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Synthesis and characterization of quaternized poly(phthalazinone ether sulfone ketone)for anion-exchange membrane

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Chinese Chemical Letters 2007年第10期18卷 1269-1272页

作者： Xi Gao Jian Chun Yan hua min zhang Shou Hai zhang Cheng Liu Ping Zhao Department of Polymer Materials Dalian University of Technology Dalian 116012 China PEMFC Key Materials ＆ Technology Laboratory Dalian Institute of Chemical Physics （DICP） Chinese Academy of Sciences Dalian 116023 China

Chloromethylated poly（phthalazinone ether sulfone ketone）（CMPPESK） was prepared from poly（phthalazinone ether sulfone ketone）（PPESK） using chloromethyl octyl ethers （CMOE） with lower toxicity as chloromethylated regent. CMPPESK was soluble in N-methyl-2-pyrrolidone （NMP）, N,N-dimethylacetamide （DMAc） and chloroform. Quaternized poly（phthalazinone ether sulfone ketone）（QAPPESK） was prepared from CMPPESK by quaternization. QAPPESK had excellent solvent resistance, which was only partly soluble in sulfuric acid （98%） and swollen in N,N-dimethylformamide （DMF）. The vanadium redox flow battery （V-RFB） using QAPPESK anion-exchange membrane had better performance with 88.3% of overall energy efficiency.

关键词： Chloromethylation Quaternization Poly(phthalazinone ether sulfone ketone) Anion-exchange membrane Vanadium redox flowbattery

Efficacy of Guhong injection versus Butylphthalide injection for mild ischemic stroke: A multicenter controlled study

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World Journal of Clinical Cases 2022年第21期10卷 7265-7274页

作者： Wei-Wei zhang Jiang Xin Guang-Yu zhang Qi-Jin Zhai hua-min zhang Cheng-Si Wu Department of Neurology The Seventh Medical Center of PLA General HospitalBeijing 100039China Department of Neurology Liaoning Provincial People’s HospitalShenyang Liaoning Provincial People's HospitalShenyang 110016Liaoning ProvinceChina Department of Neurology Cangzhou City People’s HospitalCangzhou 061000Hebei ProvinceChina Department of Neurology Huai’an Second People’s HospitalHuai’an 223002Jiangsu ProvinceChina Department of Neurology Ganyu People’s Hospital of LianyungangGanyu 222100Jiangsu ProvinceChina Department of Neurology The First Affiliated Hospital of Nanchang UniversityNanchang 330006Jiangxi ProvinceChina

BACKGROUND Most studies on Guhong injection have involved a single center with a small sample size,and the level of clinical evidence is *** To assess the safety and efficacy of Guhong injection for mild ischemic stroke(IS).METHODS A total of 399 IS patients treated at six hospitals from August 2018 to August 2019 were retrospectively *** patients were given Guhong injection(experimental group)or Butylphthalide injection(control group).Changes in National Institutes of Health Stroke Scale(NIHSS)and modified Rankin Scale(mRS)scores were observed before treatment and at 1,2,and 3 wk after treatment in each *** efficacy and safety of Guhong injection for IS were *** medications taken by the patients were confounding factors for efficacy *** factors were controlled by propensity score matching,and the results were further analyzed based on the *** The marked response rates at three follow-up visits were 64.64%,74.7%,and 66.7%in the experimental group,and 48.26%,45.4%,and 22.2%in the control *** marked response rates increased significantly in the experimental group compared with the control group(P0.05)and 64.0%and 47.7%in the control group(P<0.05)at the first

关键词： Guhong injection Ischemic stroke Propensity score matching National Institutes of Health Stroke Scale

Portable Analyzer for Rapid Analysis of Total Protein, Fat and Lactose Contents in Raw Milk Measured by Non-dispersive Short-wave Near-infrared Spectrometry

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Chemical Research in Chinese Universities 2013年第1期29卷 15-19页

作者： FENG Xu-dong SU Rui XU Nan WANG Xing-hua YU Ai-min zhang Han-qi CAO Yan-bo College of Chemistry Jilin University Changchun 130012 P. R. China

A novel portable analyzer for raw milk quality control during the material purchase at dairy plants was developed, by which the percentages（mass fraction） of main components including total protein, fat, and lactose of an unhomogenized milk sample could be determinated in 1 min with the help of non-dispersive short-wave near-infrared （NDSWNIR） spectrometry in a wavelength range from 600 nm to 1100 nm and multivariate calibration. The analyzer was designed with a single-beam optical system, which comprised a temperature control module, a multi-channel narrow-band light source（16 wavelengths）, a glass absorption cell with 15 mm sample thickness, a silicon photodiode detector, several compound lenses and a recorder module. A total of 80 raw milk samples were collected at a dairy farm twice a month for 4 months. The samples were scanned with a common UV-Vis-NIR spectrometer and analyzed according to China GB standard methods. The uninformative variables elimination（UVE） method was carried out on the spectrum data and the percentages of main components of all the samples to choose the peak emitting wavelength of each channel of the light source. Another 90 raw milk samples were collected from the same dairy farm thrice a month for 3 months. The samples were analyzed according to China GB standard methods and with the proposed analyzer. The percentages of the main components and the NDSWNIR absorption data of the samples were used for the construction and validation of the multivariate calibration model with partial least squares（PLS） method. The root-mean-square errors of prediction（RMSEP） of total protein, fat and lactose were 0.201, 0.172 and 0.247 and the coefficients of correlation（R） were 0.932, 0.981 and 0.933, respectively.

关键词： Portable analyzer Raw milk Non-dispersive short-wave near-infrared(NDSWNIR) spectrometry Multiva-riate calibration

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儿童康复机器人应用现状及发展趋势

中国康复理论与实践 2018年第6期24卷 667-670页

作者：华裕朱敏张跃南京医科大学附属儿童医院江苏南京市210008

成人康复机器人在临床的应用已逐步普及,但儿童康复机器人仍处于起步阶段。上肢机器人及下肢机器人在脑瘫儿童康复上都取得不错的效果,而拥有杰出互动性能的人形机器人也为孤独症儿童带来了希望。未来儿童康复机器人可能需要拥有更多的... 详细信息

成人康复机器人在临床的应用已逐步普及,但儿童康复机器人仍处于起步阶段。上肢机器人及下肢机器人在脑瘫儿童康复上都取得不错的效果,而拥有杰出互动性能的人形机器人也为孤独症儿童带来了希望。未来儿童康复机器人可能需要拥有更多的训练模式并结合虚拟现实等新技术来满足儿童康复的需求,同时也面临着高成本和安全性等问题。

关键词：儿童康复机器人脑性瘫痪孤独症综述

Synergistically enhanced ORR and HER performance on Co-N-C coupled in-situ generated PtCo intermetallic

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Journal of Energy Chemistry 2025年第1期100卷 721-729页

作者： Guanyu Luo min Song Lulu An Xiao huang Qian zhang Chenhao zhang Tao Shen Shuang Wang Deli Wang Key Laboratory of Material Chemistry for Energy Conversion and Storage (huazhong University of Science and Technology) ministry of Education School of Chemistry and Chemical Engineering Huazhong University of Science and Technology

Integrating multi-scale sites in a composite catalyst is vital to realize efficient ***,a synergistic composite catalyst consisting of Co atomic sites and in-situ generated PtCo intermetallic compounds （IMCs）(o-PtCo@CoNC) is proposed through Co pre-anchoring and subsequent impregnation-reduction *** loading of Co atoms provides a chance for in-situ generating PtCo ordered intermetallic *** remaining Co single atoms and PtCo IMCs construct synergistic electrocatalytic *** from the ordered structure,synergistic effect of Pt Co IMCs and Co single atoms,o-PtCo@CoNC exhibits excellent electrocatalytic performance for oxygen reduction reaction （ORR） and hydrogen evolution reaction （HER） with mass activity of 1.21 A mgPt-1（at 0.9 V） and5.70 A mgPt-1（at an overpotential of 100 mV）,***,o-PtCo@CoNC delivers negligible loss of half-wave potential and overpotential during long-term stability test in acid solutions,with 13 mV decay after 50,000 potential cycles for ORR and a 2.7 mV decay after 20,000 potential cycles for *** integration strategy of single-atomic sites coupled IMCs paves the way for enhancing the activity and durability of Pt-based electrocatalysts.

关键词： Electrolytic reduction

ImSpiRE: image feature-aided spatial resolution enhancement method

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Science China Life Sciences 2025年第1期 272-283页

作者： Yuwei hua Yizhi zhang Zhenming Guo Shan Bian Yong zhang State Key Laboratory of Cardiovascular Diseases and Medical Innovation Center Institute for Regenerative MedicineDepartment of NeurosurgeryShanghai East HospitalShanghai Key Laboratory of Signaling and Disease ResearchFrontier Science Center for Stem Cell ResearchSchool of Life Sciences and TechnologyTongji University

The resolution of most spatially resolved transcriptomic technologies usually cannot attain the single-cell level, limiting their applications in biological discoveries. Here, we introduce ImSpiRE, an image feature-aided spatial resolution enhancement method for in situ capturing spatial transcriptome. Taking the information stored in histological images, ImSpiRE solves an optimal transport problem to redistribute the expression profiles of spots to construct new transcriptional profiles with enhanced resolution, together with extending the gene expression profiles into unmeasured regions. Applications to multiple datasets confirm that ImSpiRE can enhance spatial resolution to the subspot level while contributing to the discovery of tissue domains, signaling communication patterns, and spatiotemporal characterization.

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相邻离心式喷嘴液膜撞击雾化过程仿真

推进技术 2017年第2期38卷 408-415页

作者：王凯李鹏飞杨国华张民庆西安航天动力研究所液体火箭发动机技术重点实验室陕西西安710100 西北工业大学航天学院陕西西安710072 航天推进技术研究院陕西西安710100

基于Gerris软件建立的锥形液膜雾化破碎过程数值仿真方法,对相邻多个离心式喷嘴液膜撞击雾化过程进行了数值仿真,可视化展示了喷雾场三维形态和结构特征,并做了流场分析,讨论了喷嘴之间的相互干扰作用,获得了液滴空间分布,对相邻不同数... 详细信息

基于Gerris软件建立的锥形液膜雾化破碎过程数值仿真方法,对相邻多个离心式喷嘴液膜撞击雾化过程进行了数值仿真,可视化展示了喷雾场三维形态和结构特征,并做了流场分析,讨论了喷嘴之间的相互干扰作用,获得了液滴空间分布,对相邻不同数目的喷嘴雾化效果进行了比较。结果表明:双喷嘴液膜撞击会形成一个类似互击式射流撞击形成的扇形区域,但又与其不同;锥形液膜的撞击效果主要依赖径向速度而不是切向速度,液滴平均粒径与撞击液膜间的旋向几乎无关。多喷嘴液膜撞击会使得液滴空间分布发生大的变化,液膜破碎长度会缩短。多喷嘴液膜撞击后的雾化特性是否改善与单喷嘴原先的雾化特性以及喷嘴间的距离密切相关。对于文中特定的喷嘴结构、喷嘴间距及排列方式,双喷嘴的液滴SMD均比单喷嘴的增大约4.8%~6.1%;四喷嘴的液滴SMD比单喷嘴的增大约7.3%,比双喷嘴的增大约2.4%。

关键词：离心式喷嘴锥形液膜撞击雾化过程数值仿真

A rapid advice guideline for the diagnosis and treatment of 2019 novel coronavirus(2019-nCoV) infected pneumonia(standard version)

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Military Medical Research 2020年第1期7卷 1-22页

作者： Ying-Hui Jin Lin Cai Zhen-Shun Cheng Hong Cheng Tong Deng Yi-Pin Fan Cheng Fang Di huang Lu-Qi huang Qiao huang Yong Han Bo Hu Fen Hu Bing-Hui Li Yi-Rong Li Ke Liang Li-Kai Lin Li-Sha Luo Jing Ma Lin-Lu Ma Zhi-Yong Peng Yun-Bao Pan Zhen-Yu Pan Xue-Qun Ren Hui-min Sun Ying Wang Yun-Yun Wang Hong Weng Chao-Jie Wei Dong-Fang Wu Jian Xia Yong Xiong Hai-Bo Xu Xiao-Mei Yao Yu-Feng Yuan Tai-Sheng Ye Xiao-Chun zhang Ying-Wen zhang Yin-Gao zhang hua-min zhang Yan Zhao ming-Juan Zhao Hao Zi Xian-Tao Zeng Yong-Yan Wang Xing-huan Wang 无 Center for Evidence-Based and Translational Medicine Zhongnan Hospital of Wuhan UniversityWuhan 430071China Institute of Hospital Management Wuhan UniversityWuhan 430071China Department of Respiratory Medicine Zhongnan Hospital of Wuhan UniversityWuhan 430071China Department of Pharmacy Zhongnan Hospital of Wuhan UniversityWuhan 430071China Institute of Evidence-Based Medicine and Knowledge Translation Henan UniversityKaifeng 475000China China Academy of Chinese Medical Sciences Beijing 100700China China Center for Evidence Based Traditional Chinese Medicine(CCEBTCM) Beijing 100700China Department of Critical Care Medicine Zhongnan Hospital of Wuhan UniversityWuhan 430071China Department of Clinical Laboratory Zhongnan Hospital of Wuhan UniversityWuhan 430071China Department of Infectious Diseases Zhongnan Hospital of Wuhan UniversityWuhan 430071China Division of Medical Affairs Zhongnan Hospital of Wuhan UniversityWuhan 430071China Division of Nursing Affairs Zhongnan Hospital of Wuhan UniversityWuhan 430071China Office of Nosocomial Infection Control Zhongnan Hospital of Wuhan UniversityWuhan 430071China Emergency Center Zhongnan Hospital of Wuhan UniversityWuhan 430071China Department of Radiology Zhongnan Hospital of Wuhan UniversityWuhan 430071China Department of Health Research Methods Evidenceand ImpactMcMaster UniversityHamiltonON L8S 4L8Canada Department of Traditional Chinese Medicine Zhongnan Hospital of Wuhan UniversityWuhan 430071China Global Health Institute Wuhan UniversityWuhan 430072China the Zhongnan Hospital of Wuhan University Novel Coronavirus Management and Research Team Evidence-Based Medicine Chapter of China International Exchange and Promotive Association for Medical and Health Care(CPAM)

In December 2019, a new type viral pneumonia cases occurred in Wuhan, Hubei Province;and then named "2019 novel coronavirus(2019-nCoV)" by the World Health Organization(WHO) on 12 January 2020. For it is a never been experienced respiratory disease before and with infection ability widely and quickly, it attracted the world’s attention but without treatment and control manual. For the request from frontline clinicians and public health professionals of 2019-nCoV infected pneumonia management, an evidence-based guideline urgently needs to be developed. Therefore, we drafted this guideline according to the rapid advice guidelines methodology and general rules of WHO guideline development;we also added the first-hand management data of Zhongnan Hospital of Wuhan University. This guideline includes the guideline methodology, epidemiological characteristics, disease screening and population prevention, diagnosis, treatment and control(including traditional Chinese Medicine), nosocomial infection prevention and control, and disease nursing of the 2019-nCoV. Moreover, we also provide a whole process of a successful treatment case of the severe 2019-nCoV infected pneumonia and experience and lessons of hospital rescue for 2019-nCoV infections. This rapid advice guideline is suitable for the first frontline doctors and nurses, managers of hospitals and healthcare sections, community residents, public health persons, relevant researchers, and all person who are interested in the 2019-nCoV.

关键词： 2019 novel coronavirus 2019-nCoV Respiratory disease Pneumonia Infectious diseases Rapid advice guideline Clinical practice guideline Evidence-based medicine

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光电极值法结合外差干涉法监控膜厚的研究

光学技术 2017年第2期43卷 184-186页

作者：常敏华博张学典江旻珊上海理工大学光电信息与计算机工程学院上海200093 上海市现代光学系统重点实验室上海200093

光电极值法是光学薄膜厚度监测的常用方法,该方法在镀膜前引用块状材料的折射率设计膜系。而在实际镀制过程中,用于镀制光学薄膜的材料折射率会发生改变,从而给膜厚的监控带来误差。为了避免折射率变化的影响,采用外差干涉法测量折射率... 详细信息

光电极值法是光学薄膜厚度监测的常用方法,该方法在镀膜前引用块状材料的折射率设计膜系。而在实际镀制过程中,用于镀制光学薄膜的材料折射率会发生改变,从而给膜厚的监控带来误差。为了避免折射率变化的影响,采用外差干涉法测量折射率,将实际测得的薄膜折射率应用光电极值法监控薄膜的设计,从而减少了因材料折射率的变化引起的误差。以750nm截止滤光片的镀制为被测对象进行了实验,对制备的滤光片透射率光谱曲线进行了比较。结果表明,实际的透射率曲线与设计的透射率曲线吻合较好,两次实验曲线平均吻合度均在98%以上,系统稳定性很好,从而说明结合外差干涉法的光电极值监控法可以很好地克服折射率变化引起的误差。

关键词：光电极值法光学薄膜外差干涉法