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抗大应变管线钢X80在碱性腐蚀环境中的耐蚀性

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材料热处理学报 2016年第1期37卷 175-179页

作者：赵伟邹勇夏佃秀邹增大山东大学材料液固结构演变与加工教育部重点试验室山东济南250061 济南大学机械工程学院山东济南250022

利用极化曲线、交流阻抗谱、Mott-Schottky曲线分析、循环极化曲线的方法,研究了X80抗大变形（X80HD）管线钢在模拟土壤碱性腐蚀环境（0.5 mol/L Na2CO3＋1 mol/L Na HCO3溶液）中的耐蚀性。结果表明,该钢在25~95℃范围内均会发生钝化现... 详细信息

利用极化曲线、交流阻抗谱、Mott-Schottky曲线分析、循环极化曲线的方法,研究了X80抗大变形（X80HD）管线钢在模拟土壤碱性腐蚀环境（0.5 mol/L Na2CO3＋1 mol/L Na HCO3溶液）中的耐蚀性。结果表明,该钢在25~95℃范围内均会发生钝化现象,氧气不是钝化发生的必要条件;随着温度升高,钝化变得不稳定,自腐蚀电位减小,自腐蚀电流密度增加,电荷转移电阻减小,耐蚀性变差;25℃时,加入0.5%Na Cl未见明显点蚀,而加入1.5%Na Cl后发生了严重的点蚀,表面可见大量腐蚀坑的存在;一定程度上升高温度可以降低X80HD管线钢在添加Cl-的溶液中发生点蚀的可能性,这主要是由于升高温度,OH-浓度增加所致。

关键词：腐蚀管线钢电化学点蚀

时效温度对Super304H钢析出相的影响

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材料热处理学报 2009年第6期30卷 51-56页

作者：李新梅邹勇张忠文邹增大山东大学材料液固结构演变与加工教育部重点实验室山东济南250061 山东电力研究院山东济南250002

利用扫描电子显微镜、电子探针、X射线衍射和透射电镜研究了新型奥氏体耐热钢Super304H在高温时效条件下析出相的变化。结果表明,Super304H钢经700-1250℃时效后,组织中出现4种析出相：Nb（C,N）、富Cu相、M23C6和NbCrN。随时效温度的不... 详细信息

利用扫描电子显微镜、电子探针、X射线衍射和透射电镜研究了新型奥氏体耐热钢Super304H在高温时效条件下析出相的变化。结果表明,Super304H钢经700-1250℃时效后,组织中出现4种析出相：Nb（C,N）、富Cu相、M23C6和NbCrN。随时效温度的不同,析出相发生析出或溶解的变化,同时它们的形态、分布和数量随温度变化呈现出不同的变化规律,其中M23C6在700-900℃主要沿晶界析出,这将会降低钢的高温蠕变强度及抗晶间腐蚀性能。

关键词： Super304H钢时效析出相

Super304H奥氏体耐热钢微观组织研究

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材料科学与工艺 2010年第2期18卷 256-261页

作者：李新梅邹勇张忠文邹增大山东大学材料液固结构演变与加工教育部重点实验室济南250061 山东电力研究院济南250002

为了深入认识新型奥氏体耐热钢Super304H(0.1C-18Cr-9Ni-3Cu-Nb,N)的微观组织,利用光学显微镜、扫描电子显微镜、电子探针和X射线衍射等手段,研究了Super304H钢合金元素的分布和析出相的组成及分布形态.试验结果表明,Super304H钢在供货... 详细信息

为了深入认识新型奥氏体耐热钢Super304H(0.1C-18Cr-9Ni-3Cu-Nb,N)的微观组织,利用光学显微镜、扫描电子显微镜、电子探针和X射线衍射等手段,研究了Super304H钢合金元素的分布和析出相的组成及分布形态.试验结果表明,Super304H钢在供货状态下的显微组织由γ-基体和析出相组成.与传统的18-8不锈钢相比,这种奥氏体钢晶粒均匀细小,晶粒尺寸约46μm.析出相主要由Nb(C,N)和富铜相组成,Nb(C,N)有呈方向性分布的条块状和呈弥散分布的细小颗粒状两种形态,条块状的Nb(C,N)是软化过程中残留下来的,而弥散分布的是固溶处理及冷却过程中析出形成的.其中弥散分布的Nb(C,N)与富铜相对细化晶粒和改善钢的高温强度起重要作用,而多种复合强化机制使得Super304H钢具有优异的高温性能.

关键词：奥氏体耐热钢 Super304H钢析出相微观组织高温性能

High photoluminescence Ag-In-Ga-S quantum dots based on ZnX_(2)-treated surface passivation

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Nano Research 2024年第8期17卷 7533-7541页

作者： danni Yan Yuhui Dong Naiwei Wei Shuai Yang Hong Zhu Wanzhong Gu Yousheng zou Haibo zeng MIIT Key Laboratory of Advanced Display Materials and Devices Institute of Optoelectronics&NanomaterialsSchool of Materials Science and EngineeringNanjing University of Science and TechnologyNanjing 210094China

Quaternary Ag-In-Ga-S(AIGS)quantum dot(QD)is considered a promising,spectral-tunable,and environmentally friendly luminescent display ***,the more complex surface defect states of AIGS QDs resulting from the coexistence of multiple elements lead to a low(dangling and Zn2+.The realization of high PLQY will further promote the application of AIGS QDs in luminescent displays.

关键词： I-III-VI quantum dots Ag-In-Ga-S surface defect passivation Z-type ligand photoluminescence quantum yield

新型耐热钢Super304H高温时效后的组织与性能

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材料工程 2009年第5期37卷 38-42页

作者：李新梅邹勇张忠文邹增大山东大学材料液态结构及遗传性教育部重点实验室济南250061 山东大学热科学与工程研究中心济南250061 山东电力研究院济南250002

采用光学显微镜、扫描电子显微镜及X射线衍射等手段并通过显微硬度和冲击实验，研究了Supre304H钢经750～1350℃时效后的微观组织和性能。结果表明：高温时效后Super304H钢的微观组织为7相＋析出相；随时效温度的不同，基体晶粒尺寸及... 详细信息

采用光学显微镜、扫描电子显微镜及X射线衍射等手段并通过显微硬度和冲击实验，研究了Supre304H钢经750～1350℃时效后的微观组织和性能。结果表明：高温时效后Super304H钢的微观组织为7相＋析出相；随时效温度的不同，基体晶粒尺寸及析出相的种类、分布发生不同的变化。在750℃左右因微细沉淀强化及细晶组织使得显微硬度达到最大值，而后随温度升高以及析出相、晶粒尺寸与固溶元素的变化，显微硬度呈现先快速下降后缓慢下降的趋势；时效试样的冲击功值随温度升高在850℃左右，由于M28C6沿晶界大量析出导致晶界脆化而达到最低值，后又因析出相的再溶解致使晶界脆化效果趋弱而逐渐升高。

关键词： Super304H钢时效处理析出相组织性能

Rh(Ⅱ)-catalyzed intermolecular carboamination of pyridines via double Csp^(2)-H bond activations

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Science China Chemistry 2024年第1期67卷 374-382页

作者： Zhongfeng Luo Jingxing Jiang Lifang zou Xiaoyu Zhou Junshan Liu Zhuofeng Ke Fengjuan Chen Huanfeng Jiang Wei zeng Key Laboratory of Functional Molecular Engineering of Guangdong Province School of Chemistry and Chemical EngineeringSouth China University of TechnologyGuangzhou 510641China School of Materials Science and Engineering PCFM LabSun Yat-sen UniversityGuangzhou 510275China Guangdong Provincial Key Laboratory of Chinese Medicine Pharmaceutics School of Traditional Chinese MedicineSouthern Medical UniversityGuangzhou 510515China

We disclose the development of the Rh-catalyzed amine-directed remote 5,6-carboamination protocol of pyridines via dual Csp^(2)-H functionalizations.A variety of readily available 2-aminopyridines and 1,2,3-triazoles are allowed for coupling cyclization to access polyfunctionalized *** studies including DFT calculations unveil that relay carbenoidelectrophilic addition to pyridines and the sequential pyridyl Csp^(2)-H amination are involved in this *** postsynthetic utility of this methodology is showcased by versatile and site-selective modification of azaindoles.

关键词： Rh-catalysis azaindoles pyridyl Csp^(2)-H bond carboamination coupling-cyclization

Climate state of the Three Gorges Region in the Yangtze River basin in 2022–2023

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Atmospheric and Oceanic Science Letters 2024年第5期17卷 61-66页

作者： Tong Cui Xianyan Chen Xukai zou Linhai Sun Qiang Zhang Hongling zeng National Climate Center China Meteorological AdministrationBeijingChina

Based on daily observation data of the Three Gorges Region(TGR)of the Yangtze River basin and global reanalysis data,the climate characteristics,climate events,and meteorological disasters of the TGR in 2022 and 2023 were *** the TGR,the average annual temperature for 2022 and 2023 was 0.8℃ and 0.4℃ higher than normal,respectively,making them the two warmest years in the past *** 2022,the TGR experienced its warmest summer on *** average air temperature was 2.4℃ higher than the average,and there were 24.8 days of above-average high temperature days during *** in the TGR varied significantly between 2022 and *** rainfall was 18.4%below normal and drier than normal in most parts of the *** contrast,the precipitation in 2023 was considerably higher than the long-term average,and above normal for almost the entire *** average wind speed exhibited minimal variation between the two ***,the number of foggy days and relative humidity increased in 2023 compared to *** 2022–2023,the TGR mainly experienced meteorological disasters such as extreme high temperatures,regional heavy rain and flooding,overcast rain,and inverted spring *** indicates that the abnormal western Pacific subtropical high and the abnormal persistence of the eastward-shifted South Asian high were the two important drivers of the durative enhancement of record-breaking high temperature in the summer of 2022.

关键词： Three Gorges Region Climate state Extreme high temperature Torrential summer rainfall Climate analysis

Matrix stiffening promotes chondrocyte senescence and the osteoarthritis development through downregulating HdaC3

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Bone Research 2024年第2期12卷 438-452页

作者： Bowen Fu Jianlin Shen Xuenong zou Nian Sun Ze Zhang zengping Liu Canjun zeng Huan Liu Wenhua Huang Guangdong Medical Innovation Platform for Translation of 3D Printing Application The Third Affiliated HospitalSouthern Medical UniversityGuangzhou 510630 GuangdongChina Guangdong Engineering Research Center for Translation of Medical 3D Printing Application Guangdong Provincial Key Laboratory of Digital Medicine and BiomechanicsNational Key Discipline of Human AnatomySchool of Basic Medical SciencesSouthern Medical UniversityGuangzhou 510145 GuangdongChina Department of Foot and Ankle Surgery Center for Orthopedic SurgeryThe Third Affiliated HospitalSouthern Medical UniversityGuangzhou 510630 GuangdongChina Department of Orthopedics Affiliated Hospital of Putian UniversityPutian 351100 FujianChina Central Laboratory Affiliated Hospital of Putian UniversityPutian 351100 FujianChina Guangdong Provincial Key Laboratory of Orthopedics and Traumatology Department of Spinal SurgeryThe First Affiliated Hospital of Sun Yat-sen UniversityGuangzhou 510080 GuangdongChina Nanfang Hospital Southern Medical UniversityGuangzhou 510515 GuangdongChina Guangzhou Blood Center Guangzhou 510095 GuangdongChina Department of Orthopedics The Affiliated Traditional Chinese Medicine HospitalSouthwest Medical UniversityLuzhou 646000 SichuanChina

Extracellular matrix(ECM)stiffening is a typical characteristic of cartilage aging,which is a quintessential feature of knee osteoarthritis(KOA).However,little is known about how ECM stiffening affects chondrocytes and other molecules *** study mimicked the physiological and pathological stiffness of human cartilage using polydimethylsiloxane(PDMS)*** demonstrated that epigenetic Parkin regulation by histone deacetylase 3(HdaC3)represents a new mechanosensitive mechanism by which the stiffness matrix affected chondrocyte *** found that ECM stiffening accelerated cultured chondrocyte senescence in vitro,while the stiffness ECM downregulated HdaC3,prompting Parkin acetylation to activate excessive mitophagy and accelerating chondrocyte senescence and osteoarthritis(OA)in ***,intra-articular injection with an HdaC3-expressing adeno-associated virus restored the young phenotype of the aged chondrocytes stimulated by ECM stiffening and alleviated OA in *** findings indicated that changes in the mechanical ECM properties initiated pathogenic mechanotransduction signals,promoted the Parkin acetylation and hyperactivated mitophagy,and damaged chondrocyte *** results may provide new insights into chondrocyte regulation by the mechanical properties of ECM,suggesting that the modification of the physical ECM properties may be a potential OA treatment strategy.

关键词： chondrocyte osteoarthritis stiffness

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双丝间接电弧焊的电弧形态

焊接学报 2006年第12期27卷 49-52页

作者：曹梅青邹增大杜宝帅曲仕尧山东大学材料科学与工程学院济南250061

用高速摄像系统及示波器对双丝间接电弧气体保护焊的电弧形态进行了研究。结果表明,双丝间接电弧气体保护焊在两丝端部形成电弧,其电弧本质仍然是气体放电的一种表现形式。焊接电流、电弧电压及两焊丝交点与工件间距离对电弧形态产生较... 详细信息

用高速摄像系统及示波器对双丝间接电弧气体保护焊的电弧形态进行了研究。结果表明,双丝间接电弧气体保护焊在两丝端部形成电弧,其电弧本质仍然是气体放电的一种表现形式。焊接电流、电弧电压及两焊丝交点与工件间距离对电弧形态产生较大的影响,随焊接电流的变化,电弧形态会发生不同程度的集中与分散的变化;电压越大电弧越明亮电弧的形体也越大;两丝交点与工件间距离越小,电弧越集中并且变得短而亮。燃烧过程中电弧电压随时间而周期性变化,相应的电弧形态也随着时间发生周期性变化,电弧电压与电弧形态间有很好的对应关系。

关键词：双丝间接电弧焊电弧形态焊接电流电弧电压