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Effect of Particle Size on Mechanical Properties and Fracture Behaviors of Age-Hardening SiC/Al–Zn–Mg–Cu Composites

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Acta Metallurgica Sinica(English Letters) 2021年第10期34卷 1447-1459页

作者： Guonan ma Dong Wang Bolv Xiao zongyi ma Institute of Metal Research Chinese Academy of SciencesShenyang 110016China School of materials Science and Engineering University of Science and Technology of ChinaShenyang 110016China

15 vol.% SiC/Al-6.5Zn-2.8 Mg-1.7 Cu(wt%) composites with varying particle sizes(3.5, 7.0, 14 and 20 μm), i.e., C-3.5, C-7.0, C-14, and C-20, respectively, were fabricated by powder metallurgy(PM) method and subjected to microstructural examination. The effect of particle size on mechanical properties and fracture behaviors of the T6-treated composites was revealed and analyzed in detail. Element distribution and precipitates variations in the composites with varying particle sizes were emphatically considered. Results indicated that both tensile strength and plasticity of the T6-treated composites increased first and then decreased with particle size decreasing. The C-7.0 composite simultaneously exhibited the highest ultimate tensile strength(UTS) of 686 MPa and best elongation(El.) of 3.1%. The smaller-sized SiC particle would introduce more oxide impurities, which would react with the alloying element in the matrix to cause Mg segregation and depletion. According to strengthening mechanism analysis, the weakening of precipitation strengthening in the T6-treated C-3.5 composite was the main cause of the lower tensile strength. Additionally, the larger SiC particle, the more likely to fracture, especially in the composites with high yield strength. For the T6-treated C-20 composites, more than 75% SiC particles were broken up, resulting in the lowest plasticity. As decreasing particle size, the fracture behaviors of the T6-treated composites would change from particle fracture to matrix alloy fracture gradually.

关键词： Metal matrix composites Mechanical properties Particle size Fracture behaviors Strengthening mechanisms

颗粒增强铝基复合材料热等静压近净成形有限元模拟

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精密成形工程 2024年第4期16卷 1-9页

作者：冯效铭张峻凡王东肖伯律马宗义中国科学院金属研究所师昌绪先进材料创新中心沈阳110016 中国科学技术大学材料科学与工程学院沈阳110016

目的建立可靠的模拟方法,以更高效地预测颗粒增强铝基复合材料(PRAMC)粉末热等静压中的形状变化和不同部位致密度的差异,解决传统实验试错方法适用性差且费时费力的问题,满足批量应用的需求。方法以45%(体积分数)SiCp/6092Al复合材料为... 详细信息

目的建立可靠的模拟方法,以更高效地预测颗粒增强铝基复合材料(PRAMC)粉末热等静压中的形状变化和不同部位致密度的差异,解决传统实验试错方法适用性差且费时费力的问题,满足批量应用的需求。方法以45%(体积分数)SiCp/6092Al复合材料为研究对象,构建了能预测粉末热等静压成形过程的有限元模型。使用Gurson-Tvergard-Needleman(GTN)模型作为粉末本构模型,建立了粉末尺度的代表性体积单元(RVE)对GTN模型进行修正。结果通过对比GTN模型计算结果与实验结果,发现修正后的GTN模型能更准确地预测模型的最终变形尺寸,与修正前相比,相对误差降低了1.6%~2.9%。使用修正后的GTN模型对杯形回转体零件的热等静压成形过程进行预测,最终形状的计算结果与实验结果的相对误差仅为0.2%~3.1%,致密度分布的相对误差在0.5%以内。在探究包套厚度对热等静压过程的影响时发现,随着包套厚度的增大,热等静压过程中的屏蔽作用增强,内部粉体致密度下降。结论为PRAMC热等静压近终形制备的形状和致密度控制问题提供了有限元预测工具,辅助优化了热等静压工艺和包套设计,降低了颗粒增强铝基复合材料热等静压近净成形过程开发的试错成本。

关键词：颗粒增强铝基复合材料粉末冶金体积代表单元 GTN模型近净成形

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Fabrication of high strength carbon nanotube/7055Al composite by powder metallurgy combined with subsequent hot extrusion

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Science China(Technological Sciences) 2021年第5期64卷 1081-1091页

作者： ma Kai LIU ZhenYu ZHANG XingXing XIAO BoLv ma zongyi Shi-changxu Innovation Center for Advanced materials Institute of Metal ResearchChinese Academy of SciencesShenyang 110016China School of materials Science and Engineering University of Science and Technology of ChinaShenyang 110016China

Bimodal carbon nanotube reinforced 7055Al(CNT/7055Al) composites containing coarse grain bands and ultra-fine grain zones were fabricated by high energy ball milling, vacuum hot pressing followed by hot extrusion. The effect of extrusion temperature varied from 320℃ to 420℃ on the microstructure evolution and tensile properties were investigated. Microstructure observation indicates that the elongated coarse grain bands aligned along the extrusion direction after extrusion. The width of the coarse grain bands increased, and the length of the coarse grain bands increased firstly and then decreased with the increase of extrusion temperature. The grain size of the ultra-fine grain zones changed little after hot extrusion, but the ultra-fine grains coarsened after subsequent heat treatment, especially for the composite extruded at low temperature of 320℃. By observing the CNT distribution, it was found that the higher temperature extrusion was beneficial to the CNT orientation along the extrusion ***, a precipitated free zone formed at the boundary between the coarse grain band and the ultra-fine grain zone as the composite extruded at high temperature of 420℃. As the result of the comprehensive influence of the above microstructure, the tensile strength of the composite extruded at moderate temperature of 370℃ reached the highest of 826 MPa.

关键词： carbon nanotube aluminum matrix composite hot extrusion bimodal mechanical property

EFFECT　OF　PARTICULATE　SIZE　AND　CONTENT　ON　STRENGTH　OF　SiC_p／2024Al　COMPOSITE　AND　ITS　RELATIONSHIP　WITH　T6－TREATMENT

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中国有色金属学会会刊：英文版 1995年第3期5卷 127-132页

作者： ma, zongyi Liang, Yanan Lu, Yuxiong Bi, Jing Chinese Acad of Sciences Shenyang China

ＥＦＦＥＣＴＯＦＰＡＲＴＩＣＵＬＡＴＥＳＩＺＥＡＮＤＣＯＮＴＥＮＴＯＮＳＴＲＥＮＧＴＨＯＦＳｉＣ_ｐ／２０２４ＡｌＣＯＭＰＯＳＩＴＥＡＮＤＩＴＳＲＥＬＡＴＩＯＮＳＨＩＰＷＩＴＨＴ６－ＴＲＥＡＴＭＥＮＴ￥Ｍａ，Ｚｏｎｇ... 详细信息

ＥＦＦＥＣＴＯＦＰＡＲＴＩＣＵＬＡＴＥＳＩＺＥＡＮＤＣＯＮＴＥＮＴＯＮＳＴＲＥＮＧＴＨＯＦＳｉＣ_ｐ／２０２４ＡｌＣＯＭＰＯＳＩＴＥＡＮＤＩＴＳＲＥＬＡＴＩＯＮＳＨＩＰＷＩＴＨＴ６－ＴＲＥＡＴＭＥＮＴ￥Ｍａ，Ｚｏｎｇｙｉ；Ｌｉａｎｇ，Ｙａｎａｎ；Ｌｕ?..

关键词： composite particulate aluminum T6-treatment strength

Compressive Creep Behavior of TiC/AZ91D magnesium-matrix Composites with Interpenetrating Networks

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Journal of materials Science & Technology 2007年第2期23卷 207-212页

作者： Liqing CHEN Jinhua GUO Baohai YU zongyi ma The State Key Laboratory of Rolling and Automation Northeastern University Shenyang 110004 China Institute of Metal Research Chinese Academy of Sciences Shenyang 110016 China

The 42.1 vol. pct TiC/AZ91D magnesium-matrix composites with interpenetrating networks were fabricated by in-situ reactive infiltration process. The compressive creep behavior of as-synthesized composites was investigated at temperature ranging from 673 to 723 K under loads of 95-108 MPa. For a comparative purpose,the creep behavior of the monolithic matrix alloy AZ91D was also conducted under loads of 15-55 MPa at 548-598 K. The creep mechanisms were theoretically analyzed based on the power-law relation. The results showed that the creep rates of both TiC/AZ91D composites and AZ91D alloy increase with increasing the temperature and load. The TiC/AZ91D composites possess superior creep resistance as compared with the AZ91D alloy. At deformation temperature below 573 K, the stress exponent n of AZ91D alloy approaches theoretical value of 5, which suggests that the creep process is controlled by dislocation climb. At 598 K, the stress exponentof AZ91D is close to 3, in which viscous non-basal slip deformation plays a key role in the process of creep deformation. However, the case differs from that of AZ91D alloy when the stress exponent n of TiC/AZ91D composites exceeds 9, which shows that there exists threshold stress in the creep process of the composites, similar to other types of composites. The average activation energies for the creep of the AZ91D alloy and TiC/AZ91D composites were calculated to be 144 and 152 k J/mol, respectively. The existence of threshold stress in the creep process of the composites leads to an increase in activation energy for creep.

关键词： magnesium-matrix composites TiC/AZ91D Interpenetrating networks In-situ reactive infiltration Creep

EFFECT OF maTRIX STRENGTHENING ON SLIDING WEAR PROPERTIES OF SiCp/2024Al COMPOSITES

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中国有色金属学会会刊：英文版 1998年第4期8卷 25-30页

作者： ma, zongyi Liang, Yan'an Lu, Yuxiong Bi, Jing Inst of Metal Research Chinese Acad of Sciences Shenyang China

ＩＮＴＲＯＤＵＣＴＩＯＮＴｈｅｃｅｒａｍｉｃｐａｒｔｉｃｕｌａｔｅｓｒｅｉｎｆｏｒｃｅｄａｌｕｍｉｎｕｍａｌｏｙｃｏｍｐｏｓｉｔｅｓｅｘｈｉｂｉｔｈｉｇｈｓｐｅｃｉｆｉｃｍｏｄｕｌｕｓａｎｄｓｔｒｅｎｇｔｈ，ａｌｓ... 详细信息

ＩＮＴＲＯＤＵＣＴＩＯＮＴｈｅｃｅｒａｍｉｃｐａｒｔｉｃｕｌａｔｅｓｒｅｉｎｆｏｒｃｅｄａｌｕｍｉｎｕｍａｌｏｙｃｏｍｐｏｓｉｔｅｓｅｘｈｉｂｉｔｈｉｇｈｓｐｅｃｉｆｉｃｍｏｄｕｌｕｓａｎｄｓｔｒｅｎｇｔｈ，ａｌｓｏｇｅｔａｓｉｇｎｉｆｉｃａｎｔｉ...

关键词： composite aluminum SiC wear particulate

双模CNT/Al复合材料变形过程的代表性体积单元模拟

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精密成形工程 2024年第4期16卷 71-78页

作者：石礼硕朱智吴迪张峻凡肖伯律马宗义沈阳航空航天大学材料科学与工程学院沈阳110136 中国科学院金属研究所师昌绪先进材料创新中心沈阳110016

目的研究双模CNT/Al复合材料在塑性加工过程中的微观结构演变行为。方法通过ABAQUS/Python二次开发,对双模CNT/Al复合材料代表性体积单元(RVE)进行参数化建模,并基于显式动力学求解器和欧拉-拉格朗日耦合技术,对双模CNT/Al复合材料RVE... 详细信息

目的研究双模CNT/Al复合材料在塑性加工过程中的微观结构演变行为。方法通过ABAQUS/Python二次开发,对双模CNT/Al复合材料代表性体积单元(RVE)进行参数化建模,并基于显式动力学求解器和欧拉-拉格朗日耦合技术,对双模CNT/Al复合材料RVE模型的单向压缩过程和挤压过程进行数值模拟分析。结果单向压缩模拟结果显示,结构心部异质区两侧的等效塑性应变较大,结构边缘基体区域的等效塑性应变相对较小;最大等效应力位于结构边角处的基体区域,而结构心部异质区的等效应力则相对较小。通过对异质区材料和形态的影响规律进行分析发现,当异质区为粗晶材料时,其变形后的形态更趋于扁平,而当异质区为细晶材料时,其变形后的形态更接近椭圆。通过挤压过程的模拟,实现了对变形过程中双模组织结构变化的分析,模拟结果显示,材料表面与模具贴合良好,异质区随变形的进行被不断拉长,部分异质区由于拉伸程度过大,甚至出现了分离的情况。结论提出的模拟方法为双模CNT/Al复合材料的挤压变形工艺设计和变形后组织结构预测提供了有效手段。

关键词：双模CNT/Al复合材料 RVE自动化建模塑性变形数值模拟欧拉-拉格朗日耦合技术

基于代表性体积单元的双模铝基复合材料性能拟实研究

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精密成形工程 2024年第4期16卷 36-44页

作者：庞雨婷张峻凡王文广肖伯律马宗义辽宁石油化工大学机械工程学院沈阳113001 中国科学院金属研究所师昌绪先进材料创新中心沈阳110016

目的研究双模铝基复合材料连续区(Continuous Region,CR)和非连续区(Discontinuous Region,DR)力学性能对材料整体力学性能的影响规律,以深入了解双模铝基复合材料的强韧化机理。方法基于Abaqus模拟软件,以双模CNT/Al为研究对象,建立了... 详细信息

目的研究双模铝基复合材料连续区(Continuous Region,CR)和非连续区(Discontinuous Region,DR)力学性能对材料整体力学性能的影响规律,以深入了解双模铝基复合材料的强韧化机理。方法基于Abaqus模拟软件,以双模CNT/Al为研究对象,建立了构型尺度的代表性体积单元(RVE)模型,采用GTN(Gurson-Tvergaard-Needleman)模型来描述双模CNT/Al中CR和DR的变形力学行为,通过定义力学性能参数来简化描述CR和DR复杂的力学性能。针对双模CNT/Al的CR和DR,分别设定力学性能参数HC和HD,并进行一系列的拉伸载荷模拟,研究HC和HD对双模复合材料整体力学性能的影响规律。通过与真实双模CNT/Al的力学性能进行对比,得到双模CNT/Al中CR和DR力学性能与均匀材料力学性能的差异,最后对双模CNT/Al在变形过程中的应力分布情况和断裂后的形貌进行分析。结果当HC小于4时,双模CNT/Al的抗拉强度随HD的增大而下降;当HC大于5时,双模CNT/Al的抗拉强度随HD的增大而增大;双模CNT/Al的屈服强度随着HD和HC的增大而增大,延伸率随着HD和HC的增大而降低。当HD或HC一定时,在HC=HD时,模型材料的延伸率最大。典型双模CNT/Al由“粗晶铝合金+CNT/超细晶Al复合材料”构成,与均匀结构的粗晶铝合金相比,其构型中粗晶铝合金的强度显著提升、塑韧性显著下降;与均匀结构的CNT/超细晶Al相比,其构型中的CNT/超细晶Al复合材料的强度小幅降低、塑韧性小幅提升。当HD大于HC时,裂纹优先在DR产生;当HD小于HC时,裂纹优先在CR区产生;当HD和HC接近时,裂纹产生的区域更加分散。结论建立了一种双模铝基复合材料的有限元模型,从数值上说明了双模CNT/Al复合材料微区与均匀材料的力学性能存在显著差异,为双模铝基复合材料的设计提供了参考。

关键词：铝基复合材料有限元模拟双模结构代表性体积单元 GTN模型

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Friction stir welding of carbon nanotubes reinforced Al-Cu-Mg alloy composite plates

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Journal of materials Science & Technology 2017年第9期33卷 1004-1008页

作者： Ke Zhao Zhenyu Liu Bolyu Xiao zongyi ma Shenyang National Laboratory for materials Science Institute of Metal ResearchChinese Academy of Sciences

Carbon nanotubes(CNTs) reinforced Al-Cu-Mg composite plates of 2.2 mm in thickness after extrusion and T4 treatment were joined by friction stir welding(FSW) and the joint efficiency reaches 87%. There was no precipitate in both heat-affected zone(HAZ) and nugget zone(NZ) as a medium rotation rate of 800 rpm and a relative high travel speed of 100 mm min-1were used. In the NZ, FSW disarranged the alignment of CNTs to random orientation and dispersed CNT uniformly. The orientation of CNTs perpendicular to the tensile direction and the possible dissolution of solute clusters made the HAZ become the weakest zone in the joint leading to the failure in the HAZ.

关键词： Carbon nanotubes Metal matrix composites Friction stir welding