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Luminescence study of europium(III) tris(β-diketonato)/phosphonate complexes in chloroform

Journal of Rare Earths 2008年第2期26卷 185-191页

作者： Stefan Lis Zbigniew Piskula Krzysztof Staninski Sayaka Tamaki masayuki Inoue Yuko Hasegawa Department of Rare Earths Faculty of Chemistry Adam Mickiewicz University Grunwaldzka 6 Department of Chemistry Faculty of Science Science University of Tokyo

The extraction of Eu（Ⅲ） with β-diketone, HA, and monodentate or bidentate Lewis bases, B, into chloroform and the luminescence properties of the extracted species were studied. Pivaloyltrifluoroacetone, Hpta, and 2-thenoyltfifluoroacetone, Htta, were used as the β-diketones. The Lewis bases, B, were tetraethyl methylene diphosphonate, POPO, which was bidentate, and diethyl benzylphosphonate, PhPO which was monodentate. Based on the extraction data, the stability constants, log β, of the first complexes between tfis（β-diketonato）Eu（Ⅲ） and the phosphonate, EuA3B, were determined to be 6.0 for the POPO complex and 3.40 for the PhPO complex. The Eu（Ⅲ） luminescence intensity in the EuA3POPO was larger than EuA3 where A was either pta or tta at similar concentrations of Eu（Ⅲ）, while that in Eu（pta）3PhPO was stronger than EuA3; however, in Eu（tta）3PhPO, it was weaker than Eu（tta）3. The POPO functions as a sensitizer, and the PhPO functions as a quencher for the tta chelate and as a sensitizer for the pta chelate. From the lifetime and quantum yield, φ, of the Eu（Ⅲ） luminescence in the complexes as well as the observation of the extractability of Eu（Ⅲ） with the Hpta and the phosphonates and of the luminescence spectra of the complexes, it was confirmed that the extraction of Eu（Ⅲ） was remarkably enhanced with a β-diketonate and a strong Lewis base, and also the ternary complex that was formed as the extracted species, showed luminescence enhancement. This phenomenon may be due the formation of a strong bond between the Eu（Ⅲ） and the strong Lewis base leading to more hydrophobicity in the extracted species and also to more effective energy transfer from the Lewis base to the Eu（Ⅲ）. It was not significant whether the donor atoms were N or O.

关键词： tris(β-diketonato)Eu(Ⅲ) extraction luminescence phosphonate ligands rare earths

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Joint Angle Correction in Rheumatoid Arthritis and Its Reliability Analysis Based on Phase Dispersion Quantification

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Open Journal of Medical Imaging 2022年第4期12卷 171-179页

作者： Yafei Ou Prasoon Ambalathankandy Ryunosuke Furuya Tamotsu Kamishima masayuki Ikebe Research Center for Integrated Quantum Electronics Hokkaido University Sapporo Japan Faculty of Health Sciences Hokkaido University Sapporo Japan

Background: Rheumatoid arthritis is a form of autoimmune disease characterized by synovitis that can ultimately cause joint deformities and impaired functioning. The cartilage destruction is one of the most important indicators for diagnosis and treatment of rheumatoid arthritis, and it is radiographically manifested as joint space narrowing. Issue: In the literature, the joint space narrowing progression between a baseline and its follow-up finger joint images can be quantified by using image registration algorithm. We found that the inconsistencies of joint angles may lead to characteristic mismatches and thus severely affect the accuracy of joint space narrowing quantifications. Methods: In this work, we introduce a rotation invariant phase only correlation in joint space narrowing quantification for the joint angle correction. Further, we propose a confidence index to quantify the quantification reliability of phase only correlation based on phase dispersion in phase difference spectrum. Conclusion: In our clinical experiments, the proposed quantification method can effectively overcome and manage the mismatch due to the inconsistency of joint angles. Additionally, the confidence index shows a high consistency with the joint space narrowing progression examinations manually done by a trained radiologist and one radiological technologist.

关键词： Rheumatoid Arthritis Joint Space Narrowing Frequency Domain Analysis Radiology Computer-Aided Diagnosis Phase Dispersion

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Whole-body PET tracking of a D-dodecapeptide and its radiotheranostic potential for PD-L1 overexpressing tumors

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Acta Pharmaceutica Sinica B 2022年第3期12卷 1363-1376页

作者： Kuan Hu Wenyu Wu Lin Xie Hao Geng Yiding Zhang masayuki Hanyu Lulu Zhang Yinghuan Liu Kotaro Nagatsu Hisashi Suzuki Jialin Guo Yundong Wu Zigang Li Feng Wang Mingrong Zhang Department of Advanced Nuclear Medicine Sciences National Institute of Radiological SciencesNational Institutes for Quantum and Radiological Science and TechnologyChiba 263-8555Japan Department of Nuclear Medicin5 Nanjing First HospitalNanjing Medical UniversityNanjing 210006China State Key Laboratory of Chemical Oncogenomics the School of Chemical Biology and BiotechnologyPeking UniversityShenzhen Graduate SchoolShenzhen 518055China Rensselaer Polytechnic Institute Shenzhen 518118China Institute of Chemical Biology Shenzhen Bay LaboratoryShenzhen 518038China Pingshan Translational Medicine Center Shenzhen Bay LaboratoryTroyNY 12180USA

Peptides that are composed of dextrorotary(D)-amino acids have gained increasing attention as a potential therapeutic ***,our understanding of the in vivo fate of D-peptides is *** highlights the need for whole-body,quantitative tracking of D-peptides to better understand how they interact with the living ***,we used mouse models to track the movement of a programmed death-ligand 1(PD-L1)-targeting D-dodecapeptide antagonist(DPA)using positron emission tomography(PET).More specifically,we profiled the metabolic routes of[^(64)Cu]DPA and investigated the tumor engagement of[^(64)Cu/^(68)Ga]DPA in mouse *** results revealed that intact[^(64)Cu/^(68)Ga]DPA was primarily eliminated by the kidneys and had a notable accumulation in ***,a single dose of[^(64)Cu]DPA effectively delayed tumor growth and improved the survival of ***,these results not only deepen our knowledge of the in vivo fate of D-peptides,but also underscore the utility of D-peptides as radiopharmaceuticals.

关键词： D-peptide PET imaging Radiotheranostics In vivo fate PD-L1

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Xanthogranulomatous Inflammation of Myometrium Causing Pelvic Extension: Report of Two Cases

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Open Journal of Obstetrics and Gynecology 2022年第2期12卷 147-153页

作者： Kyousuke Takeuchi Ai Yoshida Makoto Sugimoto masayuki Fujita Hiroki Morita Department of Obstetrics and Gynecology National Hospital Organization Kobe Medical Center Kobe Japan Department of Pathology National Hospital Organization Kobe Medical Center Kobe Japan Department of Obstetrics and Gynecology Kohnan Medical Center Kobe Japan

Background: Xanthogranulomatous inflammation of the female reproductive organs is a rare chronic inflammation. In most reported cases, the lesion was limited to the endometrium and fallopian tubes. Here, we report two cases of xanthogranulomatous inflammation of the myometrium with a history of endometrial biopsy. Case Reports: In two cases, myometrial xanthogranulomatous inflammation destroyed the myometrium. This inflammation developed into surrounding pelvic organs, resulting in uterine perforation. Conclusion: When inflammatory lesions are found after intrauterine manipulation, the possibility of developing xanthogranulomatous inflammation should be considered. If antibiotics are ineffective, prompt surgical treatment is necessary.

关键词： Xanthogranulomatous Inflammation Myometrium Klebsiella Pneumoniae Surgical Intervention Endometrial Biopsy

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Influence of Si,Ce,Sb and Sn on chunky graphite formation

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China Foundry 2011年第1期8卷 96-100页

作者： Hideo Nakae masayuki Fukami Takayuki Kitazawa Ying Zou Lab. for Mater. Sci. and Tech. Waseda Univ. Tokyo Japan JFE Steel Corp. Japan Nippon Steel Corp. Japan Appl. Mech. and Eng. Waseda Univ. Tokyo Japan

The thirteen mother alloys,C%+1/3Si%=4.45%,differing in their Si,Ce,Sb and Sn contents,were *** grams of these alloys was remelted in a high purity alumina crucible at 1,450oC under an Ar atmosphere,and then cooled at 30 K/min for obtaining their cooling *** graphite morphologies were observed using an optical microscope and an *** three-dimensional graphite shapes were observed by the SEM using the samples whose matrices were etched off with an acid-aqua solution,to confirm the chunky *** discussing the influence of the Si and Ce contents on the chunky graphite formation,two experiments were carried *** the first one,the Si contents were changed from 0 to 4% in the 0.15%Ce alloys,and for the second one,the 3.5%Si and 4%Si samples that differed in the Ce contents of 0.1 and 0.2% were *** the third experiment,the influence of Sb and Sn on the chunky graphite formation was investigated by using the 4%Si and 0.1%Ce *** results showed that with the increase of the Si content,the volume fraction of the chunky graphite increases,while the volume fraction of the ledeburite decreases,and the chunky graphite volume fraction in the 0.2%Ce samples is higher than that of the 0.1%Ce *** effect of the Sb and Sn additions on the prevention of chunky graphite formation cannot be confirmed due to their high Si ***,further studies will be needed in this field.

关键词：矮胖的石墨球状的石墨石墨形态学生铁的团结

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《庄子》“化”概念与“物化”思想的多层结构

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人文杂志 2023年第8期 1-15页

作者： [日]佐藤将之台湾大学哲学系中国台湾

文章透过现本《庄子》中的“化”“变”“物化”“变化”以及与此相关的用例之分析,欲阐明《庄子》“物化”论的多层意涵及其独特思想意义。文章首先将“化”论分成四种涵义:生物体本身的变化、“生死”过程以及不同生物之间连环、意识... 详细信息

文章透过现本《庄子》中的“化”“变”“物化”“变化”以及与此相关的用例之分析,欲阐明《庄子》“物化”论的多层意涵及其独特思想意义。文章首先将“化”论分成四种涵义:生物体本身的变化、“生死”过程以及不同生物之间连环、意识的变化、境界和想象中全部“物”之间的转换。接着指出《庄子》的“物化”论还具有论述上的两种重要功能:“主题的转换”和“不同主题的整合”。基于此分类,文章试图论证《庄子》中多样多层的“化”论成为“因为万物化成其他物,不同物实为同一物”之思维方式的基础。若从其“物化”论的发展来看,在《天地》的“其死也物化”一句中所看到的其生体变化和生死意涵的“物化”论可能很早就存在,而《逍遥游》“北冥有鱼”和《齐物论》“庄周梦蝶”所追求的在“万物齐同”的境界中融于“齐一”境界的“物化”论则因与《天下》“庄周论”的内容相呼应,其撰写时期应该在现本内容形成过程中属于较晚期,当为战国晚期。

关键词：道家《庄子》变化齐物物化

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Reliability of Relative Paleointensity Recorded in Chinese Loess-Paleosol Sediments

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Acta Geologica Sinica(English Edition) 2012年第5期86卷 1276-1288页

作者： YANG Tianshui LI Haiyan WU Huaichun YANG Zhenyu ZHANG Shihong HYODO masayuki State Key Laboratory of Biogeology and Environmental Geology China University of GeosciencesBeijing 100083China School of the Earth Sciences and Resources China University of GeosciencesBeijing 100083China School of Ocean Sciences and Resources China University of GeosciencesBeijing 100083China Institute of Geomechanics Chinese Academy of Geological SciencesBeijing 100081China Research Center for Inland Seas Kobe UniversityKobe 657-8501Japan

A detailed paleomagnetic and rock-magnetic investigation spanning loess L7 to paleosol S8 has been carried out at the Baoji and Xifeng sections. Results of anisotropy of magnetic susceptibility confirm that the studied loess-paleosol sediments retain primary sedimentary fabrics. Stepwise thermal demagnetization shows that two well-defined magnetization components can be isolated from both loess and paleosol specimens. A low-temperature component, isolated between 100°C and 200°C, is consistent with the present geomagnetic field direction, and a high-temperature component, isolated between 200-300°C and 620-680°C, includes clearly normal and reversed polarities. Isothermal remanent magnetization and thermomagnetic analyses indicate that characteristic remanent magnetization is mainly carried by magnetite and hematite. The Day plot, together with the stratigraphic variations of rock-magnetic parameters, shows that the uniformity of magnetic mineralogy and grain size fulfills the criteria for relative paleointensity （RPI） studies. RPI records have been constructed using natural remanent magnetization （NRM） intensity after thermal demagnetization at 300°C normalized by low-frequency magnetic susceptibility （NRM 300 /χ）. The results show that the RPI record from the Baoji section, where pedogenesis is quite weak, is compatible with the stacked PISO-1500 paleointensity record, suggesting that it might reflect the paleointensity variation of the geomagnetic field. The RPI record from the Xifeng section, where pedogenesis is rather strong, indicates a clear dissimilarity with the stacked PISO-1500 paleointensity record, implying that it does not reflect the paleointensity variation of the geomagnetic field. Our new results show that the NRM 300 /χ from the strongly pedogenetic paleosols does not completely eliminate the pedogenetic （climatic） influence, so it might be unsuitable for a reliable paleointensity study.

关键词： Chinese loess pedogenesis relative paleointensity rock magnetism geomagnetic field

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Discovery of Paleozoic rocks at northern margin of Sambagawa terrane,eastern Kyushu,Japan:Petrogenesis,U-Pb geochronology and its tectonic implication

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Geoscience Frontiers 2020年第4期11卷 1441-1459页

作者： Kenta Kawaguchi Yasutaka Hayasaka Tomoyuki Shibata masayuki Komatsu Kosuke Kimura Kaushik Das Department of Earth and Planetary Systems Science Graduate School of ScienceHiroshima University1-3-1 KagamiyamaHigashi-HiroshimaHiroshima739-8526Japan Hiroshima Institute of Plate Convergence Region Research 1-3-1 KagamiyamaHigashi-HiroshimaHiroshima739-8526Japan Ehime University 10-13 Dogo-HimataMatsuyamaEhime790-8577Japan

Ordovician diorite-quartz diorite mylonite(Saganoseki quartz diorite) was discovered in Sambagawa metamorphic terrane at the northern margin of Saganoseki Peninsula,Kyushu Island,*** LA-ICP-MS zircon U-Pb geochronology revealed that the intrusion age of Saganoseki quartz diorite was 473.3±3.6 *** rocks show the volcanic arc affinity based on the trace element *** the basis of geochronological and geochemical results,Saganoseki quartz diorite is considered to be a member of the Early Paleozoic igneous rocks of the Kurosegawa tectonic *** quartz diorite is located just south of the Median Tectonic Line(MTL)and is in close contact with the pelitic and psammitic schist without any brittle shear zone.U-Pb ages of detrital zircon grains from two psammitic schists show the estimated sedimentation age of early Late Cretaceous,indicate that these psammitic schists are the member of Sambagawa metamorphic *** with these results and the mode of occurrence in the field,we argue that the Early Paleozoic igneous rocks of the Kurosegawa tectonic zone existed as an upper structural unit of the Sambagawa *** relationship is the key to reconstruct the Mesozoic tectonics of Japan as a part of East Asia,and its evolution through time.

关键词： Outer zone of southwest Japan Sambagawa metamorphic terrane Kurosegawa tectonic zone LA-ICP-MS zircon U-Pb age Saganoseki quartz diorite

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Identification of telomere maintenance gene variations related to lung adenocarcinoma risk by genome-wide association and whole genome sequencing analyses

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Cancer Communications 2024年第2期44卷 287-293页

作者： Kouya Shiraishi Atsushi Takahashi Yukihide Momozawa Yataro Daigo Syuzo Kaneko Takahisa Kawaguchi Hideo Kunitoh Shingo Matsumoto Hidehito Horinouchi Akiteru Goto Takayuki Honda Kimihiro Shimizu Masahiro Torasawa Daisuke Takayanagi Motonobu Saito Akira Saito Yuichiro Ohe Shun-ichi Watanabe Koichi Goto Masahiro Tsuboi Katsuya Tsuchihara Sadaaki Takata Tomomi Aoi Atsushi Takano Masashi Kobayashi Yohei Miyagi Kazumi Tanaka Hiroyuki Suzuki Daichi Maeda Takumi Yamaura Maiko Matsuda Yoko Shimada Takaaki Mizuno Hiromi Sakamoto Teruhiko Yoshida Yasushi Goto Tatsuya Yoshida Taiki Yamaji Makoto Sonobe Shinichi Toyooka Kazue Yoneda Katsuhiro Masago Fumihiro Tanaka Megumi Hara Nobuo Fuse Satoshi S.Nishizuka Noriko Motoi Norie Sawada Yuichiro Nishida Kazuki Kumada Kenji Takeuchi Kozo Tanno Yasushi Yatabe Kuniko Sunami Tomoyuki Hishida Yasunari Miyazaki Hidemi Ito Mitsuhiro Amemiya Hirohiko Totsuka Haruhiko Nakayama Tomoyuki Yokose Kazuyoshi Ishigaki Toshiteru Nagashima Yoichi Ohtaki Kazuhiro Imai Ken Takasawa Yoshihiro Minamiya Kazuma Kobayashi Kenichi Okubo Kenji Wakai Atsushi Shimizu masayuki Yamamoto Motoki Iwasaki Koichi Matsuda Johji Inazawa Yuichi Shiraishi Hiroyoshi Nishikawa Yoshinori Murakami Michiaki Kubo Fumihiko Matsuda Yoichiro Kamatani Ryuji Hamamoto Keitaro Matsuo Takashi Kohno Division of Genome Biology National Cancer Center Research InstituteTokyoJapan Department of Clinical Genomics National Cancer Center Research InstituteTokyoJapan Laboratory for Statistical Analysis Center for Integrative Medical SciencesRIKENYokohamaJapan Department of Genomic Medicine Research InstituteNational Cerebral and Cardiovascular CenterOsakaJapan Laboratory for Genotyping Development Center for Integrative Medical SciencesRIKENYokohamaJapan Center for Antibody and Vaccine Therapy Research HospitalInstitute of Medical ScienceThe University of TokyoTokyoJapan Department of Medical Oncology and Cancer Center and Center for Advanced Medicine against CancerShiga University of Medical ScienceOtsuJapan Division of Medical AI Research and Development National Cancer Center Research InstituteTokyoJapan Center for Genomic Medicine Graduate School of MedicineKyoto UniversityKyotoJapan Department of Medical Oncology Japanese Red Cross Medical CenterTokyoJapan Department of Thoracic Oncology National Cancer Center Hospital EastJapan Department of Thoracic Oncology National Cancer Center HospitalTokyoJapan Department of Cellular and Organ Pathology Graduate School of MedicineAkita UniversityAkitaJapan Department of Respiratory Medicine Tokyo Medical and Dental UniversityBunkyo-kuTokyoJapan Division of General Thoracic Surgery Department of SurgeryShinshu University School of MedicineMatsumotoNaganoJapan Department of General Surgical Science Division of General Thoracic SurgeryGunma University Graduate School of MedicineIntegrative Center of General SurgeryGunma University HospitalGunmaJapan Department of Gastrointestinal Tract Surgery Fukushima Medical University School of MedicineFukushimaJapan StaGen Co. LtdTokyoJapan Division of Thoracic Surgery National Cancer Center HospitalTokyoJapan Department of Thoracic Surgery National Cancer Center Hospital EastChibaJapan Division of Translational Informatics Exploratory Oncology Research and Clinical Trial Center(EPOC

Dear editor,Lung carcinoma is responsible for the highest fatal-ity rate among cancer-related deaths globally,with lung adenocarcinoma(LADC)emerging as the prevailing sub-type.

关键词： adenocarcinoma lung Lung

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Design and Implementation of NAREGI SuperScheduler Based on the OGSA Architecture

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Journal of Computer Science & Technology 2006年第4期21卷 521-528页

作者： Satoshi Matsuoka masayuki Hatanaka Yasumasa Nakano Yuji Iguchi Toshio Ohno Kazushige Saga Hidemoto Nakada Global Scientific Information and Computing Center Tokyo Institute of Technology 2-12-10okayama Meguro-ku Tokyo 152-8550 Japan Center for Grid Research and Development National Institute of Informatics 1-105 Kanda-Jinbocho Chiyoda-ku Tokyo 101-0051 Japan Linux Software Development Div. Server Systems Unit. Fujitsu Limited 130 Miyamoto Numazu-shi Shizuoka410-0396 Japan Grid Technology Research Center National Institute of Advanced Industrial Science and Technology 1-18-13 Sotokanda Chiyoda-ku Tokyo 101-0021 Japan

NAREGI is a 5-year Japanese National Grid Project during 2003--2007, whose chief aim is to develop a set of grid middleware to serve as a basis for future e-Science. NAREGI also aims to lead the way in standardization of grid middleware, based on the OGSA architecture. Its super-scheduler is based on the proposed OGSA-EMS Architecture, in that it becomes the first working implementation that implements the documented component relationships within the OGSA-EMS architecture document v.l.0. Through the efforts and experience in the design and implementation, it has been confirmed that the documented OGSA-EMS architecture is quite feasible, but will require significant amount of refinement and speed improvements to finalize its detailed specifications. The super-scheduler also supports co-allocation across multiple sites to support automated execution of grid-based MPIs that execute across machines. Such a resource allocation requires sophisticated interactions between the OGSA-EMS components not covered in the current OGSA-EMS architecture, some of which are non-trivial. Overall, job scheduling with OGSA-EMS has proven to not only work, but also that its job allocation and execution time is within reasonable bounds.

关键词： grid scheduling resource management open grid services architecture OGSA

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