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Synthesis of porous iron hydroxy phosphate from phosphate residue and its application as a Fenton-like catalyst for dye degradation

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Journal of Environmental Sciences 2022年第2期34卷 307-319页

作者： Weilin Guo yin cao Yi Zhang Lijun Wang Lingxue Kong School of Environmental and Materials Engineering Shanghai Polytechnic UniversityShanghai 200240China Deakin University GeelongInstitutefor Frontier MaterialsVictoria 3216Australia Shanghai Innovation Institutefor Materials Shanghai 200444China

Phosphate residue is a kind of hazardous solid waste and if not properly disposed of, could cause serious environmental contaminations. The abundant iron salt available in phosphate residue can be used to prepare photo-Fenton catalytic reagent for wastewater treatment. In this study, the phosphate residue was effectively purified by a hydrothermal recrystallization method, reaching an iron phosphate purity of 94.2%. The particles of iron phosphate were further processed with ball milling with their average size reduced from 19.4 to 1.6 μm. By hydrothermal crystallization of iron phosphate and thermal decomposition of oxalate precursor, porous iron hydroxy phosphate was prepared. The modified porous iron hydroxy phosphate(m-PIHP) of higher surface area with iron oxalate on its surface can degrade 98.87% of Rhodamine B in 15 min. Cyclic experiment showed that the catalyst still had a good catalytic activity after six cycles( > 40%). The X-ray photoelectron spectroscopy results showed that the iron oxalate complex on the catalyst surface decomposed to produce ferrous ions and accelerated the rate of · OH production. The current work demonstrated that the m-PIHP synthesized from phosphate residue and modified with iron oxalate can be used as an effective dye wastewater treatment agent.

关键词： Phosphate residue Porous iron hydroxy phosphate Fenton-like ·OH

Evolution and Characterization of Damage of Concrete under Freeze-thaw Cycles

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Journal of Wuhan University of Technology(Materials Science) 2013年第4期28卷 710-714页

作者：王玲 cao yin WANG Zhendi DU Peng State Key Laboratory of Green Building Materials China Building Materials Academy

To study the internal damage of concrete under freeze-thaw cycles, concrete strains were measured using embedded strain gauges. Residual strain and coefficients of freezing expansion （CFE） derived from strain-temperature curves were used to quantify the damage degree. The experimental results show that irreversible residual strain increases with the number of freeze-thaw cycles. After 50 cycles, residual strains of C20 and C35 concretes are 320με and 100με in water, and 120με and 60 με in saline solution, respectively. In lower temperature range （- 10 ℃ to - 25 ℃） CFE of C20 and C35 concretes decrease by 9.82 × 10-6/K and 8.44×10-6/K in water, and 9.38×10-6/K and 5.47×10-6/K in saline solution, respectively. Both residual strains and CFEs indicate that during the first 50 freeze-thaw cycles, the internal damage of concrete in saline solution is less than that of concrete in water. Thus residual strain and CFE can be used to measure the frost damage of concrete.

关键词： freeze-thaw cycles saline solution strain residual strain coefficients of freezing expansion

Hydrogen-bonding Networks in Cocrystal of Melamine and 4-Fluoro-benzoic Acid

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Chemical Research in Chinese Universities 2010年第5期26卷 702-706页

作者： ZHANG Xiu-lian yin Wei cao Man-li Department of Chemistry Guangdong Institute of Education Guangzhou 510310 P R. China

A novel interpenetrating structure [（HMA^＋）（FB^- ）] ·2H2O of melamine（MA） with 4-fluoro-benzoic acid （HFB） was synthesized. It crystallized in the monoclinic system with space group P21/c. The complex has a interpenetrating 2D structure with hydrogen-bonded grid networks. Carboxylic acid to melamine proton transfer occurs in the complex. The adjacent HMA^＋ cations related by an inverse center form cationic [HMA^＋]∞ ribbons via a pair of N-H…N hydrogen bonds. Adjacent FB-anions are paired by C-H…F hydrogen bonds to form dimers, which are connected to [HMA^＋]∞ ribbons through N-H…O interactions. The supramolecular features in the complex are guided by control of strong N-H…N, N-H…O and O-H…O hydrogen bonds, as well as highly directional weak C-H…F interactions and aromatic π-π stacking interactions.

关键词： Hydrogen bond Melamine 4-Fluoro-benzoic acid

Forces Driving Changes in Cultivated Land and Management Countermeasures in the Three Gorges Reservoir Area,China

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Journal of Mountain Science 2013年第1期10卷 149-162页

作者： cao yin-gui BAI Zhong-ke ZHOU Wei WANG Jing School of Land Science and Technology China University of Geosciences Key Laboratory of Land Reconsolidation and Rehabilitation Ministry of Land and Resources Key Laboratory of Land Use Ministry of Land and Resources

The Three Gorges project accelerates economic development in the Three Gorges Reservoir *** paper aimed to investigate the distribution,changes and features of cultivated land in this area,analyze the forces driving the changes in cultivated land area,and propose the countermeasures for cultivated land *** matrix was used to analyze the features of cultivated land changes,and quantitative analysis and qualitative analysis were adopted to research the driving forces according to the features of cultivated land *** land in the Three Gorges Reservoir Area mainly lay to the northwest of the Yangtze River,especially the upper *** areas of cultivated land increased from 1996 to 1999,then decreased from 2000 to 2006,and finally increased again from 2007 to *** important forces driving changes in cultivated land included government policies,employment and food security,increasing construction land,agriculture structure adjustment,land rearrangement,*** cultivated land management,firstly,it is necessary to insist on the principle of cultivated land protection,standardize land exploitation and strictly restrict the transformation of cultivated land into non-farming ***,land rearrangement must be implemented,which can not only increase the area of the cultivated land,but also improve the quality of the cultivated ***,it is feasible to intensify eco-agriculture construction to increase the quantity and quality of cultivated ***,it is helpful to improve the traditional agriculture production methods to promote cultivated land ***,it is important to propagandize cultivated land protection and realize the enormous pressure of cultivated land shortage,making more people obligated to protect cultivated land.

关键词： Land use change Driving force Management countermeasure Cultivated land Three Gorges Reservoir Area

A Depth Video Coding In-Loop Median Filter Based on Joint Weighted Sparse Representation

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Wuhan University Journal of Natural Sciences 2016年第4期21卷 351-357页

作者： Lü Haitao yin cao CUI Zongmin HU Jinhui School of Information Science and Technology Jiujiang University National Engineering Research Center for Multimedia Software/School of Computer Wuhan University

The existing depth video coding algorithms are generally based on in-loop depth filters, whose performance are unstable and easily affected by the outliers. In this paper, we design a joint weighted sparse representation-based median filter as the in-loop filter in depth video codec. It constructs depth candidate set which contains relevant neighboring depth pixel based on depth and intensity similarity weighted sparse coding, then the median operation is performed on this set to select a neighboring depth pixel as the result of the filtering. The experimental results indicate that the depth bitrate is reduced by about 9% compared with anchor method. It is confirmed that the proposed method is more effective in reducing the required depth bitrates for a given synthesis quality level.

关键词： depth video coding virtual view synthesis joint weighted sparse representation

Preoperative inflammation-based markers predict early and late recurrence of hepatocellular carcinoma after curative hepatectomy

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Hepatobiliary & Pancreatic Diseases International 2016年第3期15卷 266-274页

作者： Yue Liu Zhong-Xia Wang yin cao Guang Zhang Wei-Bo Chen Chun-Ping Jiang Department of Hepatobiliary Surgery the Affiliated Drum Tower Hospital of Nanjing University Medical School

BACKGROUND： Recurrence of hepatocellular carcinoma （HCC） after curative resection remains a major cause of treatment failure and tumor-related death. Patterns of HCC recur- rence can be categorized into early recurrence and late recurrence which have different underlying mechanisms. In this study, we investigated if simple inflammation-based clinical markers can distinguish patterns of recurrence after curative resection of HCC.

关键词： hepatocellular carcinoma inflammation prognosis recurrence hepatectomy

Inducement of Sechenov inhibition by EtOH and NA in the Bufo toad

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Chinese Science Bulletin 2008年第8期53卷 1193-1196页

作者： LI RuXin JIA ShanShan LI yingZi cao yin CHENG XiuZhen XIE ZuoPing Department of Biological Sciences and Biotechnology National State Key Laboratory of Biomembrane and Membrane Biotechnology Tsinghua University Beijing 100084 China Department of Physiology Weifang Medical University Weifang 261042 China

Central inhibition, discovered by Sechenov in 1862, suggests that electrically stimulating the forebrain or medulla oblongata in frog generally suppresses reflexes. However, the underlying molecular mechanisms are still unclear. Using ethanol (EtOH), noradrenalin (NA), and other neurotransmitters in thalamic preparations, Sechenov inhibition was stimulated in Bufo toads in this study. The result showed that, similar to Sechenov inhibition, the acute application of EtOH or NA excited the thalamus and prolonged the latency of withdrawal reflex. Our study evidences the involvement of α-adrenoceptors in such central inhibition, and explains the role of acute EtOH application in the in- duction of reflex inhibition.

关键词：乙醇去甲肾上腺素抑制作用 NA 蟾蜍

Preoperative serum liver enzyme markers for predicting early recurrence after curative resection of hepatocellular carcinoma

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Hepatobiliary & Pancreatic Diseases International 2015年第2期14卷 178-185页

作者： Zhong-Xia Wang Chun-Ping Jiang yin cao Guang Zhang Wei-Bo Chen Yi-Tao Ding Department of Hepatobiliary Surgery the Affiliated Drum Tower Hospital of Nanjing University Medical School Department of Hepatobili-ary Surgery Nanjing Drum Tower Hospital Clinical Medical College of Nanjing Medical University Department of Hepatobiliary Surgery Nanjing Drum Tower Hospital Clinical Medical College of Nanjing Medical University

BACKGROUND：Early recurrence of hepatocellular carcinoma（HCC）is associated with worse prognosis after liver resection This study aimed to investigate the prognostic value of com mon liver enzyme markers in HCC early recurrence after cu rative hepatectomy and to establish a simple predictive model for HCC early ***： A total of 200 patients who had undergone curative resection for HCC were retrospectively analyzed. The patients were divided into early recurrence （within 2 years） and non-early recurrence groups. Demographical characteristics, preopera- tive liver function parameters, surgical factors and tumor related factors of the patients were assessed by univariate analysis to identify potential significant predictors for early recurrence after resection of HCC. Parameters with statisti- cal significance were entered into a Cox proportional hazard model to find independent risk factors. Receiver operating characteristic analysis was done to determine optimal cut-off values and the number of combined factors in multi-factor predictive model. RESULTS： Of 13 potential risk factors for early recurrence identified by univariate analysis, high lactate dehydrogenase （LDH〉206 U/L, HR=1.711, P=0.006）, high aspartate aminotransferase （AST）/alanine aminotransferase （ALT） ratio （AST/ ALT〉0.96, HR=1.769, P=0.006）, elevated alpha-fetoprotein （AFP〉8.6 ng/mL, HR=2.079, P=0.007）, small resection margin （〈1 cm, HR=2.354, P〈0.001） and advanced TNM stage （TNM III-IV, HR=2.164, P〈0.001） were independent risk factors for early recurrence of HCC shown by multivariate analysis. Patients with three or more concurrent independent risk factors had significantly higher risk for early recurrence than those with low risk factors. The sensitivity and specificity of this predictive model are 53.6% and 80.7%, respectively （area under curve=0.741, 95% CI 0.674-0.800, P〈0.0001）. CONCLUSIONS： Preoperative common fiver enzyme markers, LDH and AST/ALT ratio, were independently associated

关键词： hepatocellular carcinoma liver enzyme recurrence resection hepatectomy

From the Punjab to the Bund： Sikh Policemen in Motion

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World History Studies 2015年第1期2卷 60-84页

作者： cao yin History Department National University of Singapore

Studies on colonial history have long been trapped either by the binaryframework of the imperial history or by the linear narrative of thenational history. However, the past of transnational subjects such as theSikh policemen in Southeast and East Asia cannot be properly studiedin both paradigms. This article tries to reconstruct the experience ofthose overseas Sikh servicemen by employing a transnational *** connecting the colonial rule in India with what happened inSingapore, Hong Kong and Shanghai in the late nineteenth and earlytwentieth centuries, this paper examines how the mechanism of acolonial network shaped the birth and development of the Sikh policeunits in different colonies and settlements.

关键词： Sikh Policemen, British Empire, Hong Kong, Singapore, Shanghai