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Tungsten 2024年第2期6卷 422-427页

作者： xiu-li Wang Yong-Zhen Chen Zhi-Han Chang Yu-Chun lin Jing-Yi Ma College of Chemistry and Materials Engineering Bohai UniversityJinzhou 121013China Professional Technology Innovation Center of liaoning Province for Conversion Materials of Solar Cell Jinzhou 121013China

By employing a new semi-rigid pyrazole-amide-derived bis(pyridyl)ligand[N,N'-bis(4-picolylamine)-1-hydropyrazole(4-dpap)],a new homopolymolybdate-based two-dimensional(2D)plate-like complex[Co(4-dpap)(H_(2)O)(β-Mo_(8)O_(2)6)1/2](1)has been prepared under solvothermal condition and structurally ***β-Mo_(8)anions are fi xed between the 2D metal–organic networks[Co(4-dpap)(H_(2)O)]n 2n+via hydrogen-bonding *** 1 possesses satisfactory specifi c capacitance of 1512.4 F·g^(−1)(current density:1 A·g^(−1))and good cycling stability(90.8%after 1000 cycles).Moreover,1 represents a promising amperometric sensor for measurement of Cr(Ⅵ)with low detection limit(0.042μmol·L^(−1))and high *** insertion ofβ-Mo_(8)anions between the unique 2D metal−organic networks improves the active area of polyoxometalates,which further promotes electrochemical performance.

关键词： Homopolymolybdate Metal–organic network Pyrazole-amide-derived bis(pyridyl)ligand Supercapacitor Electrochemical sensor

Multistate transition and coupled solid-liquid modeling of motion process of long-runout landslide

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Journal of Rock Mechanics and Geotechnical Engineering 2024年第7期16卷 2694-2714页

作者： Yang Gao Yueping Yin bin li Han Zhang Weile Wu Haoyuan Gao Institute of Geomechanics Chinese Academy of Geological SciencesChina Geological SurveyBeijing100081China Key Laboratory of Active Tectonics and Geological Safety Ministry of Natural ResourcesBeijing100081China China Institute of Geological Environment Monitoring China Geological SurveyBeijing100081China School of Geological Engineering and Geomatics Chang’an UniversityXi’an710054China

The recognition,repetition and prediction of the post-failure motion process of long-runout landslides are key scientific problems in the prevention and mitigation of geological *** this study,a new numerical method involving LPF3D based on a multialgorithm and multiconstitutive model was proposed to simulate long-runout landslides with high precision and *** following results were obtained:(a)The motion process of landslides showed a steric effect with mobility,including gradual disintegration and *** sliding mass can be divided into three states(dense,dilute and ultradilute)in the motion process,which can be solved by three dynamic regimes(friction,collision,and inertial);(b)Coupling simulation between the solid grain and liquid phases was achieved,focusing on drag force influences;(c)Different algorithms and constitutive models were employed in phase-state *** volume fraction is an important indicator to distinguish different state types and solid‒liquid *** flume experimental results were favorably validated against long-runout landslide case data;and(d)In this method,matched dynamic numerical modeling was developed to better capture the realistic motion process of long-runout landslides,and the advantages of continuum media and discrete media were combined to improve the computational accuracy and *** new method can reflect the realistic physical and mechanical processes in long-runout landslide motion and provide a suitable method for risk assessment and pre-failure prediction.

关键词： Long-runout landslide Multistate transition Mixed solid‒liquid flow Post-failure process Numerical simulation

Visual and portable detection of metronidazole realized by metal-organic framework flexible sensor and smartphone scanning

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Chinese Chemical Letters 2024年第10期35卷 500-504页

作者： Xiangshuai li Jian Zhao li Luo Zhuohao Jiao Ying Shi Shengli Hou* bin Zhao Department of Chemistry Key Laboratory of Advanced Energy Materials ChemistryRenewable Energy Conversion and Storage Center(RECAST)Nankai UniversityTianjin 300071China

Metronidazole(MNZ)is a type of antibiotic that can help people and animals cure bacterial in fections,however,abuse of MNZ has posed a threat to human ***,portable and vi sual detection of MNZ is meaningful for food safety and rational administration of drugs,bu full of ***,a porous three-dimensional Tb-based metal-organic framework(MOF{(CH_(3))_(2)NH_(2)·[Tb_(5)(TDA)_(8)(H_(2)O)_(2)]·6DMF·2C_(2)H_(5)OH}_n(TDA-Tb)with good solvent and p H stabilities was pre pared,and the framework possesses one-dimensional channels with a diameter of 12 A along the c-axis Experiment results suggest that the synthesized TDA-Tb can selectively and sensitively detect MNZ in water,and the limit of detection(LOD)is as low as 4.1×10^(-7)mol/***,a flexible sensor TDA Tb-M was also constructed by incorporating TDA-Tb into membrane materials for convenient *** the TDA-Tb-M firstly realized portable and visual detection of MNZ through smartphone scanning,which may inspire more probes with wide application ranges.

关键词： Metal-organic framework Lanthanide Luminescence Antibiotic Sensor

Rock physical characteristics of deep dolomite under complex geological conditions: A case study of 4th Member of Sinian Dengying Formation in the Sichuan Basin, China

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Petroleum Science 2024年第4期21卷 2370-2382页

作者： Chuang li Shu-Xin Pan Hong-bin Wang Ji-Xin Deng Jian-Guo Zhao Zhi li Yu Zhang Northwest Branch of Research Institute of Petroleum Exploration & Development Department of Geophysics and Exploration College of Geophysics Chengdu University of Technology State Key Laboratory of Petroleum Resources and Engineering China University of Petroleum (Beijing)

The deep-ultra deep carbonate reservoir in China, commonly subjected to modification of multi-stage diagenesis, has extremely high heterogeneity. Conventional rock physics analysis cannot accurately identify the elastic responses of reservoir. Here, the rock physics properties of the dolomite from the 4th Member of the Sinian Dengying Formation are experimentally measured, and the change law of rock physics characteristics is investigated within the framework of the diagenetic processes by the analysis of the elastic and petrologic characteristics, pore structure, and sedimentary environments. The results show that the differentiated diagenesis results in different pore structure characteristics and microtexture characteristics of the rock. The microbial dolomite of the algal mound-grain beach facies is subjected to the contemporaneous microbial dolomitization and seepage-reflux dolomitization, penecontemporaneous selective dissolution, burial dolomitization, and hydrothermal dolomitization. The resultant crystalline dolomite is found with one main type of the dolomite crystal contact boundaries,and the dissolution pore is extensive development. The siliceous, muddy, and limy dolomite of the interbeach sea environment mainly experiences the weak capillary concentration dolomitization, intensive mechanical compaction-induced densification, and burial dolomitization. Such crystalline dolomite is observed with four types of contact boundaries, namely the dolomite contact, clay contact, quartz contact, and calcite contact boundaries, and porosity mostly attributed to residual primary inter-granular or crystalline pores. The samples with the same crystal boundary condition have consistent correlations between the compressional-and shear-wave velocities, and between the compressional-wave velocity and the velocity ratio. Additionally, the variation of the acoustic velocity with effective pressure and the intensity of pore-scale fluid-related dispersion are controlled by t

关键词： Deep-ultra deep carbonate reservoirs Rock physics properties Dolomite Seismic elastic properties Micro-crack Pore structure types

Dynamic Analysis of a 10 MW Floating Offshore Wind Turbine Considering the Tower and Platform Flexibility

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Journal of Ocean University of China 2024年第2期23卷 358-370页

作者： GAO Shan ZHANG lixian SHI Wei WANG Wenhua WANG bin li Xin Key Laboratory of Far-Shore Wind Power Technology of Zhejiang Province Hangzhou 311122China State Key Laboratory of Coastal and Offshore Engineering Deepwater Engineering Research CenterDalian University of TechnologyDalian 116024China Powerchina Huadong Engineering Corporation limited Hangzhou 311122China Faculty of Infrastructure Engineering Dalian University of TechnologyDalian 116024China Ningbo Institute of Dalian University of Technology Ningbo 315000China

Recently,semisubmersible floating offshore wind turbine technologies have received considerable *** the coupled simulation of semisubmersible floating offshore wind energy,the platform is usually considered a rigid model,which could affect the calculation accuracy of the dynamic *** dynamic responses of a TripleSpar floating offshore wind turbine equipped with a 10 MW offshore wind turbine are discussed *** simulation of a floating offshore wind turbine under regular waves,white noise waves,and combined wind-wave conditions is *** effects of the tower and platform flexibility on the motion and force responses of the TripleSpar semisubmersible floating offshore wind turbine are *** results show that the flexibility of the tower and platform can influence the dynamic responses of a TripleSpar semisubmersible floating offshore wind *** the flexibility of the tower and platform,the tower and platform pitch motions markedly increased compared with the fully rigid ***,the force responses,particularly for tower base loads,are considerably influenced by the flexibility of the tower and ***,the flexibility of the tower and platform for the coupled simulation of floating offshore wind turbines must be appropriately examined.

关键词： floating offshore wind turbine TripleSpar semisubmersible platform rigidity and flexibility platform coupled simulation

STGNN-LMR:A Spatial–Temporal Graph Neural Network Approach Based on sEMG Lower limb Motion Recognition

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Journal of Bionic Engineering 2024年第1期21卷 256-269页

作者： Weifan Mao bin Ma Zhao li Jianxing Zhang Yizhou Lu Zhuting Yu Feng Zhang Shanghai Advanced Research Institute Chinese Academy of SciencesShanghai 201210China University of Chinese Academy of Sciences Beijing 101408China University of Science and Technology of China Hefei 230026China Shanghai Zhongyan Jiuyi Technology Co. Ltd.Shanghai 201821China Academy of Military Science Bejing 100091China

Lower limb motion recognition techniques commonly employ Surface Electromyographic Signal(sEMG)as input and apply a machine learning classifier or Back Propagation Neural Network(BPNN)for ***,this artificial feature engineering technique is not generalizable to similar tasks and is heavily reliant on the researcher’s subject *** contrast,neural networks such as Convolutional Neural Network(CNN)and Long Short-term Memory Neural Network(LSTM)can automatically extract features,providing a more generalized and adaptable approach to lower limb motion *** this approach overcomes the limitations of human feature engineering,it may ignore the potential correlation among the sEMG *** paper proposes a spatial–temporal graph neural network model,STGNN-LMR,designed to address the problem of recognizing lower limb motion from multi-channel ***-LMR transforms multi-channel sEMG into a graph structure and uses graph learning to model spatial–temporal *** 8-channel sEMG dataset is constructed for the experimental stage,and the results show that the STGNN-LMR model achieves a recognition accuracy of 99.71%.Moreover,this paper simulates two unexpected scenarios,including sEMG sensors affected by sweat noise and sudden failure,and evaluates the testing results using hypothesis *** to the experimental results,the STGNN-LMR model exhibits a significant advantage over the control models in noise scenarios and failure *** experimental results confirm the effectiveness of the STGNN-LMR model for addressing the challenges associated with sEMG-based lower limb motion recognition in practical scenarios.

关键词： Lower limb motion recognition Exoskeleton sEMG.Graph neural network Noise Sensor failure

Dynamic Effect of Landslides Triggered by Earthquake:A Case Study in Moxi Town of Luding County,China

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Journal of Earth Science 2024年第1期35卷 221-234页

作者： Hongfu Zhou Fei Ye Wenxi Fu bin liu Tian Fang Rui li Chengdu Center China Geological SurveyChengdu 610081China State Key Laboratory of Hydraulics and Mountain Rivers Protection Sichuan UniversityChengdu 610065China Sichuan Geological Survey Chengdu610081China Shandong University of Science and Technology Qingdao 266590China

The dynamic effect is a very important issue widely debated by scholars when studying the genetic and disaster-causing mechanisms of earthquake-triggered ***,the dynamic effect mechanism and phenomena of earthquake-triggered landslides were summarized in this ***,the primary types of dynamic effects were further used to interpret the Mogangling landslide in Moxi Town of Luding County,China.A field investigation,remote sensing,numerical calculation and theoretical analysis were carried out to illustrate the failure mechanism of slope rock masses affected by *** interaction between seismic waves and slope rock masses and the induced dynamic effect of slope rock masses were primarily accounted for in the *** slope topography,rock mass weathering and unloading characteristics,river erosion,regional seismogenic structure,and rock mass structure characteristics were also *** results showed that the formation of the Mogangling landslide was mainly related to the high amplification effect of seismic acceleration and back slope effects,interface dynamic stress effects,and double-sided slope effects of seismic waves caused by the catastrophic Ms 7.75 Moxi Earthquake in *** principles for the site and route selection of large-scale infrastructure in the planning stage and the scientific prevention of seismic geological disasters were proposed on the basis of the dynamic effect of earthquake-induced landslides.

关键词： dynamic effect coupling of endogenic and exogenic processes landslides earthquakes disaster prevention

Data Quality Control Method of a New Drifting Observation Technology Named Drifting Air-Sea Interface Buoy

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Journal of Ocean University of China 2024年第1期23卷 11-22页

作者： li Shuo WANG bin DENG Zeng’an WU Baoqin ZHU Xiande CHEN Zhaohui National Ocean Technology Center Tianjin 300112China School of Marine Science and Technology Tianjin UniversityTianjin 300072China Key Laboratory of Ocean Observation Technology Ministry of Natural ResourcesTianjin 300112China People’s liberation Army 92859 Tianjin 300061China Physical Oceanography Laboratory Ocean University of ChinaQingdao 266100China

An integral quality control(QC)procedure that integrates various QC methods and considers the design indexes and operational status of the instruments for the observations of drifting air-sea interface buoy was developed in the order of basic in-spection followed by targeted *** innovative method of combining a moving Hampel filter and local anomaly detection com-plies with statistical laws and physical processes,which guarantees the QC performance of meteorological *** sets of observation data were used to verify the applicability and effectiveness of the QC procedure,and the effect was evaluated using the observations of the Kuroshio Extension Observatory buoy as the *** results showed that the outliers in the time series can be correctly identified and processed,and the quality of data improved *** linear correlation between the quality-controlled observations and the reference increased,and the difference *** correlation coefficient of wind speed before and after QC increased from 0.77 to 0.82,and the maximum absolute error decreased by approximately 2.8ms^(-1).In addition,air pressure and relative humidity were optimized by 10^(-3)–10^(-2) orders of *** the sea surface temperature,the weight of coefficients of the continuity test algorithm was optimized based on the sea area of data acquisition,which effectively expanded the applicability of the algorithm.

关键词： drifting air-sea interface buoy quality control oceanic variables meteorological variables continuity test

Cerium refinement of grains and primary carbides during solidification of Cr_(4)Mo_(4)V bearing steel

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Journal of Rare Earths 2024年第4期42卷 783-792页

作者： Weifeng liu Jianqiang Wang Mingyue Sun bin Xu Jiahao Yao Qunbo Fan Dianzhong li Chongqing Innovation Center Beijing Institute of TechnologyChongqing401135China Shenyang National Laboratory for Materials Science Institute of Metal ResearchChinese Academy of SciencesShenyang110016China

The effect of cerium(Ce)on the solidification microstructure of Cr_(4)Mo_(4)V bearing steel was investigated via a combined experimental and theoretical *** a trace amount(0.056 wt%)of Ce addition,the coarse columnar grains in as-cast microstructure transform into equiaxed ones,and the average diameter is reduced from 56 to 27μ*** network-like and bulky primary MC and M2C carbides at the interdendritic regions become disconnected and refined,and their volume percentage decreases from4.15 vol%to 2.1 vol%.Ce-inclusions acting as heterogeneous nucleation agents of prior-austenite grains and Ce atoms segregating at grain boundaries,both contribute to the refinement of *** calculations reveal that primary carbides are precipitated afterγ-austenite forms near the end of the solidification *** modification of primary carbides in size and amount is mainly attributed to the isolated remaining melt separated by refinedγ-austenite grains in which the nucleation of carbides is promoted,while the growth is restrained owing to the less segregation of alloying elements.

关键词： Cr_(4)Mo_(4)V bearing steel Rare Earths Grains Primary carbides Refinement

Trench gate GaN IGBT with controlled hole injection efficiency

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The Journal of China Universities of Posts and Telecommunications 2024年第2期31卷 10-16页

作者： Huang Yi li Yueyue Gao Sheng Wang Qi liu bin Han Genquan School of Optoelectronic Engineering Chongqing University of Posts and TelecommunicationsChongqing 400065China School of Electronic Science and Engineering Nanjing UniversityNanjing 210008China School of Microelectronics Xidian UniversityXi’an 710126China

In this paper,a novel trench gate gallium nitride(GaN)insulated gate bipolar transistor(GaN IGBT),in which the collector is divided into multiple regions to control the hole injection efficiency,is designed and theoretically *** incorporation of a P+/P-multi-region alternating structure in the collector region mitigates hole injection within the collector *** the device is in forward conduction,the conductivity modulation effect results in a reduced storage of carriers in the drift *** a result,the number of carriers requiring extraction during device turn-off is minimized,leading to a faster turn-off *** results illustrate that the GaN IGBT with controlled hole injection efficiency(CEH GaN IGBT)exhibits markedly enhanced performance compared to conventional GaN IGBT,showing a remarkable 42.2%reduction in turn-off time and a notable 28.5%decrease in turn-off loss.

关键词： gallium nitride insulated gate bipolar transistor(GaN IGBT) hole injection trench gate turn-off loss