MPa,yield strength-320 MPa and ductility of 8.1%at 0.05 wt.%*** are comparable to those for high-strength Al alloys.

关键词： Al-Si alloys Heterogeneous nucleation ductility Powder processing Selective laser melting