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Aliphatic biomarker signatures of early Oligocene-early Miocene source rocks in the central Qiongdongnan Basin:Source analyses of organic matter

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Acta Oceanologica Sinica 2023年第3期42卷 1-18页

作者： Min xu Dujie Hou Xiong Cheng Jun Gan xinde xu Gang Liang Wenjing Ding School of Energy Resources China University of GeosciencesBeijing 100083China Key Laboratory of Marine Reservoir Evolution and Hydrocarbon Accumulation Mechanism Ministry of EducationBeijing 100083China Beijing Key Laboratory of Unconventional Natural Gas Geological Evaluation and Development Engineering Beijing 100083China Exploration and Development Resource Institute Hainan Branch of China National Offshore Oil CorporationHainan 570300China China National Offshore Oil Corporation(CNOOC)Research Institute Co. Ltd.Beijing 100028China

The geochemical signatures of fifty-four rock samples and three supplementary drill stem test(DST)oils from the Yacheng-Sanya formations in the central Qiongdongnan Basin(CQB)were analysed.Reconstruction of the early Oligocene-early Miocene(36–16 Ma)palaeovegetation and source analyses of organic matter(OM)were conducted using aliphatic biomarkers in ancient sediments and DST oils.Both the interpreted aquatic and terrigenous OM contributed to the CQB source rocks(SRs)but had varying relative proportions.The four distribution patterns derived from n-alkanes,terpanes,and steranes are representative of four OM composition models of the Yacheng-Sanya SRs,including model A,model B,model C,and model D,which were classified based on the increasing contribution from terrigenous OM relative to aquatic OM.Some terrigenous higher plantderived biomarkers,including oleanane,des-A-oleanane,C_(29)ααα20R sterane,bicadinanes,the C_(19)/(C_(19)+C_(23))tricyclic terpane ratio,and other n-alkane-derived ratios suggest that angiosperms had increased proportions in the palaeoflora from early Oligocene to early Miocene,and the bloom of terrigenous higher plants was observed during deposition of upper Lingshui Formation to lower Sanya Formation.These findings are consistent with the incremental total organic carbon and free hydrocarbons+potential hydrocarbons(S_1+S_2)in the lower Lingshuilower Sanya strata with a significant enrichment of OM in the E_3l_1-N_1s_2 shales.The maturity-and environmentsensitive aliphatic parameters of the CQB SRs and DST oils suggest that all the samples have predominantly reached their early oil-generation windows but have not exceeded the peak oil windows,except for some immature Sanya Formation shales.In addition,most of the OM in the analysed samples was characterised by mixed OM contributions under anoxic to sub-anoxic conditions.Furthermore,terrestrial-dominant SRs were interpreted to have developed mainly in the Lingshui-Sanya formations and were deposited in sub-oxic to oxic environments,compared to

关键词： aliphatic biomarkers early Oligocene-early Miocene organic matter sources palaeovegetation reconstruction Qiongdongnan Basin

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Experimental Simulation Study of the Dominant Enrichment Area of Terrestrial Organic Matter in the Shallow-Delta Sedimentary System of the Yacheng Formation in the Qiongdongnan Basin

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Acta Geologica Sinica(English Edition) 2022年第5期96卷 1693-1703页

作者： xu xinde YANG Xibing QU Tong GAO Gang LIANG Gang LI Xing CNOOC China Limited Zhanjiang BranchZhanjiangGuangdong 524057China State Key Laboratory of Petroleum Resources and Prospecting China’s University of PetroleumBeijing 102249China College of Geosciences China’s University of PetroleumBeijing 102249China CNOOC China Limited Hainan BranchHaikou 570312China

Shallow-delta sedimentary systems receive both terrestrial and marine organic matter. As oil and gas exploration activities determine that the source rocks of the deep-water area of the Qiongdongnan Basin, northern South China Sea, are generally rich in and even dominated by terrestrial organic matter, this has led many researchers to examine the rules governing terrestrial organic matter enrichment in shallow-delta sea sedimentary systems. However, the deep burial of source rocks in deep-water areas and the relatively small amount of drilling undertaken have greatly restricted the study of these rules. In this study, the ‘forward modeling' research method was used to observe and analyze the deposition and preservation of terrestrial organic matter through flume experiments, where the depositional results were carefully depicted and sampled. The total organic carbon content of selected samples was measured and when combined with qualitative observations and quantitative comparison results, the dominant enrichment areas of terrestrial organic matter were identified. The experimental results show that the overbank parts of the delta front, the dune countercurrent surface, the low-lying parts, the delta front slope area and the shallow-prodelta sea area are where terrestrial organic matter is predominantly enriched. This provides an important basis and guidance for the prediction of the development areas of marine source rocks with terrestrial input in the deep-water areas of the Qiongdongnan Basin.

关键词： shallow-delta sea sedimentary system deep water area terrestrial organic matter flume experiment enrichment area Qiongdongnan Basin

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Deep learning and network analysis: Classifying and visualizing geologic hazard reports

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Journal of Earth Science 2021年

作者： Wenjia Li Liang Wu xinde xu Zhong Xie Qinjun Qiu Hao Liu Zhen Huang Jianguo Chen National Engineering Research Center for GIS School of Geography and Information Engineering， China University of Geosciences Wuhan Geomatics Institute Faculty of Earth Resources， China University of Geosciences

If progress is to be made toward improving geohazard management and emergency decision-making， then lessons need to be learned from past geohazard information. A geologic hazard report provides a useful and reliable source of information about the occurrence of an event， along with detailed information about the condition or factors of the geohazard. Analyzing such reports， however， can be a challenging process because these texts are often presented in unstructured long text formats， and contain rich specialized and detailed information. Automatically text classification is commonly used to mine disaster text data in open domains (e.g.， news and microblogs). But it has limitations to performing contextual long-distance dependencies and is insensitive to discourse order. These deficiencies are most obviously exposed in long text fields. Therefore， this paper uses the bidirectional encoder representations from Transformers (BERT)， to model long text. Then， utilizing a softmax layer to automatically extract text features and classify geohazards without manual features. The latent Dirichlet allocation (LDA) model is used to examine the interdependencies that exist between causal variables to visualize geohazards. The proposed method is useful in enabling the machine-assisted interpretation of text-based geohazards. Moreover， it can help users visualize causes， processes， and other geohazards and assist decision-makers in emergency responses.

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北部湾盆地油气成藏规律与勘探新领域、新类型、资源潜力

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石油学报 2024年第1期45卷 202-225页

作者：邓勇胡德胜朱继田刘国昌陈奎童传新张道军徐新德满勇游君君满晓吴云鹏周刚张建新油气资源与工程全国重点实验室中国石油大学(北京)北京102249 中海石油(中国)有限公司湛江分公司广东湛江524057

北部湾盆地是南海西部海域重要的原油勘探区和产区,具备多凹陷含油、多层系成藏、多种油气成藏模式等优势成藏条件,近年来在页岩油、潜山、岩性、深层油气、后备凹陷/洼陷等新领域、新类型油气勘探中取得了突破。为了落实北部湾盆地重... 详细信息

北部湾盆地是南海西部海域重要的原油勘探区和产区,具备多凹陷含油、多层系成藏、多种油气成藏模式等优势成藏条件,近年来在页岩油、潜山、岩性、深层油气、后备凹陷/洼陷等新领域、新类型油气勘探中取得了突破。为了落实北部湾盆地重要生烃凹陷的区域成藏规律,指导后续常规油气精细勘探开发及新领域、新类型油气勘探,对区域石油地质条件开展了研究,总结了成藏规律。研究结果表明,多期构造运动控制了北部湾盆地的构造演化和物质充填;古近系始新统流沙港组二段油页岩和半深湖亚相泥岩为盆地最重要的烃源岩,此外,在流沙港组三段、流沙港组一段、涠洲组二段也发育多套烃源岩;发育潜山储层和碎屑岩储层,形成了多源、多储、多盖的格局;凹陷区原生近源成藏、凹中断裂带/断隆带/陡坡带垂向成藏、斜坡区过路成藏、凸起/隆起区汇流成藏等多种成藏模式控制了北部湾盆地的多凹陷成藏;油气在多凹多带有序分布,油气的差异聚集控制了内气外油、深气浅油的油气分布特征,不同区带内的油气藏类型差异显著。在区域石油地质条件与成藏规律的指导下,从资源潜力、成藏条件、勘探开发程度综合分析,页岩油、潜山、岩性圈闭、深层油气、后备凹陷/洼陷是北部湾盆地未来勘探开发的重要领域。

关键词：北部湾盆地新领域新类型成藏条件资源潜力

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黑曲霉尿苷/尿嘧啶营养缺陷型转化系统的构建及应用

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浙江工业大学学报 2024年第1期52卷 105-111页

作者：王小平宋问张霏刘燕王升帆邵东梁玲玲许新德郑建永浙江可明生物医药有限公司浙江新昌312500 浙江工业大学生物工程学院浙江杭州310014 浙江医药股份有限公司新昌制药厂浙江新昌312500

黑曲霉(Aspergillus niger)是一种重要的工业发酵菌株,它具有强大的蛋白分泌表达能力。为了提高黑曲霉遗传操作效率及优化重组菌株的筛选策略,构建以尿苷/尿嘧啶营养缺陷型为筛选标记的转化系统。利用CRISPR/Cas9技术实现pyrG基因的敲除... 详细信息

黑曲霉(Aspergillus niger)是一种重要的工业发酵菌株,它具有强大的蛋白分泌表达能力。为了提高黑曲霉遗传操作效率及优化重组菌株的筛选策略,构建以尿苷/尿嘧啶营养缺陷型为筛选标记的转化系统。利用CRISPR/Cas9技术实现pyrG基因的敲除,在含有尿嘧啶核苷和5-氟乳清酸(5-FOA)的抗性培养基中筛选表型正确的转化子。经基因组PCR验证,黑曲霉营养缺陷型菌株可稳定遗传。利用该转化系统可成功实现增强型绿色荧光蛋白在黑曲霉中的表达。通过结合增强型绿色荧光蛋白和流式细胞仪建立了黑曲霉转化子的高通量筛选模型。

关键词：黑曲霉 CRISPR/Cas9 基因敲除尿嘧啶营养缺陷型增强型绿色荧光蛋白(EGFP)

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多重包埋技术在微囊化姜黄素中的应用

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中国食品添加剂 2024年第3期35卷 188-194页

作者：周迪王永奇许新德白亚龙姚可欣商景天浙江医药股份有限公司新昌制药厂绍兴312500

姜黄素较差的溶解性和对氧化的高度敏感性,使其存在很大的应用局限,为此对多重包埋技术在微囊化姜黄素中的应用进行了研究。通过单因素试验,分析溶剂类别、溶解温度和时间以及油相蠕动泵频率、真空乳化机转速等因素对微囊化姜黄素产品... 详细信息

姜黄素较差的溶解性和对氧化的高度敏感性,使其存在很大的应用局限,为此对多重包埋技术在微囊化姜黄素中的应用进行了研究。通过单因素试验,分析溶剂类别、溶解温度和时间以及油相蠕动泵频率、真空乳化机转速等因素对微囊化姜黄素产品的影响,确定了姜黄素最佳溶解工艺条件和一次包埋工艺条件;然后通过正交实验分析,针对产品感观质量和稳定性等因素,确定了合理的多重包埋技术微囊化姜黄素10%冷水溶性(Cold Water Solubility,CWS)产品配方。结果表明:最佳工艺条件是以丙酮作溶剂,溶解温度55℃、时间少于45 min,蠕动泵频率20 Hz,真空乳化机转速控制在15000 r/min;产品配方为12%姜黄素、25%聚乙二醇6000、3.5%吐温-60、35%辛烯基琥珀酸淀粉钠、4.5%dl-α生育酚、20%玉米淀粉。此项技术的应用很大程度上提高了姜黄素的水溶性、稳定性与生物利用度,拓宽了其应用范围和领域。

关键词：姜黄素壁材纳米分散微胶囊多重包埋

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Petroleum Origins and Accumulation Patterns in the Weixinan Sag in the Beibu Gulf Basin,Using Subsag B as an Example

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Acta Geologica Sinica(English Edition) 2020年第5期94卷 1515-1530页

作者： GAO Gang xu xinde QU Tong GAN Jun DANG Wenlong ZHOU Xiaoxiao LIU Fengyan School of Geosciences Chinese University of PetroleumBeijing 102249China State Key Laboratory of Petroleum Resource and Prospecting Chinese University of PetroleumBeijing 102249China Research Institute of Zhanjiang Branch of CNOOC Ltd.Zhanjiang Guangdong 524057China Exploration&Development Research Institute Petro China Huabei Oilfield CompanyRenqiuHebei 062552China

Crude oil has been discovered in the Paleogene and Neogene units of the Weixinan Sag in the Beibu Gulf Basin.To determine the source and accumulation mode of this crude oil,12 crude oil samples and 27 source rock samples were collected and an extensive organic geochemical analysis was conducted on them.Based on the geological conditions and the analytical results,the types,origins and accumulation patterns of crude oil in the study area were elucidated.Except for a shallowly-buried and biodegraded crude oil deposit in Neogene rocks,the crude oil samples in the study area were normal.All of the crude oils were derived from lacustrine source rocks.According to biomarker compositions,the crude oils could be divided into two families,A and B,distinctions that were reinforced by differences in carbon isotope composition and spatial distribution.Oil-source correlation analysis based on biomarkers revealed that Family A oils were derived from the mature oil shale at the bottom of the second member of the Liushagang Formation,while the Family B oils formed in the mature shale of the Liushagang Formation.The Family A oils,generated by oil shale,mainly migrated laterally along sand bodies and were then redistributed in adjacent reservoirs above and below the oil shale layer,as well as in shallow layers at high structural positions,occupying a wide distribution range.The Family B oils were generated by other shale units before migrating vertically along faults to form reservoirs nearby,resulting in a narrow distribution range.

关键词： crude oil family oil shale shale petroleum migration Weixinan Sag Beibu Gulf Basin

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Measurement and Influence Factors of the Flowability of Microcapsules with High-content β-Carotene

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Chinese Journal of Chemical Engineering 2007年第4期15卷 579-585页

作者：许新德姚善泾韩宁邵斌 Department of Chemical and Biochemical Engineering Zhejiang University Hangzhou 310027 China Xinchang Pharma. Factory Zhejiang Medical Co. Ltd. Xinchang 312500 China

The flowability of five kinds of microencapsulation powders,with differentβ-carotene contents and by two alternative particle-forming technologies i.***.spray-drying and starch-catching beadlet technology,was meas- ured.The actual flow properties of the five powders were compared based on bin-flow test,and three flow indexes (Hausner ratio,repose angle and flow index)were measured.It was found that the repose angle is the most suitable index to reflect the flowability of these powders for the particle properties would not be altered due to compaction or tapping during the measuring process.Particle size and particle size distribution play most important roles in the flowability of these granular materials,which was also influenced by other factors like shape,surface texture,sur- face roughness,etc.Microcapsules with wall material of gelatin and a layer of modified starch absorbed on the sur- face showed excellent flowabilities and good mechanical properties,and they are favorable for tabletting to supply β-carotene.

关键词：微囊剂粉体流动性胡萝卜素B 豪斯纳尔理论静安息角

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Meso-Zeaxanthin:One of Important Carotenoids for Human Health

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Journal of Northeast Agricultural University(English Edition) 2010年第3期17卷 76-81页

作者： xu xinde JIANG Lianzhou ZHANG Lihua SHAO Bin Zhejiang Medicine Co. Ltd. Xinchang Pharmaceutical Factory Xinchang 312500 Zhejiang China College of Food Sciences Northeast Agricultural University Harbin 150030 China

As one of optical isomers of zeaxanthin, meso-zeaxanthin is an important ingredient of macular pigment. Compared with lutein and zeaxanthin, meso-zeaxanthin may display strong functions as antioxidant and filtering short-wavelength, for example, the blue light. Comparisons among lutein, zeaxanthin and meso-zeaxanthin as well as functions and distributions together with the source of meso-zeaxanthin were discussed. The application as a supplement of diet and issues should be studied in the future for mesozeaxanthin were also analyzed.

关键词： meso-zeaxanthin function distribution source application

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三角洲—浅海沉积体系泥质沉积规律模拟实验——以琼东南盆地崖南凹陷为例

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岩性油气藏 2022年第1期34卷 24-33页

作者：屈童高岗徐新德王瑞甘军梁刚游君君中国石油大学(北京)油气资源与探测国家重点实验室北京102249 中国石油大学(北京)地球科学学院北京102249 中海石油(中国)有限公司湛江分公司广东湛江524057

三角洲—浅海沉积体系由于同时具有陆源有机及海洋有机质备受众多学者的关注,近年来南海地区油气勘探实践表明崖城组陆源海相泥岩是油气生成的重要来源之一,但由于深水区烃源岩埋深较大、现有钻井较少,极大地限制了该地区烃源岩研究与... 详细信息

三角洲—浅海沉积体系由于同时具有陆源有机及海洋有机质备受众多学者的关注,近年来南海地区油气勘探实践表明崖城组陆源海相泥岩是油气生成的重要来源之一,但由于深水区烃源岩埋深较大、现有钻井较少,极大地限制了该地区烃源岩研究与勘探进展。为了对泥质沉积物沉积与分布规律进行研究,本文以琼东南盆地崖南凹陷崖城组地质背景为基础,设计沉积模拟实验,对沉积物沉积过程进行观察,并对沉积体进行取样,测定样品粒度组成,结合定性观察与定量对比,对三角洲—浅海沉积体系泥质沉积物的沉积规律进行探究,对陆源海相烃源岩的优势发育部位进行揭示。研究结果表明,由物源向浅海方向,沉积物的泥质含量呈整体增大的趋势,在三角洲前缘斜坡处由于水动力条件的骤降出现突增,但沉积物的总量呈先增大后减小的趋势,使得泥质沉积物的总量向深水方向呈减少趋势;三角洲前缘斜坡—浅海沉积范围是泥岩发育的优势区域,在三角洲沉积体内局部低地势、弱水动力条件的部位也可沉积并保存泥质沉积物;地形坡度的增大有利于泥质沉积物向深水区搬运。三角洲前缘—浅海区是泥质沉积物堆积的主要部位,即近海盆地的近岸地区,这对琼东南盆地深水区陆源海相烃源岩优势发育部位的预测提供了重要依据与指导。

关键词：三角洲—浅海沉积体系陆源海相烃源岩泥质沉积物沉积模拟实验优势发育区琼东南盆地

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