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Open Journal of Applied Sciences 2014年第6期4卷 354-359页

作者： Umar Salami Ameuru mohammed kabir yakubu Kasali Ademola Bello Department of Textile Science and Technology Ahmadu Bello University Zaria Nigeria

Nitrosonaphthol dyes and other corresponding analogues were synthesised from 1-Naphthol. The dyes were applied onto chrome and vegetable tanned leather upon characterization. The results indicate that the dye bath exhaustion was better on chrome tanned leather than on vegetable tanned leather. This may be attributed to the chelating effect of chrome on leather and the higher temperature of dyeing the chrome tanned leather compared with the vegetable tanned leather. The fastness properties of the dyes of washing ranging from (3 - 5), perspiration on acid (4 - 5), alkaline (4 - 5) and light (4 - 7) were impressive on both vegetable and chrome tanned leather respectively.

关键词： 2-Nitroso-1-Naphthol Tanned Leather Exhaustion Fastness

Synthesis of Some Azo Disperse Dyes from 1-Substituted 2-Hydroxy-6-pyridone Derivatives and Their Colour Assessment on Polyester Fabric

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Open Journal of Applied Sciences 2012年第1期2卷 54-59页

作者： Kurenkaka Johnson Sakoma Kasali Ademola Bello mohammed kabir yakubu Department of Textile Science and Technology Ahmadu Bello University Zaria Nigeria

The synthesis of a series of 3-(p-substituted phenylazo)-6-pyridone dyes which is suitable for the dyeing of polyester fabrics, is described. Visible absorption spectra of the dyes were examined in various solvents and the compounds in solution exhibited hydrazone-common anion equilibrium. The electronic absorption spectra cover a λmax range of 404 - 464 nm in DMF at uniformly high absorption intensity between 5.33 × 104 - 8.55 × 104 lmol–1cm–1 and gave bright intense hues of yellow to orange on polyester fabrics. The colour parameters of the dyed fabrics were measured and the dyes have excellent exhaustion between 72% - 79% for polyester fabrics, more intense and of very good fastness properties on polyester fabrics. The remarkable degree of levelness and brightness after washing is indicative of good penetration and excellent affinity of these dyes for the polyester fabric.

关键词： Pyridone Disperse Dye Exhaustion Carrier Polyester Fastness

The Synthesis of Diaminoanthraquinone Coloured Cross Linked Epoxy Resins and Their Application in Paint and Selected Polymers

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Open Journal of Applied Sciences 2014年第1期4卷 13-21页

作者： Zwahruddeen Muhammad Salisu mohammed kabir yakubu Peter Obinna Nkeonye Hamza Abba Department of Chemistry Ahmad Bello University Zaria Nigeria Department of Textile Science and Technology Ahmadu Bello University Zaria Nigeria National Research Institute for Chemical Technology (NARICT) Zaria Nigeria

Novel polymeric pigments were synthesized in xylene by cross linked epoxy resin with 1,4 and 1,5-diaminoanthraquinones, by varying weight fractions from 5% to 20% of the diaminoanthraquinone derivatives. FTIR, UV and solubility tests were carried out. The pigments were then used to colour PLA, PMMA, PE and also in emulsion paints using polyvinyl alcohol as binder. Their light fastness, surface drying time and surface hardening time were assessed. It was found that λmax of the 1,4-diaminoanthraquinone shifted towards longer wavelength after the cross linkage, in contrast to the 1,5-diaminoanthraquinone which suffered a blue shift. However in all the cases, the λmax was not affected by the weight fractions of the anthraquinones, but the absorptivity coefficients was significantly increased as the weight fractions of the anthraquinones increased. The light fastness properties of the coloured plastics varied from 4 to 7, indicating a trend of increase with the weight fractions of the anthraquinones. Similar observations were seen with the emulsion paints produced. In all the cases, the 1,4-diaminoanthraqunione produced better result.

关键词： Epoxy Resin Diaminoanthraquinone Derivatives Chromophore Pigments

Synthesis and Characterisation of Colorants Derived from 1,4-Diamino Anthraquinone Polyamides

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Advances in Chemical Engineering and Science 2012年第2期2卷 300-308页

作者： mohammed kabir yakubu Mohammad Sani Gumel Mansur Bala Ibrahim Rakesh Kumar Centre for Scientific and Industrial Research (CSIR) Materials Science and Manufacturing Port Elizabeth South Africa Department of Pure and Industrial Chemistry Bayero University Kano Nigeria Department of Textile Science and Technology Ahmadu Bello University Zaria Nigeria

In this study, the polycondensation products of a diamine anthraquinone (1,4-diamino anthraquinone) and some aliphatic diacids with different methylene numbers were synthesised. Their UV-visible spectroscopy and thermal properties were then characterised. The synthesis was achieved by reacting equimolar solutions of the amine and the acid halides. The structure and thermal properties of the products were characterised. FT-IR Spectra of all the three products revealed the formation of amide due to the presence of strong bands at 1565 and 3390 cm?1 assignable to C=O stretching and N-H vibrations. Differential Scanning Calorimetry revealed high melting exotherms for the products. Thermogravimetry revealed moderate thermal stabilities for Poly NAM and Poly NAS and low thermal stability for Poly NAA which indicated 5.9%, 7.1% and 61.2% weight losses at 285℃, 285℃ and 374℃ for the three products respectively. The wavelengths of maximum absorbance for the dye samples are 601.5, 591 and 589 nm respectively with absorptivity coefficients (a1cm1% ) of 11640000, 11610000 and 11560000 respectively.

关键词： Anthraquinone Polymeric Dyes Polyamide Synthesis Characterisation

Optimisation of Crude Oil Adsorbent Developed from a Modified Styrene Kenaf Shive

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Journal of Materials Science and Chemical Engineering 2019年第2期7卷 38-51页

作者： Zwahruddeen Muhammad Salisu Ishiaku S. Umaru Danladi Abdullahi mohammed kabir yakubu Diya’uddeen Bashir Hasan National Research Institute for Chemical Technology (NARICT) Zaria Nigeria Department of Polymer and Textile Engineering Ahmadu Bello University (ABU) Zaria Nigeria Center for Energy Research and Training (CERT) Ahmadu Bello University (ABU) Zaria Nigeria

A new kind of hydrophobic crude oil sorbent was successfully developed by grafting kenaf shive with styrene monomer. In this paper, crude oil sorbents were developed through regeneration method by varying the initiator concentration, monomer ratio and particle sizes in the range of 0.5 - 2.5 wt%, 0.5 - 2.0 wt % and 125 - 1000 μm respectively. This research approach for the development of crude oil sorbent from graft modified kenaf shive/core and the aforementioned variable optimization has not been reported. The effect studies of the individual and combine factors were carried out using a statistical experimental design matrix using five-level central composite design (CCD). Respond surface methodology (RSM) was used to optimise and develop equations of the aforementioned variables (initiator concentration, monomer ratio and particle sizes). The optimal swelling capacity of 616% and 267% lower retention were achieved at initiator concentration, monomer ratio and particle size of 12.5 wt%, 1.50 wt% and 562 μm respectively. TGA-DTA, XRD and BET analysis were carried out on optimised sample and, FTIR was carried on both unmodified (UG) and optimized sorbent. Further computations were done for grafting efficiency (GE), homopolymers and density. The findings display the effect of the three variables and navigation equations were generated for further investigations on them. However, the results show the feasibility and robustness of facile oil sorption.

关键词： Sorbent Initiator Crude Oil Kenaf Shive Respond Surface Methodology (RSM)

Pattern of Eye Diseases among Tea Workers

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Open Journal of Ophthalmology 2024年第2期14卷 117-127页

作者： Rifat Binth Rezayee Md. Showkat kabir mohammed Moinul Hoque Nirupam Chowdhury Mohammad Shish Rahman Nawreen Binte Anwar Shah-Noor Hassan Department of Community Ophthalmology Bangabandhu Sheikh Mujib Medical University Dhaka Bangladesh Department of Ophthalmology Bangabandhu Sheikh Mujib Medical University Dhaka Bangladesh

Background: Bangladesh’s tea industry is essential to the country’s economic expansion. Since tea workers in Bangladesh are marginalized within our community, they have limited access to comprehensive eye care services. Productivity and well-being are cornerstones of comprehensive health care strategy. Ocular disorders are influenced by life expectancy, sociodemographic status, and the epidemiological transition. In this context, the state of ocular health and the many eye illnesses remain to be significantly addressed. Purpose: To evaluate the pattern of eye diseases among tea workers in a tea estate of Bangladesh. Methods: This cross-sectional observational study was carried out in Halda Valley Tea Estate, Nazirhat, Fatickchari, Chattogram, Bangladesh, under the supervision of the Department of Community Ophthalmology, BSMMU, following ethical clearance and approval by the IRB board of BSMMU. With informed written consent and approval from the authority of the tea estate, a total of 110 tea workers were recruited. Socio-demographic characteristics, ocular findings, and patterns of eye diseases were determined and recorded. Results: The mean age of the study participants was 39.60 ± 11.63 years. The maximum (58.1%) study participants were 31 - 50 years old, female (64.5%), illiterate (82.7%), and tribal (71.8%) indigenes. Eye diseases were found in 94.5% of workers. Presbyopia (28.2%), cataracts (27.3%), and refractive error (26.4%) were the most common. Tea workers with eye diseases were significantly older than those who did not have any eye diseases (40.20 ± 11.57 vs. 29.17 ± 7.31 years, p Conclusion: A significant number of tea workers had eye diseases, of which presbyopia, cataracts, and refractive error were the most common.

关键词： Tea Workers Eye Diseases Presbyopia Cataract Refractive Errors

Thermo-Physical Potential of Recycled Banana Fibers for Improving the Thermal and Mechanical Properties of Biosourced Gypsum-Based Materials

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Journal of Renewable Materials 2024年第4期12卷 843-867页

作者： Youssef Maaloufa Soumia Mounir Sara Ibnelhaj Fatima Zohra El Wardi Asma Souidi yakubu Aminu Dodo Malika Atigui Mina Amazal Abelhamid Khabbazi Hassan Demrati Ahmed Aharoune National School of Architecture Agadir New ComplexIbn Zohr UniversityAgadirMorocco Energy Materials and Sustainable Development(EMDD)Center for WaterNatural ResourcesEnvironment and Sustainable Development(CERNE2D)Mohammed V UniversityRabatMorocco Thermodynamics and Energetics Laboratory Faculty of ScienceIbn Zohr UniversityAgadirMorocco Architectural Engineering Department Najran UniversityNajranSaudi Arabia The Centre of Scientific and Engineering Research Najran UniversityNajranSaudi Arabia Physics Department LPMAT LaboratoryFaculty of Sciences Ain ChockHassan II UniversityCasablancaMorocco

The development of bio-sourced materials is essential to ensuring sustainable construction;it is considered a locomotive of the green ***,it is an abundant material in our country,to which very little attention is being *** work aims to valorize the waste of the trunks of banana trees to be used in ***,the physicochemical properties of the fiber,such as the percentage of crystallization and its morphology,have been determined by X-ray diffraction tests and scanning electron microscopy to confirm the potential and the impact of the mode of drying on the quality of the banana fibers,with the purpose to promote the use of this material in ***,the results obtained with the gypsum matrix allowed us to note a preponderant improvement in the composite’s thermal properties thanks to the variation of the banana fiber ***,the impact of the nature of the banana fiber distribution(either fiber mixed in matrix or fiber series model)on the flexural and compressive strengths of the composites was *** results obtained indicate that the insulation gain reaches up to 40%.It depends on the volume fraction and type of distribution of the banana ***,the thermal inertia of the composites developed,represented by thermal diffusivity and thermal effusivity,was *** indicate a gain of 40%and 25%,respectively,in terms of thermal diffusivity and thermal effusivity of the developed composites compared to plaster *** the mechanical properties,the flexural strength depends on the percentage of the volume fraction of banana fibers used,and it can reach 20%more than the flexural strength of plaster;nevertheless,there is a significant loss in terms of the compressive strength of the studied *** results obtained are confirmed by the microstructure of the fiber *** fact,the morphology of the banana fibers was improved by the drying *** reduces the amorphous area an

关键词： Biosourced materials fiber banana flexural strength mechanical properties open-air drying plaster thermal properties waste management

Study of Hygrothermal Behavior of Bio-Sourced Material Treated Ecologically for Improving Thermal Performance of Buildings

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Journal of Renewable Materials 2024年第5期12卷 1007-1027页

作者： Soumia Mounir Miloudia Slaoui Youssef Maaloufa Fatima Zohra El Wardi yakubu Aminu Dodo Sara Ibn-Elhaj Abdelhamid Khabbazi National School of Architecture Agadir New Complex Ibn Zohr AgadirHay dakhla80000Morocco EMDD CERNE2DUniversity Mohammed V in RabatEst SaléSaléMedinaMorocco Physics Department LPMAT LaboratoryFaculty of Sciences Ain ChockHassan II UniversityCasablancaMorocco Architectural Engineering Department College of Engineering Najran UniversityNajran66426Saudi Arabia The Centre of Scientific and Engineering Research Najran UniversityNajranSaudi Arabia

Creating sustainable cities is the only way to live in a clean environment,and this problem can be solved by using bio-sourced and recycled *** this purpose,the authors contribute to the valuation of sheep wool waste as an eco-friendly material to be used in *** paper investigates the thermal,hygrothermal,and biological aspects of sheep wool by testing a traditional *** biological method of aerobic mesophilicﬂora has been *** X was used to determine the chemical composition of the materials ***,thermal characterization has been *** thermal conductivity is above 0.046(W·m^(-1)·K^(-1))and the thermal diffusivity is 1.56.10^(-6) m^(2)·s^(-1).Besides,the energy efﬁciency of using sheep wool in buildings was ***,its humidity behavior was evaluated in different aspects in both winter and *** of biological analyses show the efﬁciency of the treatment by removing the majority of the microorgan-isms:the value of yeast and mildew was reduced from 38.10^(2) to 2.10^(2)(UFC·g^(-1)).In addition to that,sheep wool permits obtaining a low thermal transmittance on the scale of the walls and low cooling needs on the scale of the building with a gain of 45%and 52%,respectively.

关键词： Sustainability sheep wool biological treatment hygrothermal wool behavior hot wire method

The alteration in the architecture of a T-DNA insertion rice mutant osmtd1 is caused by up-regulation of Micro RNA156f

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Journal of Integrative Plant Biology 2015年第10期57卷 819-829页

作者： Qing Liu Gezhi Shen Keqin Peng Zhigang Huang Jianhua Tong mohammed Humayun kabir Jianhui Wang Jingzhe Zhang Genji Qin Langtao Xiao Hunan Provincial Key Laboratory of Phytohormones and Growth Development Hunan Provincial Key Laboratory for Crop Germplasm Innovation and Utilization Hunan Agricultural University Crop Institute Shanghai Academy of Agricultural Sciences Horticulture Institute Sichuan Academy of Agricultural Sciences State Key Laboratory of Protein and Plant Gene Research College of Life Sciences Peking University

Plant architecture is an important factor for crop production. Some members of microRNA156 (miR156) and their target genes SQUAMOSA Promoter-Binding Protein-Like (SPL) were identified to play essential roles in the establishment of plant architecture. However, the roles and regulation of miR156 is not well understood yet. Here, we identified a T-DNA insertion mutant Osmtd1 (Oryza sativa multi-tillering and dwarf mutant). Osmtd1 produced more tillers and displayed short stature phenotype. We determined that the dramatic morphological changes were caused by a single T-DNA insertion in Osmtd1. Further analysis revealed that the T-DNA insertion was located in the gene Os08g34258 encoding a putative inhibitor I family protein. Os08g34258 was knocked out and OsmiR156f was significantly upregulated in Osmtd1. Overexpression of Os08g34258 in Osmtd1 complemented the defects of the mutant architecture, while overexpression of OsmiR156f in wild-type rice phenocopied Osmtd1. We showed that the expression of OsSPL3, OsSPL12, and OsSPL14 were significantly downregulated in Osmtd1 or OsmiR156f overexpressed lines, indicating that OsSPL3, OsSPL12, and OsSPL14 were possibly direct target genes of OsmiR156f. Our results suggested that OsmiR156f controlled plant architecture by mediating plant stature and tiller outgrowth and may be regulated by an unknown protease inhibitor I family protein.

关键词： Oryza sativa OsmiR156f plant architecture protease inhibitor T-DNA insertion

Occurrence of <i>Escherichia coli</i>O157 in Retailed-Beef and Related Meat Products in Zaria, Nigeria

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Food and Nutrition Sciences 2014年第6期5卷 481-487页

作者： Salome Y. Tafida Jacob K. P. Kwaga mohammed Bello Junaidu kabir Veronica J. Umoh Sabo E. yakubu Andrew J. Nok Centre for Biotechnology Research and Training Ahmadu Bello University Zaria Nigeria Department of Livestock and Pest Control Services Federal Ministry of Agriculture Gombe Nigeria Department of Microbiology Faculty of Science Ahmadu Bello University Zaria Nigeria Department of Veterinary Public Health and Preventive Medicine Faculty of Veterinary Medicine Ahmadu Bello University Zaria Nigeria

This study evaluated retailed-beef and related meat products for E. coli O157 in Zaria, Nigeria. Sample types included raw meat, “suya” (roasted meat), “balangu” (barbequed meat), “kilishi” (spiced sun dried meat) and “dambu” (shredded fried meat). A total of 182 samples were analyzed for E. coli O157. Isolates were characterized using conventional biochemical methods and Microbact 12E test kit. Susceptibilities of the isolates to 18 commonly used antimicrobial agents were determined by the disk diffusion method. The carriage of stx1 and stx2 genes was determined by PCR. Microbact confirmed 4 E. coli isolates. All isolates exhibited multiple drug resistance to the antimicrobial agents tested. An overall prevalence of 2.2% was obtained for E. coli O157. All 4 isolates of E. coli O157 were isolated from raw meat;two of which harboured the stx1 gene.

关键词： E. coli O157 Meat Products Multiple Drug Resistance Food Safety