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MXene Hybridized Polymer with Enhanced Electromagnetic Energy Harvest for Sensitized Microwave Actuation and Self‑Powered Motion Sensing

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Nano-Micro Letters 2025年第3期17卷 265-279页

作者： Yu‑ze Wang Yu‑Chang Wang ting‑ting Liu Quan‑Liang zhao Chen‑Sha Li Mao‑Sheng Cao School of Materials Science and Engineering Beijing Institute of TechnologyBeijing 100081People’s Republic of China School of Materials Science and Engineering Peking UniversityBeijing 100871People’s Republic of China School of Mechanical and Material Engineering North China University of TechnologyBeijing 100144People’s Republic of China Key Laboratory of Functional Inorganic Material Chemistry Ministry of Education of the People’s Republic of ChinaHeilongjiang UniversityHarbin 150080People’s Republic of China

Polymeric microwave actuators combining tissue-like softness with programmablemicrowave-responsive deformation hold great promise for mobile intelligentdevices and bionic soft robots. However, their application is challenged by restricted electromagneticsensitivity and intricate sensing coupling. In this study, a sensitized polymericmicrowave actuator is fabricated by hybridizing a liquid crystal polymer with Ti3C2Tx(MXene). Compared to the initial counterpart, the hybrid polymer exhibits unique spacechargepolarization and interfacial polarization, resulting in significant improvements of230% in the dielectric loss factor and 830% in the apparent efficiency of electromagneticenergy harvest. The sensitized microwave actuation demonstrates as the shortenedresponse time of nearly 10 s, which is merely 13% of that for the initial shape memory polymer. Moreover, the ultra-low content of MXene (upto 0.15 wt%) benefits for maintaining the actuation potential of the hybrid polymer. An innovative self-powered sensing prototype that combinesdriving and piezoelectric polymers is developed, which generates real-time electric potential feedback (open-circuit potential of ~ 3 mV) duringactuation. The polarization-dominant energy conversion mechanism observed in the MXene-polymer hybrid structure furnishes a new approachfor developing efficient electromagnetic dissipative structures and shows potential for advancing polymeric electromagnetic intelligent devices.

关键词： Microwave absorption Electromagnetic response Energy harvest Self-sensing Soft actuator

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Direct Photolithography of WO_(x)Nanoparticles for High‑Resolution Non‑Emissive Displays

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Nano-Micro Letters 2025年第3期17卷 297-309页

作者： Chang Gu Guojian Yang Wenxuan Wang Aiyan Shi Wenjuan Fang Lei Qian Xiaofei Hu ting.z.ang Chaoyu Xiang Yu‑Mo zhang Laboratory of Optoelectronic Information Technology and Devices Ningbo Institute of Materials Technology and EngineeringChinese Academy of SciencesNingbo 315201People’s Republic of China Hangzhou Bay Laboratory of Advanced Nano‑Optoelectronic Materials and Devices Qianwan Institute of CNITECHNingbo 315336People’s Republic of China Smart Materials for Architecture Research Lab Innovation Center of Yangtze River DeltaZhejiang UniversityJiaxing 314100People’s Republic of China University of Science and Technology of China Hefei 230026People’s Republic of China State Key Lab of Supramolecular Structure and Materials College of ChemistryJilin UniversityChangchun 130012People’s Republic of China

High-resolution non-emissive displays based on electrochromic tungsten oxides(WOx)are crucial for future near-eye virtual/augmented reality interactions,given their impressive attributes such as high environmental stability,ideal outdoor readability,and low energy ***,the limited intrinsic structure of inorganic materials has presented a significant challenge in achieving precise patterning/pixelation at the micron ***,we successfully developed the direct photolithography for WOx nanoparticles based on in situ photo-induced ligand *** strategy enabled us to achieve ultra-high resolution efficiently(line widthting device exhibited impressive electrochromic performance,such as fast response(3600 cycles),as well as promising applications in electronic logos,pixelated displays,flexible electronics,*** success and advancements presented here are expected to inspire and accelerate research and development(R&D)in high-resolution non-emissive displays and other ultra-fine micro-electronics.

关键词： Electrochromic Direct photolithography WOx nanoparticles In situ photo-induced ligand exchange High-resolution displays

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Endoplasmic reticulum stress and autophagy in cerebral ischemia/reperfusion injury:PERK as a potential target for intervention

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Neural Regeneration Research 2025年第5期20卷 1455-1466页

作者： Ju zheng Yixin Li ting.z.ang Yanlin Fu Peiyan Long Xiao Gao zhengwei Wang zhizhong Guan Xiaolan Qi Wei Hong Yan Xiao Key Laboratory of Endemic and Ethnic Diseases Ministry of Education&Key Laboratory of Medical Molecular Biology of Guizhou ProvinceGuizhou Medical UniversityGuiyangGuizhou ProvinceChina Guizhou Center for Disease Control and Prevention GuiyangGuizhou ProvinceChina Department of Histology and Embryology Guizhou Medical UniversityGuiyangGuizhou ProvinceChina Collaborative Innovation Center for Prevention and Control of Endemic and Ethnic Regional Diseases Co-constructed by the Province and Ministry GuiyangGuizhou ProvinceChina

Several studies have shown that activation of unfolded protein response and endoplasmic reticulum(ER)stress plays a crucial role in severe cerebral ischemia/reperfusion *** occurs within hours after cerebral ischemia,but the relationship between ER stress and autophagy remains *** this study,we established experimental models using oxygen-glucose deprivation/reoxygenation in PC12 cells and primary neurons to simulate cerebral ischemia/reperfusion *** found that prolongation of oxygen-glucose deprivation activated the ER stress pathway protein kinase-like endoplasmic reticulum kinase(PERK)/eukaryotic translation initiation factor 2 subunit alpha(e IF2α)-activating transcription factor 4(ATF4)-C/EBP homologous protein(CHOP),increased neuronal apoptosis,and induced ***,inhibition of ER stress using inhibitors or by si RNA knockdown of the PERK gene significantly attenuated excessive autophagy and neuronal apoptosis,indicating an interaction between autophagy and ER stress and suggesting PERK as an essential target for regulating *** autophagy with chloroquine exacerbated ER stress-induced apoptosis,indicating that normal levels of autophagy play a protective role in neuronal injury following cerebral ischemia/reperfusion *** from this study indicate that cerebral ischemia/reperfusion injury can trigger neuronal ER stress and promote autophagy,and suggest that PERK is a possible target for inhibiting excessive autophagy in cerebral ischemia/reperfusion injury.

关键词： apoptosis ATF4 autophagy C/EBP homologous protein cerebral ischemia/reperfusion injury eIF2α endoplasmic reticulum stress PERK

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Mechanical criterion for coal and gas outburst:a perspective from multiphysics coupling

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International Journal of Coal Science & Technology 2021年第6期8卷 1423-1435页

作者： ting Liu Baiquan Lin Xuehai Fu ang Liu School of Safety Engineering China University of Mining&TechnologyXuzhou 221116China Key Laboratory of CBM Resources and Dynamic Accumulation Process China University of Mining&TechnologyXuzhou 221008China Department of Energy and Mineral Engineering G3 Center and EMS Energy InstituteThe Pennsylvania State UniversityUniversity ParkPAUSA

Although a series of hypotheses have been proposed,the mechanism underlying coal and gas outburst remains *** the low-index outbursts encountered in mining practice,we attempt to explore this mechanism using a multiphysics coupling model considering the effects of coal strength and gas mass transfer on *** on force analysis of coal ahead of the heading face,a risk identification index C_(m)and a critical criterion(C_(m)≥1)of coal instability are *** to this criterion,the driving force of an outburst consists of stress and gas pressure gradients along the heading direction of the roadway,whereas resistance depends on the shear and tensile strengths of the *** results show that outburst risk decreases slightly,followed by a rapid increase,with increasing vertical stress,whereas it decreases with increasing coal strength and increases with gas pressure *** the response surface method,a coupled multi-factor model for the risk identification index is *** results indicate strong interactions among the controlling ***,the critical values of the factors corresponding to outburst change depending on the environment of the coal seams,rather than being *** the buried depth of a coal seam increases,the critical values of gas pressure and coal strength decrease slightly,followed by a rapid *** to its controlling factors,outburst can be divided into stress-dominated,coal-strength-dominated,gas-pressure-dominated,and multi-factor compound *** on this classification,a classified control method is proposed to enable more targeted outburst prevention.

关键词： Coal and gas outburst Critical criterion Multiphysics coupling Response surface method

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Precise large deviations for sums of random vectors in a multidimensional size-dependent renewal risk model

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Applied Mathematics(A Journal of Chinese Universities) 2018年第4期33卷 491-502页

作者： SHEN Xin-mei FU Ke-ang zHONG Xue-ting School of Mathematical Sciences Dalian University of Technology School of Statistics and Mathematics Zhejiang Gongshang University

Consider a multidimensional renewal risk model, in which the claim sizes {Xk, k ≥1} form a sequence of independent and identically distributed random vectors with nonnegative components that are allowed to be dependent on each other. The univariate marginal distributions of these vectors have consistently varying tails and finite means. Suppose that the claim sizes and inter-arrival times correspondingly form a sequence of independent and identically distributed random pairs, with each pair obeying a dependence structure. A precise large deviation for the multidimensional renewal risk model is obtained.

关键词： Precise large deviation Size-dependent Consistent variation Multidimensional risk model Renewal counting process

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Refining constitutive relation by integration of finite element simulations and Gleeble experiments

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Journal of Materials Science & Technology 2019年第6期35卷 1039-1043页

作者： D.J. Yu D.S. Xu H. W ang z.B. zhao G.z. Wei R. Yang College of Sciences Northeastern University Shenyang 110004 China Institute of Metal Research Chinese Academy of Sciences Shenyang 110016 China

Thermo-mechanical coupled finite element calculations were carried out to simulate the Gleeble compression of the samples of a titanium alloy(Ti60), and the results are analyzed and compared with the actual compression tests conducted on a Gleeble 3800 thermo-mechanical simulator. The changes in temperature, stress and strain distribution in the samples and the source of error on the constitutive relations from Gleeble hot compression test were analyzed in detail. Both simulations and experiments showed that the temperature distribution in the specimen is not uniform during hot compression, resulting in significant deformation inhomogeneity and non-ignorable error in the flow stress strain relation,invalidating the uniform strain assumption commonly assumed when extracting the constitutive relation from Gleeble tests. Based on the finite element simulations with iterative corrections, we propose a scheme to refine the constitutive relations from Gleeble tests.

关键词： Titanium alloy Constitutive relation Finite element Compression Temperature distribution

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Gradient Structured Copper by Rotationally Accelerated Shot Peening

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Journal of Materials Science & Technology 2017年第7期33卷 758-761页

作者： X.Wang Y.S.Li Q.z.ang Y.H.zhao Y.T.zhu Nano Structural Materials Center School of Materials Science and Engineering Nanjing University of Science and Technology Nanjing 210094 China School of Mechanical Engineering Nanjing University of Science and Technology Nanjing 210094 China Department of Materials Science and Engineering North Carolina State University Raleigh NC 27695 USA

A new technology-rotationally accelerated shot peening（RASP）, was developed to prepare gradient structured materials. By using centrifugal acceleration principle and large steel balls, the RASP technology can produce much higher impact energy compared to conventional shot peening. As a proof-of-concept demonstration, the RASP was utilized to refine the surface layer in pure copper（Cu） with an average grain size of 85 nm. The grain size increases largely from surface downwards the bulk, forming an800 ？m thick gradient-structured surface layer and consequently a micro-hardness gradient. The difference between the RASP technology and other established techniques in preparing gradient structured materials is discussed. The RASP technology exhibits a promoting future for large-scale manufacturing of gradient materials.

关键词： Microstructure Rotationally accelerated shot peening Gradient structure Hardness Copper

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Reconcile the contradictory wettability requirements for the reduction and oxidation half-reactions in overall CO_(2) photoreduction via alternately hydrophobic surfaces

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Journal of Energy Chemistry 2024年第6期93卷 202-212,I0006页

作者： Hailing Huo ting Hu Chengxi Huang Fang Wu Tongyu Wang Xuan Liu Liang zhang Qiang Ju zhiqing zhong Hongbin Xing Erjun Kan ang Li MIIT Key Laboratory of Semiconductor Microstructure and Quantum Sensing Nanjing University of Science and TechnologyNanjing 210094JiangsuChina College of Information Science and Technology Nanjing Forestry UniversityNanjing 210037JiangsuChina

The overall photocatalytic CO_(2) reduction reaction(OPCRR)that can directly convert CO_(2) and H_(2)O into fuels represents a promising renewable energy conversion *** a typical redox reaction,the OPCRR involves two half-reactions:the CO_(2) reduction half-reaction(CRHR)and the water oxidation half-reaction(WOHR).Generally,both half-reactions can be promoted by adjusting the wettability of ***,there is a contradiction in wettability requirements for the two ***,CRHR prefers a hydrophobic surface that can accumulate more CO_(2) molecules on the active sites,ensuring the appropriate ratio of gas-phase(CO_(2))to liquid-phase(H_(2)O)***,the WOHR prefers a hydrophilic surface that can promote the departure of the gaseous product(O_(2))from the catalyst surface,preventing isolation between active sites and the reactant(H_(2)O).Here,we successfully reconciled the contradictory wettability requirements for the CRHR and WOHR by creating an alternately hydrophobic *** was achieved through a selectively hydrophobic modification method and a charge-transfer-control ***,the collaboratively promoted CRHR and WOHR led to a significantly enhanced OPCRR with a solar-to-fuel conversion efficiency of 0.186%.Notably,in ethanol production,the catalyst exhibited a 10.64-fold increase in generation rate(271.44μmol g^(-1)h~(-1))and a 4-fold increase in selectivity(55.77%)compared to the benchmark *** innovative approach holds great potential for application in universal overall reactions involving gas participation.

关键词： Hydrophobic Hydrophilic Gas transport Overall CO_(2)photoreduction z-scheme

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Microelectrode Array-evaluation of Neurotoxic Effects of Magnesium as an Implantable Biomaterial

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Journal of Materials Science & Technology 2016年第1期32卷 89-96页

作者： ting Huang zhonghaiWang Lina Wei Mark Kindy Yufeng zheng tingfei Xi Bruce z. Gao Center for Biomedical Materials and Tissue Engineering Academy for Advanced Interdisciplinary Studies Peking University Beijing 100871 China Department of Bioengineering Clemson University Clemson SC29634 USA Departments of Neurosciences and Regenerative Medicine and Cell Biology Medical University of South Carolina Charleston SC29466 USA Ralph H. Johnson VA Medical Center Charleston SC29403 USA Department of Materials Science and Engineering College of Engineering Peking University Beijing 100871 China Shenzhen Key Laboratory of Human Tissue Regeneration and Repair Shenzhen Institute Peking University Shenzhen 518057 China

Magnesium （Mg）-based biomaterials have shown great potential in clinical applications. However, the cytotoxic effects of excessive Mg2. and the corrosion products from Mg-based biomaterials, particularly their effects on neurons, have been little studied. Although viability tests are most commonly used, a functional evaluation is critically needed. Here, both methyl thiazolyl tetrazolium （MTT） and lactate de- hydrogenase （LDH） assays were used to test the effect of Mg2. and Mg-extract solution on neuronal viability. Microelectrode arrays （MEAs）, which provide long-term, real-time recording of extracellular electro- physiological signals of in vitro neuronal networks, were used to test for toxic effects. The minimum effective concentrations （ECmin） of Mg2. from the MTr and LDH assays were 3 mmol/L and 100 mmol/L respec- tively, while the ECmin obtained from the MEA assay was 0.1 mmol/L MEA data revealed significant loss of neuronal network activity when the culture was exposed to 25% Mg-extract solution, a concentra- tion that did not affect neuronal viability. For evaluating the biocompatibility of Mg-based biomaterials with neurons, MEA electrophysiological testing is a more precise method than basic cell-viability testing.

关键词： Magnesium Microelectrode array Neuroelectrophysiology Neuron viability Neuronal network

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Precise asymptotics in the law of the logarithm for random fields in Hilbert space

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Journal of zhejiang University-Science A(Applied Physics & Engineering) 2007年第4期8卷 651-659页

作者： FU Ke-ang zHang Li-xin Department of Mathematics Zhejiang University Hangzhou 310027 China

Consider the positive d-dimensional lattice z^d（d≥2） with partial ordering ≤, let {XK; K∈z＋^d} be i.i.d, random variables taking values in a real separable Hilbert space （H, ｜｜·｜｜） with mean zero and covariance operator ∑ and set partial sums SN =∑K≤nXK,K,N∈z＋^d. Under some moment conditions, we obtain the precise asymptotics of a kind of weighted infinite series for partial sums SN as ε↓ by using the truncation and approximation methods. The results are related to the convergence rates of the law of the logarithm in Hilbert space, and they also extend the results of （Gut and Spataru, 2003）.

关键词： The law of the logarithm Random field Hilbert space. Tail probabilitv. Truncation method

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