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Journal of Materials Science & Technology 2022年第33期128卷 22-30页

作者： Weizong Bao Jie Chen guoqiang xie School of Materials Science and Engineering Harbin Institute of Technology(Shenzhen)Shenzhen 518055China State Key Laboratory of Advanced Welding and Joining Harbin Institute of TechnologyHarbin 150001China

A superiority in interfacial bonding is favorable to fabricate high-strength conductive composites for electrical contact *** the present work,high strength and high conductivity multi-scale metallic glass composites(including micron-scale Cu Zr Al metallic glass reinforcement,hundred-nanometer-scale Cu Cr Zr crystalline grain matrix,and nano-scale precipitated phase)were fabricated by a one-step spark plasma sintering(SPS).The strength and conductivity of the bulk copper matrix metallic glass composites(BCMGCs)were enhanced simultaneously with the increase in the sintering pressure of the *** excellent performance is attributed to the improved interfacial bonding between the metallic glass reinforcement and the copper alloy matrix due to the high pressure assisted by temperature and pulsed *** particular,the precipitation of nanoprecipitates at the interface further reduces the interfacial resistance and improves the mechanical properties of the *** work broadens the horizon for the selection and optimization of reinforcements and manufacturing processes for high-performance electrical contact materials(ECMs).

关键词： CuZrAl metallic glass Spark plasma sintering Mechanical properties Electrical performance

Dual phase equal-atomic NbTaTiZr high-entropy alloy with ultra-fine grain and excellent mechanical properties fabricated by spark plasma sintering

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Journal of Materials Science & Technology 2021年第31期90卷 150-158页

作者： Tao Xiang Zeyun Cai Peng Du Kun Li Zongwei Zhang guoqiang xie School of Materials Science and Engineering Harbin Institute of Technology(Shenzhen)Shenzhen 518055China

Super-high strength NbTaTiZr high-entropy alloys(NbTaTiZr HEAs)have been successfully fabricated by the mechanical alloying(MA)with spark plasma sintering(SPS)technology,which is 2-fold compared with that of NbTaTiZr HEAs prepared by vacuum arc melting(VAM).After the SPS process,the bulk NbTaTiZr alloy samples are provided with dual-phase body-centered cubic(BCC)structure and nanoscale grain size about 500 nm that is obviously smaller than that of NbTaTiZr HEA fabricated by *** the sintering temperature is 800℃,the compressive fracture strength is the highest reaching at 2511±78 *** the sintering temperature is 1000℃,the fracture strain is the highest reaching at 12.8%,and compressive fracture strength and yield strength also reach at 2274±91 MPa and 2172±47 MPa,*** excellent mechanical properties of bulk NbTaTiZr alloy samples are attributed to the merits of MA and SPS,and the collaboration effect of ultra-fine grains strengthening,solid solution strengthening and interstitial solid solution strengthening.

关键词： NbTaTiZr high-entropy alloys Mechanical alloying Ultra-fine grain Spark plasma sintering Mechanical properties Corrosion behavior

Fabrication of porous TiZrNbTa high-entropy alloys/Ti composite with high strength and low Young’s modulus using a novel MgO space holder

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Journal of Materials Science & Technology 2023年第36期167卷 59-73页

作者： Tao Xiang Jie Chen Weizong Bao Shuyan Zhong Peng Du guoqiang xie School of Materials Science and Engineering Harbin Institute of Technology(Shenzhen)Shenzhen 518055China State Key Laboratory of Advanced Welding and Joining Harbin Institute of TechnologyHarbin 150001China

Stress shielding is caused by the mismatch of stiffness between bone and implant materials,which may give rise to bone resorption and loosening,thereby causing implantation *** is a huge gap between Young’s modulus of human bone and low Young’s modulusβTi alloys.A porous structure design can achieve the target of low Young’s modulus,and thus achieve the matching between human bone and implant ***,a suitable space holder(SH)that can be applied at high temperatures and sintering pressure has not been *** this study,the TiZrNbTa/Ti titanium matrix composite(TMC)with high strength and large ductility was used as scaffold materials and combined the SH technique with the spark plasma sintering(SPS)technique to obtain a porous structure.A novel space holder,i.e.,MgO particles was adopted,which can withstand high-temperature sintering accompanied by a sintering *** porous TiZrNbTa/Ti with 40 vol.%MgO added exhibits a maximum strength of 345.9±10.4 MPa and Young’s modulus of 24.72±0.20 GPa,*** possesses higher strength compared with human bone and matches Young’s modulus of human bone,which exhibits great potential for clinical application.

关键词： TiZrNbTa/Ti titanium matrix composite MgO space holder Low Young’s modulus High strength

Phase-tunable equiatomic and non-equiatomic Ti-Zr-Nb-Tahigh-entropy alloys with ultrahigh strength for metallic biomaterials

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Journal of Materials Science & Technology 2022年第22期117卷 196-206页

作者： Tao Xiang Peng Du Zeyun Cai Kun Li Weizong Bao Xinxin Yang guoqiang xie School of Materials Science and Engineering Harbin Institute of Technology(Shenzhen)Shenzhen 518055China State Key Laboratory of Advanced Welding and Joining Harbin Institute of TechnologyHarbin 150001China

The contradiction between the strength and ductility of metallic materials is a major scientific problemthat has been researched for a long time. Dual-phase equiatomic and non-equiatomic Ti-Zr-Nb-Ta highentropy alloys (HEAs) with super-high strength and excellent ductility have been successfully developedvia mechanical alloying (MA) combined with spark plasma sintering (SPS) technology. This is adjustedby altering the atomic ratios of the different phases. X-ray diffraction (XRD) and transmission electronmicroscopy (TEM) were performed to confirm the dual-phase microstructure. After the SPS process, theaverage grain size of the aforementioned equiatomic Ti_(25)Zr_(25)Nb_(25)Ta_(25) HEAs (134 ± 50 nm) evaluated byelectron back-scattering diffraction (EBSD) is smaller than that of the Ti-Zr-Nb-Ta HEAs (150 μm), whichwere fabricated using arc melting. According to the Hall-Petch formula, the grain boundary strengthening contribution in the Ti-Zr-Nb-Ta system is 33-fold higher than those fabricated using the arc-meltingprocess. When the alloy phase comprises the equivalent dual-phase, equiatomic Ti_(25)Zr_(25)Nb_(25)Ta_(25) HEAshave good comprehensive performance compared to non-equiatomic Ti-Zr-Nb-Ta HEAs prepared usingthe same process. The yield strength of equiatomic Ti_(25)Zr_(25)Nb_(25)Ta_(25) HEAs (2212 ± 38 MPa) is two-foldhigher than that of Ti-Zr-Nb-Ta HEAs (1100 ± 90 MPa) fabricated via arc melting. This can be attributed tothe ultra-fine grain size. Notably, the equiatomic Ti_(25)Zr_(25)Nb_(25)Ta_(25) HEAs possess approximately the samebiocompatibility as commercial pure Ti (CP-Ti), indicating that the equiatomic Ti_(25)Zr_(25)Nb_(25)Ta_(25) HEAs areprovided with a possibility as an advanced biomaterial for the applications of the medical field.

关键词： Equiatomic Nb_(25)Ta_(25)Ti_(25)Zr_(25)HEAs Ultra-fine grain Phase-tunable Mechanical properties Biocompatibility

An Algorithm for Short-Circuit Current Interval in Distribution Networks with Inverter Type Distributed Generation Based on Affine Arithmetic

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Energy Engineering 2024年第7期121卷 1903-1920页

作者： Yan Zhang Bowen Du Benren Pan GuannanWang guoqiang xie Tong Jiang Electric Power Research Institute State Grid Jiangxi Electric Power Co.Ltd.Nanchang330096China School of Electrical and Electronic Engineering North China Electric Power UniversityBeijing102206China

During faults in a distribution network,the output power of a distributed generation(DG)may be ***,the output currents of distributed power sources are also affected by the output power,resulting in uncertainties in the calculation of the short-circuit current at the time of a ***,the impacts of such uncertainties around short-circuit currents will increase with the increase of distributed power ***,it is very important to develop a method for calculating the short-circuit current while considering the uncertainties in a distribution *** this study,an affine arithmetic algorithm for calculating short-circuit current intervals in distribution networks with distributed power sources while considering power fluctuations is *** proposed algorithm includes two *** the first stage,normal operations are considered to establish a conservative interval affine optimization model of injection currents in distributed power *** by the fluctuation range of distributed generation power at the moment of fault occurrence,the model can then be used to solve for the fluctuation range of injected current amplitudes in distributed power *** second stage is implemented after a malfunction *** this stage,an affine optimization model is first *** model is developed to characterizes the short-circuit current interval of a transmission line,and is constrained by the fluctuation range of the injected current amplitude of DG during normal ***,the range of the short-circuit current amplitudes of distribution network lines after a short-circuit fault occurs is *** algorithm proposed in this article obtains an interval range containing accurate results through interval *** with traditional point value calculation methods,interval calculation methods can provide more reliable analysis and calculation *** range of short-circuit current amplitude ob

关键词： Short circuit calculation inverter type distributed power supplies affine arithmetic distribution network

Optimization of mechanical properties and corrosion resistance of Zn-0.4Mn-0.8Li alloy using the hot rolling process

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Journal of Materials Science & Technology 2023年第14期145卷 136-147页

作者： Xinxin Yang Peng Du Kun Li Weizong Bao Tao Xiang Jie Chen Xingjun Liu guoqiang xie School of Materials Science and Engineering Harbin Institute of Technology(Shenzhen)Shenzhen 518055China State Key Laboratory of Advanced Welding and Joining Harbin Institute of TechnologyHarbin 150001China

Zinc-based degradable metals are considered one of the most promising biodegradable materials due to their moderate corrosion rate,excellent mechanical properties,and good *** this work,biodegradable Zn-0.4Mn-0.8Li alloy was fabricated and rolled in multiple passes at different tem *** the hot rolling temperature increases,the grain size of Zn-0.4Mn-0.8Li alloy was found to increase ***,a multi-scale structure with the coexistence of coarse grains and fine grains was *** results demonstrated that the mechanical strength and corrosion resistance were improved by increasing the rolled *** was observed that Zn-0.4Mn-0.8Li alloy with a total reduction of 90%after hot rolling at 325℃ exhibited excellent mechanical and corrosion *** cooperation of multi-scale microstructure and twinning was found to improve the strength and guarantee the duc-tility of Zn-0.4Mn-0.8Li alloy significantly so that the 325℃ hot-rolled Zn-0.4Mn-0.8Li alloy has optimal comprehensive ***,yield strength,ultimate tensile strength,and elongation were found to be 449.7±5.3 MPa,505.1±6.5 MPa,and 40.5%±7.5%,***,Zn-0.4Mn-0.8Li al-loy via 325℃ hot-rolled processes also exhibited excellent corrosion *** corrosion current density and corrosion potential were found to be 8.8×10-5 mA cm^(-2)and−0.929 V,*** preliminary study indicates that Zn-0.4Mn-0.8Li alloy is a promising candidate material for medical de-vice applications.

关键词： Zn-based degradable metal Hot rolling Mechanical property Corrosion behavior

Demonstration of 85%pump depletion and 10-6 noise content in quasi-parametric chirped-pulse amplification

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Light(Science & Applications) 2022年第10期11卷 2406-2414页

作者： Jingui Ma Kainan Xiong Peng Yuan Xiaoniu Tu Jing Wang guoqiang xie Yanqing Zheng Liejia Qian Key Laboratory for Laser Plasmas(MOE) Collaborative Innovation Center of IFSA(CICIFSA)School of Physics and AstronomyShanghai Jiao Tong UniversityShanghai 200240China Shanghai Institute of Ceramics Chinese Academy of SciencesShanghai 201800China School of Material Science and Chemical Engineering Ningbo UniversityNingboZhejiang 315211China Tsung-Dao Lee Institute Shanghai Jiao Tong UniversityShanghai 200240China

Full pump depletion corresponds to the upper limit of the generated signal photons relative to the pump pulse;this allows the highest peak power to be produced in a unit area of ultraintense laser *** practical systems based on optical parametric chirped-pulse amplification,however,the typical pump depletion is only~35%.Here,we report quasi-parametric chirped-pulse amplification(QPCPA)with a specially designed 8-cm-thick Sm∶YCOB crystal that highly dissipates the idler and hence improves pump *** demonstrate 56%QPCPA energy efficiency for an 810-nm signal converted from a 532-nm pump,or equivalently 85%pump *** another advantage,such a record high depletion greatly suppresses the parametric superfluorescence noise in QPCPA to only~1.5×10-6 relative to the amplified signal *** results pave the way to beyond the ten-petawatt peak power of the currently most intense lasers.

关键词： pump pulse depletion

Formation and crystallization behavior of Fe-based amorphous precursors with pre-existingα-Fe nanoparticles-Structure and magnetic properties of high-Cu-content Fe-Si-B-Cu-Nb nanocrystalline alloys

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Journal of Materials Science & Technology 2021年第6期65卷 171-181页

作者： Yanhui Li Xingjie Jia Wei Zhang Yan Zhang guoqiang xie Zhiyong Qiu Junhua Luan Zengbao Jiao Key Laboratory of Materials Modification by Laser Ionand Electron Beams(Ministry of Education)School of Materials Science and EngineeringDalian University of TechnologyDalian 116024China Institute for Materials Research Tohoku UniversitySendai 980-8577Japan School of Materials Science and Engineering Harbin Institute of Technology(Shenzhen)Shenzhen 518055China Center for Advanced Structural Materials Department of Materials Science and EngineeringCity University of Hong KongHong KongChina Department of Mechanical Engineering The Hong Kong Polytechnic UniversityHong KongChina

Structure,crystallization behavior,and magnetic properties of as-quenched and annealed Fe_(81.3)Si_(4)O_(13)Cu_(1.7)(Cu1.7)alloy ribbons and effects of Nb alloying have been ***-dimensional atom probe and transmission electron microscopy analyses reveal that high-number-density Cu-clusters and Pre-existing Nano-sized a-Fe Particles(PN-a-Fe)are coexistence in the melt-spun Cu1.7 amorphous matrix,and the PN-α-Fe form by manners of one-direction adjoining and enveloping the ***-step crystallization behavior associated with growth of the PN-a-Fe and subsequent nucleation and growth of newly-formedα-Fe is found in the primary crystallization stage of the Cu1.7 *** number densities of the Cu-clusters and PN-a-Fe in melt-spun Fe8_(1.3-x)Si_(4)B_(13)Cu_(1.7)Nb_(x)alloys are gradually reduced with enriching of Nb,and a fully amorphous structure forms at 4 at.%Nb,although smaller Cu-clusters still *** annealing,2 at.%Nb coarsens the average size(D_(α-F)e)of theα-Fe grains from 14.0 nm of the Nb-free alloy to 21.6 nm,and 4 at.%Nb refines the D_(α-Fe)to 8.9 *** mechanisms of theα-Fe nucleation and growth during quenching and annealing for the alloys with large quantities of PN-α-Fe as well as after Nb alloying have been discussed,and an annealing-induced oc-Fe growth mechanism in term of the barrier co-contributed by competitive growth among the PN-a-Fe and diffusion-suppression effect of Nb atoms has been proposed.A coercivity(HC)αDα-Fe^(3)correlation has been found for the nanocrystalline alloys,and the permeability is inverse with the H_(C).

关键词： Fe-based nanocrystalline alloy Cu-cluster Pre-existingα-Fe nanoparticle Crystallization behavior Soft magnetic property

Mechanical properties and corrosion resistance of powder metallurgical Mg-Zn-Ca/Fe bulk metal glass composites for biomedical application

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Journal of Materials Science & Technology 2022年第8期103卷 73-83页

作者： Kun Li Luxin Liang Peng Du Zeyun Cai Tao Xiang Hiroyasu Kanetaka Hong Wu guoqiang xie School of Materials Science and Engineering Harbin Institute of Technology(Shenzhen)Shenzhen 518055China State Key Laboratory of Powder Metallurgy Central South UniversityChangsha 410083China Graduate School of Biomedical Engineering Tohoku UniversitySendai980-8579Japan Graduate School of Dentistry Tohoku UniversitySendai 980-8575Japan State Key Laboratory of Advanced Welding and Joining Harbin Institute of TechnologyHarbin 150001China

Magnesium(Mg)alloys can be regarded as the most promising biodegradable implant materials for orthopedic and stent applications due to their good biocompatibility and low Young’s modulus which is near to that of natural ***,its applicability is hindered because it exhibits a high corrosion rate in the physiological *** this work,we fabricated Mg_(66)Zn_(30)Ca_(4)/Fe bulk metallic glass composites via spark plasma sintering(SPS).We studied the influence of different contents of Fe on the properties of the *** results indicated that Fe was uniformly distributed on the surface of Mg_(66)Zn_(30)Ca_(4) metallic glass(MG)as a second phase,which led to an improvement in the corrosion resistance and mechanical *** standard potential of Mg_(66)Zn_(30)Ca_(4)/Fe bulk metallic glass(BMG)composites increased as compared to Mg_(66)Zn_(30)Ca_(4),while their mechanical strength improved from 355 MPa to 616 ***,cytotoxicity was investigated via the CCK-8 assay and calcein-AM staining,which revealed that the extraction mediums diluted 6 times(EM×6)of the Mg_(66)Zn_(30)Ca_(4) and Mg_(66)Zn_(30)Ca_(4)/Fe did not cause cell toxicity on day 3 and 5,while the EM×6 of the Mg_(66)Zn_(30)Ca_(4) showed cytotoxicity on day 1,3 and ***,Mg_(66)Zn_(30)Ca_(4)/Fe BMG composites exhibit significant potential for fabricating implants with good mechanical strength and corrosion resistance.

关键词： Mg_(66)Zn_(30)Ca_(4)/Fe bulk metallic glass composites Spark plasma sintering Corrosion behaviour Mechanical strength

Toward 5.2μm terawatt few-cycle pulses via optical parametric chirped-pulse amplification with oxide La3Ga5.5Nb0.5O14crystals

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High Power Laser Science and Engineering 2019年第4期7卷 21-32页

作者： Jinsheng Liu Jingui Ma Jing Wang Peng Yuan guoqiang xie Liejia Qian Key Laboratory for Laser Plasmas(Ministry of Education) Collaborative Innovation Centre of IFSA(CICIFSA)School of Physics and AstronomyShanghai Jiao Tong UniversityShanghai 200240China Tsung-Dao Lee Institute Shanghai Jiao Tong UniversityShanghai 200240China

High-power femtosecond lasers beyond 5μm are attractive for strong-field physics with mid-infrared(IR)fields but are difficult to scale *** optical parametric chirped-pulse amplification(OPCPA)at mid-IR wavelengths,a nonlinear crystal is vital,and its transmittance,dispersion,nonlinear coefficient and size determine the achievable power and *** beyond 5μm routinely relies on semiconductor crystals because common oxide crystals are not transparent in this spectral ***,the small size and low damage threshold of semiconductor crystals fundamentally limit the peak power to *** this paper,we design a terawatt-class OPCPA system at 5.2μm based on a new kind of oxide crystal of La3Ga5.5Nb0.5O14(LGN).The extended transparent range,high damage threshold,superior phase-matching characteristics and large size of LGN enable the generation of 0.13 TW seven-cycle pulses at5.2μ*** design fully relies on the state-of-the-art OPCPA technology of an octave-spanning ultrafast Ti:sapphire laser and a thin-disk Yb:YAG laser,offering the performance characteristics of high power,a high repetition rate and a stable carrier-envelope phase.

关键词： few-cycle mid-infrared OPCPA oxide LGN crystals