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Long-term corrosion evolution associated with the structural heterogeneities of an Fe-based amorphous coating in H_(3)BO_(3)solution at various temperatures

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j.urnal of Materials Science & Technology 2023年第9期140卷 233-248页

作者： D.B.wang j.Wu j.P.Cui q.wang T.R.Li W.Emori S.D.Zhang j.q.wang Shenyang National Laboratory for Materials Science Institute of Metal ResearchCASShenyang110016China School of Materials Science and Engineering University of Science and Technology of ChinaShenyang110016China Key Laboratory of Biorheological Science and Technology Ministry of EducationCollege of BioengineeringChongqing UniversityChongqing400044China School of Materials Science and Engineering Sichuan University of Science and EngineeringZigong 643000SichuanChina

Understanding the long-term corrosion behavior of neutron absorber materials in H_(3)BO_(3)solution is crucial for the materials applications in spent fuel *** this paper,long-term corrosion evolution for 180 d in relation to the structural heterogeneities of an Fe-based amorphous coating(AMC)in H_(3)BO_(3)solution at various temperatures was systematically *** indicate that the coating corrosion could be divided into three distinct ***,the corrosion resistance increased owing to the thickening and composition evolution of the passive ***,the corrosion rate was kept almost constant in the second stage,which connected with the steady state of the passive ***,the corrosion resistance of coating reduced gradually owing to the initiation and penetration of local-ized ***,it was revealed that the localized corrosion was initiated at the relatively Cr-depleted amorphous matrix in the deep pores of the *** could be attributed to the synergy of Cr-depletion and occlusive effect in the deep pores during long-term *** the elevation of temperature,the localized corrosion was enhanced due to the accumulation of the H+in the pores to swiftly reach the critical conditions for passive film *** work provides insights into the long-term corrosion mechanism of Fe-based AMCs in H_(3)BO_(3)solution and offers meaningful contributions to the design of new corrosion resistant neutron absorbing coatings for spent fuel storage applications.

关键词： AMC Boric acid EIS Long-term corrosion Temperature

PARAMETRIC STUDY FOR THE PREPARATION OF ALIGNED SINGLE-WALLED CARBON NANOTUBES BY ANODE-ARC DISCHARGE METHOD

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Acta Metallurgica Sinica(English Letters) 2005年第3期18卷 261-268页

作者： j.F.Dai q.wang W.X.Li Z.q.Wei G.j.Xu StateKeyLaboratoryofNewNonferrousMetalMaterials DepartmentofPhysicsLanzhouUniversityofTechnologyLanzhou730050China StateKeyLaboratoryofNewNonferrousMetalMaterials InstituteofMaterialsLanzhouUniversityofTechnologyLanzhou730050China

Well aligned quasi-straight single-walled carbon nanotubes (SWCNTs) and straight SWCNTs bundle have been prepared in large scale by anode-arc vaporization of gr aphite with metallic catalysts. Various parameters such as the catalyst preparat ion, the kinds and pressure of the buffer gases, the quantity of anode-arc curre nt intensity, and the method of purification have been examined. The influence o f these parameters on the deposited carbon yield is reported, together with obse rvations of the produced material. Improvement in synthetic techniques has resul ted in the optimal conditions for the production of large quantities of high qua lity SWCNTs in our semi-continuous synthesis method. The formation of carbon nan otubes (CNTs) was studied briefly in this paper. Owing to the magnetic pinching effect of arc current, the CNTs arrange in parallel lines along the arc current direction.

关键词： carbon nanotubes anode-arc preparation catalyst

Homogeneous Plastic Flow of Fully Amorphous and Partially Crystallized Zr_(41.2)Ti_(13.8)Cu_(12.5)Ni_(10)Be_(22.5) Bulk Metallic Glass

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j.urnal of Materials Science & Technology 2003年第6期19卷 557-560页

作者： q.wang j.j.Blandin M.Suery B.Van de Moortele j.M.Pelletier GPM2 ENSPG D.U. B.P.46 38042 Grenoble France Institute of Materials Shanghai University Shanghai 200072 ChinaGPM2 ENSPG D.U. B.P.46 38042 Grenoble FranceGPM2 ENSPG D.U. B.P.46 38042 Grenoble FranceGEMPPM Bat. B. PascalINSA 69621 Villeurbanne Cedex FranceGEMPPM Bat. B. PascalINSA 69621 Villeurbanne Cedex France

The homogeneous plastic flow of fully amorphous and partially crystallized Zr(41.2)Ti(13.8)Cu(12.5)Ni(10)Be(22.5) bulk metallic glass (Vitl) has been investigated by compression tests at high temperatures in supercooled liquid region. Experimental results show that at sufficiently low strain rates, the supercooled liquid of the fully amorphous alloy reveals Newtonian flow with a linear relationship between the flow stress and strain rate. As the strain rate is increased, a transition from linear Newtonian to nonlinear flow is detected, which can be explained by the transition state theory. Over the entire strain rate interval investigated, however, only nonlinear flow is present in the partially crystallized alloy, and the flow stress for each strain rate is much higher. It is found that the strain rate-stress relationship for the partially crystaltized alloy at the given temperature of 646 K also obeys the sinh law derived from the transition state theory, similar to that of the initial homogeneous amorphous alloy. Thus, it is proposed that the flow behavior of the nanocrystalline/amorphous composite at 646 K is mainly controlled by the viscous flow of the remaining supercooled liquid.

关键词： Homogeneous plastic flow Zr41.2Ti13.8Cu12.5Ni10Be22.5 amorphous alloy,Partially crystallized amorphous alloy

Rational design of chemically complex metallic glasses by hybrid modeling guided machine learning

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npj.Computational Materials 2021年第1期7卷 1242-1251页

作者： Z.q.Zhou q.F.He X.D.Liu q.wang j.H.Luan C.T.Liu Y.Yang Department of Mechanical Engineering College of EngineeringCity University of Hong KongKowloonHong KongChina College of Mechatronics and Control Engineering Shenzhen UniversityShenzhenChina Laboratory for Structures Institute of Materials ScienceShanghai UniversityShanghaiChina Department of Materials Science and Engineering College of EngineeringCity University of Hong KongKowloonHong KongChina Department of Advanced Design and System Engineering College of EngineeringCity University of Hong KongChina

The compositional design of metallic glasses(MGs)is a long-standing issue in materials science and ***,traditional experimental approaches based on empirical rules are time consuming with a low *** this work,we successfully developed a hybrid machine learning(ML)model to address this fundamental issue based on a database containing~5000 different compositions of metallic glasses(either bulk or ribbon)reported since *** the prior works relying on empirical parameters for featurization of data,we designed modeling guided data descriptors in line with the recent theoretical models on amorphization in chemically complex alloys for the development of the hybrid classification-regression ML *** hybrid ML modeling was validated both numerically and *** importantly,it enabled the discovery of MGs(either bulk or ribbon)through the ML-aided deep search of a multitude of quaternary to scenery alloy *** computational framework herein established is expected to accelerate the design of MG compositions and expand their applications by probing the complex and multi-dimensional compositional space that has never been explored before.

关键词： alloy glasses metallic

Designing ultrastrong maraging stainless steels with improved uniform plastic strain via controlled precipitation of coherent nanoparticles

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j.urnal of Materials Science & Technology 2021年第34期93卷 60-70页

作者： Z.H.wang B.Niu q.wang C.Dong j.C.j.e T.M.wang T.G.Nieh Key Laboratory of Materials Modification by Laser Ion and Electron Beams(Ministry of Education)School of Materials Science and EngineeringDalian University of TechnologyDalian116024China Department of Materials Science and Engineering The University of TennesseeKnoxville37996TennesseeUSA

The development of ultrastrong maraging stainless steels(MSSs)is always in high ***,traditional high-strength MSSs generally exhibit early plastic instability with a low uniform strain since the precipitated nanoparticles are non-coherent with the body-centered-cubic(BCC)lath martensitic ***,we design a novel ultrahigh strength MSS(Fe-5.30 Cr-13.47 Ni-3.10 Al-1.22 Mo-0.50 W-0.23 Nb-0.03 C-0.005 B,wt.%)using a cluster formula approach.A fabulous microstructure consisting of a uniform distribution of high-density coherent B2-Ni Al nanoprecipitates(3-5 nm)in BCC martensitic matrix was successfully *** alloy has not only an exceedingly high ultimate tensile strength of 2.0 GPa,but also a decent uniform elongation of 4.2%-5.1%,which is almost triple of the value observed in existing *** present an in-depth discussion on the origins of ultrahigh strength and uniform plastic strain in the new alloy to validate our design strategy and further offer a new pathway to exploit highperformance MSSs.

关键词： Maraging stainless steel Ultrahigh strength Coherent precipitation Strengthening mechanisms Uniform deformation

PARTICLE SIZE AND MICROSTRUCTURE OF Ni NANOPOWDERS PREPARED BY ANODIC ARC PLASMA

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Acta Metallurgica Sinica(English Letters) 2005年第3期18卷 209-216页

作者： Z.q.Wei H.X.qiao j.F.Dai W.j.Feng q.wang P.X.Yan SchoolofSciences LanzhouUniversityofTechnologyLanzhou730050China CollegeofCivilEngineering LanzhouUniversityofTechnologyLanzhou730050China SchoolofPhysicalScienceandTechnology LanzhouUniversityLanzhou730000China

Pure Ni nanopowders were successfully prepared by the method of anodic arc disch arged plasma with homemade experimental apparatus. The particle size, mircostruc ture and morphology of the particles by this process were characterized via X-ra y powder diffraction (XRD), transmission electron microscopy (TEM) and the corre sponding selected area electron diffraction (SAED); The specific surface area an d pore parameters were investigated by multi-point full analysis of nitrogen ads orption-desorption isotherms at 77K by Brunauer- Emmett-Teller (BET) surface are a analyzer; The chemical composition were determined by X-ray energy dispersive spectrometry (XEDS) equipped in SEM and element analyze instrument. The experime nt results indicate that the samples by this method with high purity,the crystal structure of the particles is as same as the bulk material, is fcc structure, w ith average particle sizes about 47nm, ranging from 20 to 70nm, and distributed uniformly in spherical chain shapes, the specific surface areavis 14.23m2/g, po re volume of pore is 0.09cm3/g and average pore diameter is 23nm.

关键词： anodic arc plasma Ni nanopowder particle size structure composition.

Delayed plasticity during spherical nanoindentation of an iron-chromium-aluminum alloy:Effect of ferric ion irradiation

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j.urnal of Materials Science & Technology 2023年第36期167卷 228-236页

作者： Y.Zhang C.W.Li j.L.j.ang j.F.Gu H.wang Y.D.j.a G.wang X.G.An q.wang j.Lu Institute of Materials Shanghai UniversityShanghai 200072China School of Materials Science and Engineering Shanghai Jiao Tong UniversityShanghai 200240China Department of Mechanical Engineering City University of Hong KongKowloonSARChina Science and Technology on Reactor Fuel and Materials Laboratory Nuclear Power Institute of ChinaChengdu 610041China Interdisciplinary Materials Research Center Institute for Advanced StudyChengdu UniversityChengdu610106China

Spherical nanoindentation of an iron-chromium-aluminum alloy was conducted to study the effect of ferric-ion(Fe 3+)irradiation on the time-dependent plasticity behavior in the surface layers of this *** was observed that the initiation of plasticity by the appearance of displacement burst or“pop-in”event occurred after a period of waiting time in the apparent elastic regime and that Fe^(3+)irradiation at 360°C and up to∼0.5 displacements per atom could make it happen under the lower applied loads but with a reduced *** the experimental data,an activation volume and activation energy were extracted for the delayed *** results show that Fe^(3+)-irradiation significantly reduced its acti-vation volume from∼3.05 b 3 to∼1.75 b 3(where b=Burgers vector),but slightly increased its activation energy from∼0.65 to∼0.71 *** the other hand,high-resolution scanning transmission electron mi-croscopy observations reveal that the irradiation at the elevated temperature created interstitial atom pair onto the(100)habit plane that can serve as the nucleation site of a100dislocation loop while elim-inating the pre-existing ***,it is indicated that heterogeneous nucleation of the dislocation loop was predominant in the delayed plasticity initiation of this alloy and that the nucleation of the interstitial-type dislocation loop was involved due to Fe^(3+)-irradiation.

关键词： Spherical nanoindentation Delayed plasticity FeCrAl alloy Fe^(3+)-irradiation

A Study on Nanoparticle Aerosol Filtration via Different Fibrous Filters by Using CFD Approach

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j.urnal of Donghua University(English Edition) 2006年第5期23卷 97-100页

作者： q.wang B.Maze H.Vahedi Tafreshi B.Pourdeyhimi Nonwovens Cooperative Research Center North Carolina State University Raleigh NC 27695-8301 Fiber and Polymer Science Program North Carolina State University Raleigh NC 27695-8301 Nonwovens Cooperative Research Center North Carolina State University Raleigh NC 27695-8301

Fibrous filters such as nonwoven media are generally characterized by their collection efficiency and pressure drop. The traditional computational studies in this area typically based on unrealistic over-simplified geometries with the fibers placed in a lattice perpendicular to the flow. This paper describes the filter properties made of different Nonwoven materials by using Computational Fluid Dynamics （CFD） approach. In this study, for the first time, a virtual 3- D web is generated based on the fiber orientation information obtaining from analyzing microscopic images of both long-fiber and short-fiber nonwoven structures. Pressure drop and collection efflcicucy of our virtual filter are simulated and compared with the previous analytical and numerical models as well as experiment.

关键词： permeability CFD simulation nonwoven.

Fatigue Properties Improvement of Low-Carbon Alloy Axle Steel by Induction Hardening and Shot Peening:A Prospective Comparison

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Acta Metallurgica Sinica(English Letters) 2022年第8期35卷 1343-1356页

作者： G.C.Chu F.Z.Hu X.j.j.n Y.Zhang q.wang j.P.Hou Z.F.Zhang Shi-Changxu Innovation Center for Advanced Material Institute of Metal ResearchChinese Academy of SciencesShenyang 110016.China School of Materials Science and Engineering University of Science and Technology of ChinaHefei 230026China Manshan Iron and Steel Co. Ltd.Maanshan 243000China School of Materials Science and Engineering Shanghai Jiao Tong UniversityShanghai 200240China Baowu Group Masteel Rail Transit Materials Technology Company Limited Maanshan 243000China

Fatigue fracture is the maj.r threat to the railway axle, which can be avoided or delayed by surface strengthening. In this study, a low-carbon alloy axle steel with two states was treated by surface induction hardening and shot peening, respectively, to reveal the mechanism of fatigue property improvement by microstructure characterization, microhardness measurement, residual stress analysis, roughness measurement, and rotary bending fatigue tests. The results indicate that both quenching and tempering treatment can effectively improve the fatigue properties of the modified axle steel. In addition, induction hardening can create an ideal hardened layer on the sample surface by phase transformation from the microstructure of ferrite and pearlite to martensite. By comparison, shot peening can modify the microstructure in surface layer by surface severe plastic deformation introducing a large number of dislocation and even cause grain refinement. Both induction hardening and shot peening create compressive residual stress into the surface layer of axle steel sample, which can effectively reduce the stress level applied to the metal surface during the rotary bending fatigue tests. On the whole, the contribution of induction hardening to the fatigue life of axle steel sample is better than that of the shot peening, and induction hardening shows obvious advantages in improving the fatigue life of axle steel.

关键词： Surface strengthening Induction hardening Shot peening Axle steel Fatigue property improvement