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New mesomorphic benzothiazol derivatives: Synthesis and characterization

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Chinese Chemical Letters 2013年第10期24卷 926-928页

作者： teck-ming koh Sie-Tiong Ha Guan-Yeow Yeap Hong-Cheu Lin Faculty of Engineering & Science Universiti Tunku Abdul RahmanJln Genting KlangSetapak Faculty of Science Universiti Tunku Abdul RahmanJln Universiti Centre for Biodiversity Research Universiti Tunku Abdul RahmanJln Universiti Liquid Crystal Research Laboratory School of Chemical SciencesUniversiti Sains Malaysia Department of Materials Science & Engineering National Chiao Tung University

In this paper, the synthesis of new mesomorphic benzothiazolyl derivatives, 6-ethoxy-2-[4-（4- alkyloxybenzoyloxy）benzylidenamino]benzothiazoles, is presented. The structures of the title compounds were elucidated using spectroscopic techniques, such as FT-IR, NMR （1H and 13C）, elemental analysis and El-MS. The mesomorphic behaviours of these compounds were determined by differential scanning calorimetric and polarizing optical microscopic techniques. Compounds exhibited nematic and tilted smectic phases upon heating from crystal phase. An obvious odd-even effect was observed in this homologous series.

关键词： Benzothiazole Nematic Smectic C Mesomorphic

Synthesis and mesomorphic evaluation of new calamitic liquid crystals containing benzothiazole core

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Chinese Chemical Letters 2011年第5期22卷 619-622页

作者： teck ming koh Sie Tiong Ha teck Leong Lee Siew Ling Lee Guan Yeow Yeap Hong Cheu Lin Ramesh T.Subramaniam Department of Science Faculty of Engineering & ScienceUniversiti Tunku Abdul RahmanJln Genting KlangSetapak53300 Kuala Lumpur.Malaysia Department of Chemistry National University of SingaporeSingapore 117543Singapore Department of Chemical Science Faculty of ScienceUniversiti Tunku Abdul RahmanJln UniversitiBandar Barat31900 KamparPerakMalaysia Ibnu Sina Institute for Fundamental Science Studies Universiti Teknologi Malaysia81310 UTM SkudaiJohorMalaysia Liquid Crystal Research Laboratory School of Chemical SciencesUniversiti Sains Malaysia11800 MindenPenangMalaysia Department of Materials Science & Engineering National Chiao Tung UniversityHsinchu 300Taiwan Center for Ionics University Malaya Department of Physics Faculty of ScienceUniversity of Malaya50603 Kuala LumpurMalaysia

The design and synthesis of new calamitic benzothiazole-based liquid crystals,2-[4-（4-alkyloxybenzoyloxy）-phenyl]ben-zothiazoles are *** target compound was characterized using spectroscopic techniques,such as FT-IR,NMR（~1H and ^（13）C）,microanalysis and *** liquid crystalline behaviours of these compounds were thoroughly examined by differential scanning calorimetry and polarizing optical microscope *** materials exhibited enantiotropic nematic phase with high thermal stability（168℃）.Smectic A phase starts to emerge as monotropic（metastable） phase from C10 member and changes into enantiotropic（stable） phase from C12 and persists up to C16 members.

关键词： Benzothiazole Alkoxy chain Nematic Smectic A Liquid crystal

New mesogenic Schiff base esters comprising benzothiazole moiety:Synthesis and mesomorphic properties

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Chinese Chemical Letters 2009年第9期20卷 1081-1084页

作者： Sie Tiong Ha teck ming koh Guan Yeow Yeap Hong Cheu Lin Jun Kit Beh Yip Foo Win Peng Lim Boey Faculty of Engineering & Science Universiti Tunku Abdul RahmanJln Genting KlangSetapak 53300 Kuala LumpurMalaysia Liquid Crystal Research Laboratory School of Chemical SciencesUniversiti Sains Malaysia 11800 MindenPenangMalaysia Department of Materials Science & Engineering National Chiao Tung University1001 Ta-Hsueh RoadHsinchu 300Taiwan Faculty of Science Engineering & TechnologyUniversiti Tunku Abdul RahmanJln UniversitiBandar Barat 31900 KamparPerakMalaysia

A homologous series of Schiff base esters, 6-methoxy-2-（2-hydroxy-4-alkanoyloxybenzylidenamino）benzothiazoles, compris- ing a benzothiazole moiety as the core was synthesized. All the members of this series exhibited an enantiotropic nematic phase. The azomethine linkage along with the lateral hydroxyl and terminal methoxyl groups were found to exert an effect on the mesomorphic properties. 2009 Sie Tiong Ha. Published by Elsevier B.V. on behalf of Chinese Chemical Society. All rights reserved.

关键词： Schiff bases Benzothiazoles Mesomorphic Nematic Structure-liquid crystal property relationship

Synthesis and mesomorphic properties of new Schiff base esters with different alkyl chains

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Chinese Chemical Letters 2009年第7期20卷 767-770页

作者： Sie Tiong Ha Lay Khoon Ong Siew Teng Ong Guan Yeow Yeap Joanna Pik Wan Wong teck ming koh Hong Cheu Lin Faculty ofEngineering & Science Universiti Tunku Abdul RahmanJln Genting KlangSetapak 53300 Kuala LumpurMalaysia Faculty of Engineering & Science Universiti Tunku Abdul RahmanJln Genting KlangSetapak 53300 Kuala LumpurMalaysia Liquid Crystal Research Laboratory School of Chemical SciencesUniversiti Sains Malaysia 11800 MindenPenangMalaysia Department of Chemistry University of YorkHeslingtonYork YO10 5DDUnited Kingdom.

A new series of Schiff base esters, 4-（dimethylamino）benzylidene-4＇-alkanoyloxyanilines containing even number of carbons at the end group of the molecules （Cn-1H2n-1COO, n = 6, 8, 10, 12, 14, 16, 18） were synthesized. The present compounds were monotropic liquid crystals. It was also found that the end groups of the molecules had effect on the mesomorphic properties. C 2009 Sie Tiong Ha. Published by Elsevier B.V. on behalf of Chinese Chemical Society. All rights reserved.

关键词： Liquid crystals Schiff base esters Monotropic compounds Mesomorphic properties

Towards efficient and stable perovskite photovoltaics with F-contained phosphoric salt surface passivation

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Towards efficient and stable perovskite photovoltaics with F...

Mechano-responsive hydrogel for direct stem cell manufacturing to therapy

第六届新型太阳能电池材料科学与技术学术研讨会

作者： Guifang Han teck ming koh Jia Li Benny Febriansyah Nur Fadilah Jamaludin Subodh Mhaisalkar Nripan Mathews Energy Research Institute NTU (ERI N) Nanyang Technological UniversityResearch Techno Plaza School of Materials Science and Engineering Nanyang Technological University

Surface passivation has been proved as an effective strategy to improve the efficiency and stability of perovskite solar cells. However there is no report on how to choose the passivator, whether it should form as strong or weak bond with perovskite beneath. Here we selectively choose two molecular, alkali carbon chain phosphoric

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Bioactive Materials 2023年第6期24卷 387-400页

作者： Yufeng Shou Ling Liu Qimin Liu Zhicheng Le Khang Leng Lee Hua Li Xianlei Li Dion Zhanyun koh Yuwen Wang Tong ming Liu Zheng Yang Chwee teck Lim Christine Cheung Andy Tay Department of Biomedical Engineering National University of Singapore117583Singapore Institute for Health Innovation&Technology National University of Singapore117599Singapore School of Civil Engineering and Architecture Wuhan University of Technology430070WuhanChina NUS Tissue Engineering Program National University of Singapore117510Singapore Lee Kong Chian School of Medicine Nanyang Technological University636921Singapore School of Mechanical and Aerospace Engineering Nanyang Technological University639798Singapore Institute of Molecular and Cell Biology Agency for ScienceTechnology and Research(A*STAR)138648Singapore Department of Orthopaedic Surgery Yong Loo Lin School of MedicineNational University of Singapore119288Singapore Mechanobiology Institute National University of Singapore117411Singapore

Bone marrow-derived mesenchymal stem cell(MSC)is one of the most actively studied cell types due to its regenerative potential and immunomodulatory *** cell expansion methods using 2D tissue culture plates and 2.5D microcarriers in bioreactors can generate large cell numbers,but they compromise stem cell potency and lack mechanical preconditioning to prepare MSC for physiological loading expected in *** overcome these challenges,in this work,we describe a 3D dynamic hydrogel using magneto-stimulation for direct MSC manufacturing to *** our technology,we found that dynamic mechanical stimulation(DMS)enhanced matrix-integrinβ1 interactions which induced MSCs spreading and *** addition,DMS could modulate MSC biofunctions including directing MSC differentiation into specific lineages and boosting paracrine activities(e.g.,growth factor secretion)through YAP nuclear localization and FAK-ERK *** our magnetic hydrogel,complex procedures from MSC manufacturing to final clinical use,can be integrated into one single platform,and we believe this‘all-in-one’technology could offer a paradigm shift to existing standards in MSC therapy.

关键词： Mesenchymal stem cell Dynamic mechanical stimulation Magnetic hydrogel Stem cell manufacturing Cell therapy

Microwave torrefaction of empty fruit bunch pellet:Simulation and validation of electric field and temperature distribution

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Journal of Bioresources and Bioproducts 2022年第4期7卷 270-277页

作者： Peter Nai Yuh Yek Sieng Huat Kong ming Chiat Law Changlei Xia Rock Keey Liew teck Sung Sie Jun Wei Lim Su Shiung Lam Centre for Research of Innovation and Sustainable Development University of Technology SarawakJalan UniversitySibuSarawak 96000Malaysia School of Foundation Studies University of Technology SarawakJalan UniversitySibuSarawak 96000Malaysia Department of Mechanical Engineering Faculty of Engineering and ScienceCurtin University Malaysia CampusMiriSarawak 98009Malaysia Jiangsu Co-Innovation Center of Efficient Processing and Utilization of Forest Resources International Innovation Center for Forest Chemicals and MaterialsCollege of Materials Science and EngineeringNanjing Forestry UniversityNanjing 210037China NV WESTERN PLT GeorgetownPenang 10400Malaysia Department of Fundamental and Applied Sciences HICoE-Centre for Biofuel and Biochemical ResearchInstitute of Self-Sustainable BuildingUniversity Technology PETRONASDarul RidzuanSeri IskandarPerak 32610Malaysia Higher Institution Centre of Excellence(HICoE) Institute of Tropical Aquaculture and Fisheries(AKUATROP)University Malaysia TerengganuKuala NerusTerengganu 21030Malaysia Sustainability Cluster School of EngineeringUniversity of Petroleum&Energy StudiesDehradunUttarakhand 248007India

Microwave simulation is significant in identifying a reactor design allowing the biomass to be heated and processed *** study integrated the radio frequency and transient heat transfer modules to simulate the microwave distribution and investigated the performance of microwave heating in the *** simulation results were compared with the experimental findings us-ing the finite element analysis software of COMSOL MULTIPHYSICS to predict the temperature profile and electric field of microwave in the biomass(empty fruit bunch pellets).The higher temperature distribution was observed at the bottom and centre section of the empty fruit bunch pellet bed in the reactor,showing the uniqueness of microwave *** to the simula-tion results,the temperature profile obtained through the specific cavity geometry and dielectric properties agreed with the experimental temperature *** simulated temperature profile demonstrated a logarithmic increase of 120°C/min at the first 50 s followed by 50°C/min until 350 *** experimental temperature profile showed three different heating rates before reaching 300°C,including 78.3°C/min(50-120°C),30.6°C/min(121-250°C),and 105°C/min(250-300°C).The results of this study might contribute to the improvement of microwave heating in biomass torrefaction.

关键词： Microwave Torrefaction Simulation Energy Temperature

Modular micro-PCR system for the onsite rapid diagnosis of COVID-19

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Microsystems & Nanoengineering 2022年第4期8卷 125-136页

作者： Phuong Quoc Mai Nguyen ming Wang Nelisha Ann Maria Adelicia Yongling Li Hsih Yin Tan Gordon Minru Xiong Meng-Kwang Marcus Tan Ali Asgar S.Bhagat Catherine W.M.Ong Chwee teck Lim Institute for Health Innovation and Technology(iHealthtech) National University of SingaporeMD614 Medical Drive#14-01Singapore 117599Singapore Department of Biomedical Engineering National University of Singapore4 Engineering Drive 3Block 4#04-08Singapore 117583Singapore Advanced MedTech 2 Venture Drive#23-18 Vision ExchangeSingapore 608526Singapore Infectious Diseases Translational Research Programme Department of MedicineYong Loo Lin School of MedicineNational University of SingaporeNUHS Tower Block1E Kent Ridge Road Level 11Singapore 119228Singapore

Effective containment of the COVID-19 pandemic requires rapid and accurate detection of the *** chain reaction(PCR)remains the gold standard for COVID-19 *** this article,we report the performance of a cost-effective modular microfluidic reverse transcription(RT)-PCR and RT-loop mediated isothermal amplification(RTLAMP)platform,Epidax®,for the point-of-care testing and confirmation of *** platform is versatile and can be reconfigured either for screening using endpoint RT-PCR or RT-LAMP tests or for confirmatory tests using realtime ***®is highly sensitive and detects as little as 1 RNA copy perµL for real-time and endpoint RT-PCR,while using only half of the *** achieved comparable results with those of a commercial platform when detecting SARS-CoV-2 viruses from 81 clinical RNA ***®can also detect SARS-CoV-2 from 44 nasopharyngeal samples without RNA extraction by using a direct RT-PCR assay,which shortens the sample-to-answer time to an hour with minimal user ***,we validated the technology using an RT-LAMP assay on 54 clinical RNA ***,our platform provides a sensitive,cost-effective,and accurate diagnostic solution for lowresource settings.

关键词： fir confirmation diagnosis

Functional micro‐concrete 3D hybrid structures f abricated by two‐photon polymerization

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光电工程 2017年第4期44卷 393-399,469页

作者： Yang Li Lianwei Chen Fang Kong Zuyong Wang ming Dao Chwee teck Lim Fengping Li minghui Hong National University of Singapore 4 Engineering Drive 3 Singapore 117576 Singapore State Key Laboratory of Optical Technologies for Nano-Fabrication and Micro-Engineering Institute of Optics and Electronics Chinese Academy of Sciences Chengdu 610209 China Singapore MIT Alliance Research and Technology Singapore 138602 Singapore College of Mechanical and Electrical Engineering Wenzhou University Wenzhou 325025 China

Arbitrary micro-scale three-dimensional(3D)structures fabrication is a dream to achieve many exciting goals that have been pursued for a long *** all these applications,the direct 3D printing to fabricate human organs and integrated photonic circuits are extraordinary attractive as they can promote the current technology to a new *** all the 3D printing methods available,two-photon polymerization(2PP)is very competitive as it is the unique method to achieve sub-micron resolution to make any desired tiny *** the conventional 2PP,the building block is the ***,the requirement for the building block is different for different *** is very necessary to investigate and improve the photoresist properties according to different *** this paper,we presented one hybrid method to modify the mechanical strength and light trapping efficiency of the photoresist,which transfers the photoresist into the *** micro-concrete structure can achieve±22%strength modification via a silica nano-particles *** structures doped with gold nano-particles show tunable plasmonic *** doped hybrid structure shows great potential to fabricate 3D micro-chip laser.

关键词： 3D打印光子集成电路发展现状技术创新