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In vivo and in vitro study of resorbable magnesium wires for medical implants:Mg purity,surface quality,Zn alloying and polymer coating

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journal of Magnesium and Alloys 2024年第6期12卷 2472-2488页

作者： K.Tesar j.luňácková M.jex M.Žaloudková R.Vrbová M.Bartoš P.Klein L.Vištejnová j.Dušková E.Filová Z.Sucharda M.Steinerová S.Habr K.Balík A.Singh Department of Materials Faculty of Nuclear Sciences and Physical EngineeringCzech Technical University in PragueTrojanova 13Prague 12000Czech Republic Institute of Physics Czech Academy of SciencesNa Slovance 2Prague 18221Czech Republic Institute of Dental Medicine First Faculty of MedicineCharles University and General University Hospital in PragueKaterinská32Prague 12801Czech Republic Department of Physics Faculty of Nuclear Sciences and Physical EngineeringCzech Technical University in PragueBrehová7Prague 11519Czech Republic Department of Composites and Carbon Materials Institute of Rock Structure and MechanicsCzech Academy of SciencesV Holešovickách 41Prague 18209Czech Republic Institute of Anatomy First Faculty of MedicineCharles UniversityU Nemocnice 3Prague 12800Czech Republic Biomedical Center Faculty of Medicine in PilsenCharles UniversityAlej Svobody 76Pilsen 32300Czech Republic Department of Pathological Physiology Faculty of Medicine in PilsenCharles UniversityAlej Svobody 7632300 PilsenCzech Republic Department of Histology and Embryology Faculty of Medicine in PilsenCharles UniversityAlej Svobody 7632300 PilsenCzech Republic Institute of Pathology First Faculty of MedicineCharles University and General University Hospital in PragueStudnickova 2Prague 12800Czech Republic Department of Biomaterials and Tissue Engineering Institute of PhysiologyCzech Academy of SciencesVidenska 1083Prague 14200Czech Republic Research Center for Structural Materials National Institute for Materials Science1-2-1 SengenTsukuba 305-0047Japan

Magnesium is an excellent material in terms of biocompatibility and its corrosion products can serve as an active source for new bone ***,localized corrosion and H_(2)generation limit the potential of Mg-based *** low-alloyed Mg-Zn wires can strongly reduce problems with large H_(2)bubbles and improve the mechanical properties considerably while maintaining excellent long-term *** pickling and a polymer coating can be effectively used to lower the rate of in vivo *** this work,microstructural,mechanical,and in vitro characterization of 250μm and 300μm extruded wires made from ultra-pure Mg,commercially pure Mg,Mg-0.15Zn,Mg-0.4Zn and Mg-1Zn was ***,Mg-0.4Zn wires together with a variant coated with a copolymer of L-lactide andε-caprolactone were tested in vivo on artificially damaged Wistar rat *** on the observed Mg-induced osteogenesis,polymer-coated Mg wires with a small addition of Zn are a perspective material for bone-support applications,such as cerclage and fixation wires.

关键词： Magnesium Resorbable Mg wire Mg-Zn implant degradation Biocompatibility study Zn grain boundary segregation

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Grating‐like anechoic layer for broadband underwater sound absorption

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International journal of Mechanical System Dynamics 2022年第3期2卷 265-277页

作者： Chenlei Yu Mingyu Duan Wei He Xin Chen Fengxian Xin Tian j.lu State Key Laboratory for Strength and Vibration of Mechanical Structures School of Aerospace EngineeringXi'an Jiaotong UniversityXi'anChina MOE Key Laboratory for Multifunctional Materials and Structures School of Aerospace EngineeringXi'an Jiaotong UniversityXi'anChina Department of Advanced Manufacturing and Robotics College of EngineeringPeking UniversityBeijingChina Xi'an Modern Chemistry Research Institute Xi'anChina State Key Laboratory for Mechanics and Control of Mechanical Structures College of Aerospace EngineeringNanjing University of Aeronautics and AstronauticsNanjingChina MIIT Key Laboratory of Multifunctional Lightweight Materials and Structures College of Aerospace EngineeringNanjing University of Aeronautics and AstronauticsNanjingChina

To address the challenging task of effective sound absorption in the low and broad frequency band for underwater structures,we propose a novel grating‐like anechoic layer by filling rubber blocks and an air backing layer into metallic *** metallic gratings are incorporated into the anechoic layer as a skeleton for enhanced viscoelastic dissipation by promoting shear deformation between rubber and metal *** introduction of an air backing layer releases the bottom constraint of the rubber,thus intensifying its deformation under acoustic *** on the homogenization method and the transfer matrix method,a theoretical model is developed to evaluate the sound absorption performance of the proposed anechoic layer,which is validated against finite element simulation *** is demonstrated that a sound absorption coefficient of the grating‐like anechoic layer of 0.8 can be achieved in the frequency range of 1294-10000 *** the importance of sound absorption at varying frequencies,the weighted average method is subsequently used to comprehensively evaluate the performance of the anechoic ***,with structural density taken into consideration,an integrated index is proposed to further evaluate the acoustic properties of the proposed anechoic ***,the backing conditions and the boundary conditions of finite‐size structures are *** results provide helpful theoretical guidance for designing novel acoustic metamaterials with broadband low‐frequency underwater sound absorption.

关键词： underwater sound absorption broadband transfer matrix method rubber coating

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Hardness-thermal stability synergy in nanograined Ni and Ni alloys:Superposition of nanotwin and low-energy columnar boundary

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journal of Materials Science & Technology 2023年第6期137卷 123-131页

作者： F.H.Duan Y.Lin Q.Li j.H.luan j.lu j.Pan Y.Li Shenyang National Laboratory for Materials Science Institute of Metal ResearchChinese Academy of SciencesShenyang 110016China Laboratory of Nanomaterials&Nanomechanics Department of Mechanical EngineeringCity University of Hong KongHong KongChina State Key Laboratory of Material Processing and Die&Mould Technology and School of Materials Science and Engineering Huazhong University of Science and TechnologyWuhan 430074China Department of Materials Science and Engineering City University of Hong KongHong KongChina Centre for Advanced Structural Materials Greater Bay Joint DivisionShenyang National Laboratory for Materials ScienceCity University of Hong Kong Shenzhen Research InstituteShenzhen 518057China City U-Shenzhen Futian Research Institute Shenzhen 518045China

Refining grains into nanoscale can significantly strengthen and harden metallic materials;however,nanograined metals generally exhibit low thermal stability,hindering their practical *** this work,we exploit the superposition of the contribution of nanotwins,low-angle grain boundaries,and microalloying to tailor superior combinations of high hardness and good thermal stability in Ni and Ni *** the nanotwinned Ni having a twin thickness of∼2.9 nm and grain size of 28 nm,it exhibits a hardness over 8.0 GPa and an onset coarsening temperature of 623 K,both of which are well above those of nanograined ***/Mo microalloying can further improve the onset coarsening temperature to 773 K without comprising *** analyses reveal that high hardness is achieved via strengthen-ing offered by extremely fine ***,the superior thermal stability is mainly ascribed to the low driving force for grain growth induced by the low-angle columnar boundary architecture and to the additional pinning effect on the migration of twin/columnar boundaries provided by minor Re/Mo *** present work not only reveals a family of nanotwinned metals possessing the combination of ultra-high hardness and high thermal stability but also provides a strategy for tailoring properties of metallic materials by pairing low-angle grain boundaries and twin boundaries.

关键词： Nanotwin Thermal stability Hardness Low-angle grain boundary Microalloying

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Delayed plasticity during spherical nanoindentation of an iron-chromium-aluminum alloy:Effect of ferric ion irradiation

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journal of Materials Science & Technology 2023年第36期167卷 228-236页

作者： Y.Zhang C.W.Li j.L.jiang j.F.Gu H.Wang Y.D.jia G.Wang X.G.An Q.Wang j.lu Institute of Materials Shanghai UniversityShanghai 200072China School of Materials Science and Engineering Shanghai Jiao Tong UniversityShanghai 200240China Department of Mechanical Engineering City University of Hong KongKowloonSARChina Science and Technology on Reactor Fuel and Materials Laboratory Nuclear Power Institute of ChinaChengdu 610041China Interdisciplinary Materials Research Center Institute for Advanced StudyChengdu UniversityChengdu610106China

Spherical nanoindentation of an iron-chromium-aluminum alloy was conducted to study the effect of ferric-ion(Fe 3+)irradiation on the time-dependent plasticity behavior in the surface layers of this *** was observed that the initiation of plasticity by the appearance of displacement burst or“pop-in”event occurred after a period of waiting time in the apparent elastic regime and that Fe^(3+)irradiation at 360°C and up to∼0.5 displacements per atom could make it happen under the lower applied loads but with a reduced *** the experimental data,an activation volume and activation energy were extracted for the delayed *** results show that Fe^(3+)-irradiation significantly reduced its acti-vation volume from∼3.05 b 3 to∼1.75 b 3(where b=Burgers vector),but slightly increased its activation energy from∼0.65 to∼0.71 *** the other hand,high-resolution scanning transmission electron mi-croscopy observations reveal that the irradiation at the elevated temperature created interstitial atom pair onto the(100)habit plane that can serve as the nucleation site of a100dislocation loop while elim-inating the pre-existing ***,it is indicated that heterogeneous nucleation of the dislocation loop was predominant in the delayed plasticity initiation of this alloy and that the nucleation of the interstitial-type dislocation loop was involved due to Fe^(3+)-irradiation.

关键词： Spherical nanoindentation Delayed plasticity FeCrAl alloy Fe^(3+)-irradiation

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Universality of quenching-partitioning-tempering local equilibrium model

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journal of Materials Science & Technology 2022年第29期124卷 116-120页

作者： j.Z.Zhang L.Y.Zeng X.W.Zuo j.F.Wan Y.H.Rong N.Min j.lu N.L.Chen Department of Mechanical Engineering City University of Hong KongGreater Bay Joint DivisionShenyang National Laboratory for Materials ScienceTat Chee AvenueKowloonHong KongChina Shanghai Key Laboratory of Materials Laser Processing and Modification School of Materials Science and EngineeringShanghai Jiao Tong UniversityShanghai 200240China Laboratory for Microstructures Shanghai UniversityShanghai 201900China CityU-Shenzhen Futian Research Institute Shenzhen 518045China

*** As typical 3rd generation advanced high strength steels(AHSSs),quenching and partitioning(Q&P)steel has attracted lots of attention for excellent performance in strength-ductility[1–5].With absorbing carbon partitioning as the core idea of Q&P process,quenching-partitioning-tempering(Q-P-T)process was proposed with emphasis on precipitation strengthening for better combination of strength and ductility[6–10].

关键词： tempering strength ductility

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帕金森病病人脑铁氧代谢的时空模式

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国际医学放射学杂志 2024年第4期 497-497页

作者： S.Yan j.lu Y.Li j.Cho S.Zhang W.Zhu 王笑男

摘要目的铁沉积和线粒体功能障碍与帕金森病（PD）的发生和发展密切相关。旨在提取深部灰质（DGM）的磁敏感值和氧摄取分数（OEF），探讨PD脑铁氧代谢的时空进展模

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PhaseⅠ/Ⅱtrial evaluating concurrent carbon-ion radiotherapy plus chemotherapy for salvage treatment of locally recurrent nasopharyngeal carcinoma

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Chinese journal of Cancer 2016年第12期35卷 743-753页

作者： Lin Kong jing Gao jiyi Hu Weixu Hu Xiyin Guan Rong lu jiade j.lu Department of Radiation Oncology Shanghai Proton and Heavy Ion CenterFudan University Shanghai Cancer HospitalShanghai 200321P.R.China. Department of Radiation Oncology Shanghai Proton and Heavy Ion CenterShanghai 200321P.R.China. Department of Outpatient Clinic Shanghai Proton and Heavy Ion CenterShanghai 200321P.R.China. Shanghai Proton and Heavy Ion Center 4365 Kangxin RoadPudongShanghai 201315P.R.China.

Background: After deinitive chemoradiotherapy for non-metastatic nasopharyngeal carcinoma(NPC), more than 10% of patients will experience a local recurrence. Salvage treatments present signiicant challenges for locally recurrent NPC. Surgery, stereotactic ablative body radiotherapy, and brachytherapy have been used to treat locally recurrent NPC. However, only patients with small-volume tumors can beneit from these treatments. Re-irradiation with X-ray—based intensity-modulated radiotherapy(IMXT) has been more widely used for salvage treatment of locally recurrent NPC with a large tumor burden, but over-irradiation to the surrounding normal tissues has been shown to cause frequent and severe toxicities. Furthermore, locally recurrent NPC represents a clinical entity that is more radioresistant than its primary counterpart. Due to the inherent physical advantages of heavy-particle therapy, precise dose delivery to the target volume(s), without exposing the surrounding organs at risk to extra doses, is highly feasible with carbon-ion radiotherapy(CIRT). In addition, CIRT is a high linear energy transfer(LET) radiation and provides an increased relative biological efectiveness compared with photon and proton radiotherapy. Our prior work showed that CIRT alone to 57.5 Gy E(gray equivalent), at 2.5 Gy E per daily fraction, was well tolerated in patients who were previously treated for NPC with a deinitive dose of IMXT. The short-term response rates at 3–6 months were also acceptable. However, no patients were treated with concurrent chemotherapy. Whether the addition of concurrent chemotherapy to CIRT can beneit locally recurrent NPC patients over CIRT alone has never been addressed. It is possible that the beneits of high-LET CIRT may make radiosensitizing chemotherapy unnecessary. We therefore implemented a phase I/II clinical trial to address these questions and present our methodology and *** and design: The maximal tolerated dose(MTD) of re-treatment usi

关键词： Recurrent nasopharyngeal cancer Carbon ion radiotherapy Re-irradiation Salvage therapy Chemotherapy

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Low-Temperature Nitriding by Means of SMAT

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材料热处理学报 2004年第5期25卷 301-306页

作者： W.P.Tong H.W.Zhang N.R.Tao Z.B.Wang j.lu K.lu ShenyangNationalLaboratoryforMaterialsScience InstituteofMetalResearchChineseAcademyofSciencesShenyang110016China LASMIS UniversityofTechnologyofTroyes10000TroyesFrance.

The microstructure in the surface layer of iron and steel samples can be refined at the nanometer scale by means of a surface mechanical attrition treatment (SMAT) that generates repetitive severe plastic deformation to the surface layer. The subsequent nitriding kinetics of the as-treated samples with the nanostructured surface layer is greatly enhanced so that the nitriding temperatures can be reduce to 300 - 400 °C regions. This enhanced processing method demonstrates both the technological significance of nanomaterials in advancing the traditional processing techniques, and provides a new approach for selective surface reactions in solids. This article reviews the present state of the art in this field. The microstructure and properties of SMAT samples nitrided will be summarized. Further considerations of the development and applications of this new technique will also be presented.

关键词：低温渗氮 SMAT 纳米结晶表面机械损耗

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The combined effects of grain and sample sizes on the mechanical properties and fracture modes of gold microwires

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journal of Materials Science & Technology 2019年第1期35卷 76-83页

作者： H.K.Yang K.Cao Y.Han M.Wen j.M.Guo Z.L.Tan j.lu Y.lu Hong Kong Branch of National Precious Metals Material Engineering Research Center City University of Hong Kong Department of Mechanical and Biomedical Engineering City University of Hong Kong State Key Laboratory of Advanced Technologies for Comprehensive Utilization of Platinum Metals Sino-platinum Metals Co.Ltd Center for Advanced Structural Materials City University of Hong Kong Shenzhen Research Institute

Hall-Petch relation was widely applied to evaluate the grain size effect on mechanical properties of metallic material. However, the sample size effect on the Hall-Petch relation was always ignored. In the present study, the mechanical test and microstructure observation were performed to investigate the combined effects of grain and sample sizes on the deformation behaviors of gold microwires. The polycrystalline gold microwires with diameter of 16 ?m were annealed at temperatures from 100°C to 600°C, leading to different ratios(t/d) of wire diameter(t) to grain size(d) from 0.9 to 16.7. When the t/d was lower than 10, the yield stress dropped fast and deviated from the Hall-Petch relation. The free-surface grains played key role in the yield stress softening, and the volume fraction of free-surface grains increased with the t/d decreasing. Furthermore, the effects of t/d on work-hardening behaviors and fracture modes were also studied. With t/d value decreasing from 17 to 3.4, the samples exhibited necking fracture and the dislocation pile-ups induced work-hardening stage was gradually *** the t/d value further decreasing(t/d lure, and the work-hardening capability lost. As the gold microwire for wire bonding is commonly applied in the packaging of integrated circuit chips, and the fabrication of microwire suffers multi-pass cold-drawing and annealing treatments to control the grain size. The present study could provide instructive suggestion for gold microwire fabrication and bonding processes.

关键词： Gold microwire Wire bonding Tensile testing Grain size Hall-Petch relationship

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Carbon ion radiotherapy boost in the treatment of glioblastoma:a randomized phase Ⅰ/Ⅲ clinical trial

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Cancer Communications 2019年第1期39卷 39-50页

作者： Lin Kong jing Gao jiyi Hu Rong lu jing Yang Xianxin Qiu Weixu Hu jiade j.lu Department of Radiation Oncology Shanghai Proton and Heavy Ion CenterFudan University Shanghai Cancer CenterShanghai 201321P.R.China Department of Radiation Oncology Shanghai Proton and Heavy Ion CenterPudong4365 Kangxin RoadShanghai 201321P.R.China

Background: Glioblastoma (GBM) is a highly virulent tumor of the central nervous system, with a median survival < 15 months. Clearly, an improvement in treatment outcomes is needed. However, the emergence of these mal... 详细信息

Background: Glioblastoma (GBM) is a highly virulent tumor of the central nervous system, with a median survival luoro-ethyl-tyrosine positron emission tomography [MET/FET PET] or magnetic resonance imaging [MRI] and detection of serologic immune markers). We hypothesize that the induction CIRT boost will result in a greater initial tumor-killing ability and prime the tumor microenvironment for enhanced immunologic tumor clearance, resulting in an expected 33% improvement in OS rates. Discussion: The prognosis of GBM remains grim. The mechanism underpin

关键词： Glioblastoma Anaplastic astrocytoma Carbon ion radiotherapy Proton radiotherapy Temozolomide Overall survival Progression-free survival Toxicity Serologic immune response O-6-methylguanine-DNA methyltransferase

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