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Influence of post-heat treatment on the microstructure and mechanical properties of Al-Cu-Mg-Zr alloy manufactured by selective laser melting

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Journal of Materials Science & Technology 2022年第16期111卷 35-48页

作者： Yanfang wang Xin Lin Nan Kang zihong wang Yuxi Liu Weidong Huang State Key Laboratory of Solidification Processing Northwestern Polytechnical UniversityXi’an 710072China Key Laboratory of Metal High Performance Additive Manufacturing and Innovative Design MIIT ChinaNorthwestern Polytechnical UniversityXi’an 710072China

The properties of modified conventional wrought aluminum alloys cannot be significantly enhanced by normal post-heat treatment in that the fine-grained strengthening,arising from high cooling rate in SLM,is underutilized.In this work,compared with the normal T6 heat treatment,a novel simple direct aging regime was proposed to maintain the grain-boundary strengthening and to utilize the precipitation strengthening of secondary AlZr.It was found that a heterogeneous grain structure,which consisted of ultrafine equiaxed(~0.82μm)and columnar(~1.80μm)grains at the bottom and top of molten pool,respectively,was formed in the SLM processed sample.After direct aging(DA),the ultrafine grains were maintained and a mass of spherical coherent L1-AlZr particles with a mean radius of approximately1.15 nm was precipitated.In contrast,after solution treatment and aging(STA),a significant grain coarsening occurred in the equiaxed grain region.Meanwhile,the coarsening L1-AlZr particles,nano-sized S phases and GPB zones were detected in the STA sample.This subsequently induced that the yield strength of the DA sample(~435 MPa)was higher than that of the STA sample(~402 MPa)owing to the grain boundary strengthening and precipitation strengthening.Both the STA and DA samples exhibited a higher strength than that of the other SLMed Al-Cu-Mg series alloys;this was comparable to that of the wrought AA2024-T6 alloy(~393 MPa).Both the STA and DA samples exhibited a higher strength than that of the other SLMed Al-Cu-Mg series alloys;this was comparable to that of the wrought AA2024-T6alloy(~393 MPa).

关键词： Selective laser melting Al-Cu-Mg alloy Heat treatment Microstructure Mechanical properties

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Laser powder bed fusion of Zr-modified Al-Cu-Mg alloy:Processability and elevated-temperature mechanical properties

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Journal of Materials Science & Technology 2023年第5期136卷 223-235页

作者： Yanfang wang Xin Lin Yufan Zhao zihong wang Xiaobin Yu Xuehao Gao Weidong Huang State Key Laboratory of Solidification Processing Northwestern Polytechnical UniversityXi’an 710072China Key Laboratory of Metal High Performance Additive Manufacturing and Innovative Design MIIT ChinaNorthwestern Polytechnical UniversityXi’an 710072China

Zr modification is an effective method for improving hot-cracking resistance and elevated-temperature mechanical properties during laser powder bed fusion(L-PBF)of traditional medium and high strength wrought aluminum alloys.This study investigated the l-PBF processability and elevated-temperature mechanical properties of a Zr-modified 2024Al alloy.It was found that the hot-cracking susceptibility increased with the increased scanning speed,which was in reasonable agreement with the modified Rappaz-Drezet-Gremaud criterion.Furthermore,the primary L1_(2)-Al_(3)Zr precipitates,which acted as ef-ficient nucleation sites,precipitated at the fusion boundary of the melt pool,leading to the formation of a heterogeneous grain structure.The yield strength(YS)of the as-fabricated samples at 150,250,and 350℃was 363,210,and 48 MPa,respectively.Despite the slight decrease to 360 MPa of the YS when tested at 150℃,owing to the additional precipitate strengthening from the L1_(2)-Al_(3)Zr precipitates,the YS achieved yield strengths of 253 and 69 MPa,an increase of 20.5%and 30.4%,when tested at 250 and 350℃,respectively.The yield strengths in both the as-fabricated and T6-treated conditions tested at 150 and 250℃were comparable to those of casting Al-Cu-Mg-Ag alloys and superior to those of traditionally heat-resistant 2219-T6 and 2618-T6 of Al-Cu alloys.

关键词： Laser powder bed fusion Zirconium Al-Cu-Mg alloy Processability Elevated-temperature mechanical property

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Solidification microstructure evolution and its correlations with mechanical properties and damping capacities of Mg-Al-based alloy fabricated using wire and arc additive manufacturing

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Journal of Materials Science & Technology 2023年第13期144卷 28-44页

作者： zihong wang Jingfeng wang Xin Lin Nan Kang Tianchi Zhang Yanfang wang Li wang Cong Dang Weidong Huang College of Materials Science and Engineering Chongqing UniversityChongqing 400045China National Engineering Research Center for Magnesium Alloys Chongqing UniversityChongqing 400044China Key Laboratory of Metal High Performance Additive Manufacturing and Innovative Design MIIT ChinaNorthwestern Polytechnical UniversityXi’an 710072China Arts et Métiers Institute of Technology MSMPHESAM UniversitéChâlons-en-Champagne F-51006France Chongqing Construction Science Research Institute Chongqing 401147China

Magnesium(Mg)alloys,as the lightest metal structural material with good damping capacities,have im-portant application prospects in realizing structural lightweight and vibration reduction.However,their engineering application is greatly limited by poor plastic formability.Wire and arc additive manufactur-ing(WAAM)provides a potential approach for fabricating large-scale Mg alloy components with high manufacturing flexibility.In this study,the evolution of the solidification microstructure of a WAAM-processed Mg-Al-based alloy was quantitatively analyzed based on the analytical models;then,the cor-relations between the solidification microstructure and mechanical properties/damping capacities were investigated.The results revealed that the WAAM-processed Mg-Al-based alloy with an equiaxed-grain-dominated microstructure displayed a simultaneous enhancement in mechanical properties and damping capacities compared to those of the cast Mg-Al-based alloy.The good combination of mechanical prop-erties and damping capacities are mainly attributed to the weakened basal texture with a relatively high Schmid factor for basalslip,the twinning-induced plasticity(TWIP)effect associated with the profuse{10-12}tensile twinning,and the relatively high dislocation density caused by the thermal stress during the WAAM process.

关键词： Wire and arc additive manufacturing Magnesium alloy Microstructure evolution Mechanical properties Damping capacities

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Durable semi-crystalline interphase engineering to stabilize high voltage Ni-rich cathode in dilute ether electrolyte

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Journal of Energy Chemistry 2023年第4期79卷 110-117页

作者： Zhuangzhuang Cui Shunqiang Chen Qingshun Nian Yecheng Li Yawei Chen Bing-Qing Xiong zihong wang Zixu He Shuhong Jiao Xiaodi Ren School of Chemistry and Materials Science University of Science and Technology of ChinaHefei 230026AnhuiChina

Ethers are promising electrolyte solvents for secondary Li metal batteries because of their excellent reduction stability.However,their oxidation stability has been mostly relying on the high concentration approach,and limited progress has been made on building effective interphase to protect the cathode from the corrosion of the electrolyte.In this work,we construct a semi-crystalline interfacial layer on the surface of Li(Ni_(0.8)Co_(0.1)Mn_(0.1))O_(2)cathode that can achieve improved electrochemical stability in the highly corrosive chemical environment formed by the decomposition of ether molecules.Different from traditional brittle crystalline interphases,the optimized semi-crystalline layer with low modulus and high ionic conductivity can effectively relieve electrode strain and maintain the integrity of the interface layer.Due to this design,the continuous oxidation decomposition of ether-based electrolytes could be significantly suppressed and the battery shows outstanding cycling stability(84%capacity retention after 300 cycles).This article provides a solution to address the oxidation instability issue of ether-based electrolytes.

关键词： Cathode/electrolyte interphase Semi-crystalline Ether electrolyte High-voltage cathode Li-metal batteries

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Wasserstein GAN-Based Small-Sample Augmentation for New-Generation Artificial Intelligence: A Case Study of Cancer-Staging Data in Biology

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Engineering 2019年第1期5卷 156-163页

作者： Yufei Liu Yuan Zhou Xin Liu Fang Dong Chang wang zihong wang College of Life Science and Technology Huazhong University of Science and Technology Wuhan 430074 China School of Public Policy and Management Tsinghua University Beijing 100084 China School of Mechanical Science and Engineering Huazhong University of Science and Technology Wuhan 430074 China Center for Strategic Studies Chinese Academy of Engineering Beijing 100088 China

It is essential to utilize deep-learning algorithms based on big data for the implementation of the new generation of artificial intelligence. Effective utilization of deep learning relies considerably on the number of labeled samples, which restricts the application of deep learning in an environment with a small sample size. In this paper, we propose an approach based on a generative adversarial network (GAN) combined with a deep neural network (DNN). First, the original samples were divided into a training set and a test set. The GAN was trained with the training set to generate synthetic sample data, which enlarged the training set. Next, the DNN classifier was trained with the synthetic samples. Finally, the classifier was tested with the test set, and the effectiveness of the approach for multi-classification with a small sample size was validated by the indicators. As an empirical case, the approach was then applied to identify the stages of cancers with a small labeled sample size. The experimental results verified that the proposed approach achieved a greater accuracy than traditional methods. This research was an attempt to transform the classical statistical machine-learning classification method based on original samples into a deep-learning classification method based on data augmentation. The use of this approach will contribute to an expansion of application scenarios for the new generation of artificial intelligence based on deep learning, and to an increase in application effectiveness. This research is also expected to contribute to the comprehensive promotion of new-generation artificial intelligence.

关键词： Artificial intelligence Generative adversarial network Deep neural network Small sample size Cancer

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Laser-based directed energy deposition of novel Sc/Zr-modified Al-Mg alloys:columnar-to-equiaxed transition and aging hardening behavior

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Journal of Materials Science & Technology 2021年第10期69卷 168-179页

作者： zihong wang Xin Lin Yao Tang Nan Kang Xuehao Gao Shuoqing Shi Weidong Huang State Key Laboratory of Solidification Processing Northwestern Polytechnical UniversityXi'an 710072China Key Laboratory of Metal High Performance Additive Manufacturing and Innovative Design MIIT ChinaNorthwestern Polytechnical UniversityXi'an 710072China

The control of grain morphology is important in laser additive manufacturing(LAM),as grain morphology further affects the hot cracking resistance,anisotropy,and strength–ductility synergy of materials.To develop a solidification-control solution and achieve columnar-to-equiaxed transition(CET)in Al-based alloys during LAM,Sc-and-Zr-modified Al-Mg alloys were processed via directed energy deposition(DED).CET was achieved by introducing high potent primary Al_(3)(Sc,Zr)nucleation sites ahead of the solidification interface.Furthermore,the relationship between the solidification control parameters and precipitation behavior of primary Al_(3)(Sc,Zr)nucleation sites was established using the time-dependent nucleation theory.Then,the CET was studied according to the Hunt criterion.The results indicated that coarse columnar grain structure was still obtained at the inner region of the molten pool at low Sc/Zr contents owing to the effective suppression of the precipitation of the primary Al_(3)(Sc,Zr)nucleation sites via rapid solidification during DED.In addition,the relatively low melt temperature at the fusion boundary unavoidably promoted the precipitation of primary Al_(3)(Sc,Zr)nucleation sites,which resulted in a fine equiaxed grains band at the edge of the molten pool.As the Sc/Zr content increased,the solidification cooling rate was not sufficient to suppress the precipitation of the primary Al_(3)(Sc,Zr)nucleation sites,and a fully equiaxed grain structure was obtained.Furthermore,the effect of the layer-by-layer manufacturing process on the subsequent precipitation strengthening of secondary Al_(3)(Sc,Zr)precipitates was discussed.Both the remelting and subsequent aging during thermal cycling should be considered to achieve greater precipitation strengthening.

关键词： Al-Mg-Sc-Zr alloys Additive manufacturing Directed energy deposition Columnar-to-equiaxed transition Phase precipitation

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Effect of Cu content on microstructure and mechanical properties of in-situ β phases reinforced Ti/Zr-based bulk metallic glass matrix composite by selective laser melting(SLM)

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Journal of Materials Science & Technology 2021年第8期67卷 174-185页

作者： Xuehao Gao Xin Lin Qiaodan Yan zihong wang Xiaobin Yu Yinghui Zhou Yunlong Hu Weidong Huang State Key Laboratory of Solidification Processing Northwestern Polytechnical UniversityXi’an710072China Key Laboratory of Metal High Performance Additive Manufacturing and Innovative Design MUT ChinaNorthwestern Polytechnical UniversityXi'an710072China

In this study,non-toxic in-situβphases of reinforced Ti/Zr-based bulk metallic glass matrix composites(BMGCs)of(Ti_(0.65)Zr_(0.35))100-xCux(x=5,10,15 at.%)are fabricated via selective laser melting.The effect of Cu content on phase formation,microstructure,and mechanical properties is investigated.The average volume fraction and width of theβphase decreases with increasing Cu content,while a more amorphous phase and the(Ti,Zr)_(2)Cu phase forms.In the center zone of the molten pool,theβphase grows in the direction of the temperature gradient,and the amorphous phase distributes among theβphases.This occurs using:sphere morphology(for x=5),a more continuous elongated sphere and network morphology(for x=10),and network morphology(for x=15),respectively.In the edge zone of the molten pool,due to the smaller cooling rate and the existence of a partially molten zone,theβphase becomes coarser,and an amorphous phase forms for more continuous networks.Furthermore,the hardness improves significantly with increasing Cu content.No crack is found for x=5.Although the average volume fraction of theβphase for x=5 is about 90%,the compression yield strength is 1386±64 MPa,reaching to an average level of conventionally fabricated counterparts,due to finer microstructure,and twinning and martensitic transformation of theβphase.

关键词： Metallic glass Amorphous phase βPhase Bulk metallic glass matrix composites(BMGCs) Additive manufacturing(AM) Selective laser melting(SLM)

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智能算法在新能源企业价值因素评估中的应用

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集成电路应用 2024年第2期41卷 390-391页

作者：王梓宏黑龙江科技大学黑龙江150022

阐述新能源企业的价值驱动因素,人工智能算法在新能源企业中的应用,包括数据收集与处理、预测与优化模型。人工智能算法在提升技术创新能力、市场需求预测中发挥关键作用。

关键词：新能源应用价值驱动因素智能算法

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基于多空间属性信息融合的序列推荐

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计算机科学 2024年第3期51卷 102-108页

作者：王子泓邵蓥侠何吉元刘金宝北京邮电大学计算机学院北京100876 美团平台搜索推荐算法部北京100102

序列推荐旨在从用户的历史行为中建模用户不断变化的兴趣,从而做出与用户兴趣相关的推荐。近年来,物品属性信息被证明可以提升序列推荐的性能,很多工作基于属性信息融合去提升序列推荐的性能,都取得了成效但仍存在一定的不足。首先,它... 详细信息

序列推荐旨在从用户的历史行为中建模用户不断变化的兴趣,从而做出与用户兴趣相关的推荐。近年来,物品属性信息被证明可以提升序列推荐的性能,很多工作基于属性信息融合去提升序列推荐的性能,都取得了成效但仍存在一定的不足。首先,它们没有显式地建模出用户对物品属性的偏好或者只建模了一个属性偏好向量,无法充分表达用户的偏好。其次,它们的物品属性信息融合过程未考虑用户个性化信息的影响。因此,针对上述不足,提出了基于多空间属性信息融合的序列推荐(MAIF-SR)。文中提出了多空间属性信息融合框架,在不同的属性空间下融合属性序列并建模出用户对不同属性的偏好,用多维兴趣充分表达用户的偏好;设计了个性化属性注意力机制,在融合信息的过程中引入用户个性化信息,增强融合信息的个性化效果。在两个公开数据集以及一个工业私有数据集上进行实验,结果表明,MAIF-SR优于用于对比的基于属性信息融合的序列推荐。

关键词：序列推荐物品属性信息融合用户个性化注意力机制多维兴趣

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Laser powder bed fusion of high-strength Sc/Zr-modified Al–Mg alloy:phase selection,microstructural/mechanical heterogeneity,and tensile deformation behavior

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Journal of Materials Science & Technology 2021年第36期95卷 40-56页

作者： zihong wang Xin Lin Nan Kang Jing Chen Hua Tan Zhe Feng Zehao Qin Haiou Yang Weidong Huang State Key Laboratory of Solidification Processing Northwestern Polytechnical UniversityXi'an 710072China Key Laboratory of Metal High Performance Additive Manufacturing and Innovative Design MIIT ChinaNorthwestern Polytechnical UniversityXi'an 710072China

Laser powder bed fusion(L-PBF)of Sc/Zr-modified Al-based alloys has recently become a promising method for developing a new generation of high-performance Al alloys.To clarify the modification roles of Sc/Zr elements,an Al–4.66Mg–0.48Mn–0.72Sc–0.33Zr(wt.%)alloy was processed using L-PBF.The effect of the local solidification condition of the molten pool on the precipitation behavior of primary Al_(3)(Sc,Zr)was analyzed based on time-dependent nucleation theory.It was found that primary Al_(3)(Sc,Zr)inevitably precipitated at the fusion boundary,while its precipitation could be effectively suppressed in the inner region of the molten pool.This subsequently induced the formation of a heterogeneousα-Al matrix.After direct aging,the heredity of solidification microstructure introduced heterogeneous secondary Al_(3)(Sc,Zr)precipitates withinα-Al matrix.Owing to the inverse relationship between grain boundary strengthening and precipitation strengthening,the direct-aged sample with dual heterogeneous structures exhibited reduced mechanical heterogeneity,resulting in lowered hetero-deformation-induced hardening.The low strain-hardening capability in the direct-aged sample promoted necking instability while inducing a large Lüders elongation,which effectively improved the tensile ductility.

关键词： Additive manufacturing Al–Mg–Sc–Zr alloys Laser powder bed fusion Heterogeneous microstructure Deformation behavior

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