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Insights into in-situ imbibition behavior of fracturing fluid in propped shale fractures based on nuclear magnetic resonance:A case study from Longmaxi Formation shale,Sichuan Basin,China

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Petroleum Science 2024年第1期21卷 410-429页

作者： Jing-Jing Guo Kai-Xiang Di Lie-hui zhang Yu-Long Zhao hui-Ying tang Rui-Han zhang Ye tian National Key Laboratory of Oil and Gas Reservoir Geology and Exploitation Southwest Petroleum UniversityChengdu610500SichuanChina

Shale gas is an important component of unconventional oil and gas *** the imbibition behavior is helpful to optimize flowback parameters and enhance gas *** imbibition studies have focused on shale matrix,and the pressure conditions discussed were mostly *** initial imbibition behavior begins from propped fractures to matrix,but there are few studies working on explaining the imbibition behavior in propped fractures or the phenomenon of many shale wells exhibit higher productivity after a“soaking”***,propped fracture samples were designed for imbibition and migration *** order to accurately study the mechanism and main influencing factors of fracturing fluid imbibition and migration in propped and unpropped shale fractures under high temperature and high pressure,a series of experiments based on nuclear magnetic resonance(NMR)were carried *** showed that NMR T_(2) spectra of all samples exhibited a bimodal *** final imbibition volume of fracturing fluid was positively related to pressure and fracture *** imbibition effect of fracturing fluid was more evident in matrix pores under high *** the migration during soaking stage,the fracturing fluid gradually migrated from large pores to small pores and gradually displaced the shale gas from the matrix,thus allowing the water blocking in propped fractures to self-unlock to some *** permeability decreased in the imbibition stage,while it recovered in the migration stage to some extent.

关键词： Forced imbibition Migration Soaking NMR T_(2)spectra Propped fracture Permeability recovery

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Experimental Study of Electrical‑Assisted Nanomachining of Monocrystalline Copper Using Customized Tungsten Tip

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Nanomanufacturing and Metrology 2024年第2期7卷 60-75页

作者： Tao Wang Yanling tian Zhilai Lu Weijie Wang Zhao zhang Guangwei Zhu hui tang Dawei zhang Key Laboratory of Mechanism Theory and Equipment Design of Ministry of Education Tianjin UniversityTianjin 300072China School of Engineering University of WarwickCoventry CV47ALUK State Key Laboratory of High Performance Complex Manufacturing Central South UniversityChangsha 410083China State Key Laboratory of Precision Electronic Manufacturing Technology and Equipment Guangdong University of TechnologyGuangzhou 510006China

As a promising micro/nanofabrication method,electrical-assisted nanomachining has obtained substantial attention due to its high material removal rate and attainable superior surface *** this study,a rectangular wave electrical signal was applied for nanomachining by a customized tungsten *** to the coupling effect between the electric field and mechanical force,the cutting depth of the machined grooves can be *** electrical-assisted groove processing,a depth of 270 nm and an aspect ratio of 0.6 on the copper sample can be *** influence of operation parameters including applied voltage,frequency,duty ratio,normal force and cutting speed on the machining performance was investigated in terms of the groove depth,width,aspect ratio,and surface *** potential machining mechanisms should be a combination of electric field force,nanoscale electric discharge,electric contact thermal effects,possible annealing behavior,and scraping and plowing actions induced by mechanical forces.

关键词： Tip-based nanofabrication Electrical-assisted machining Nanoscale scratching Machining parameters

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Local Discontinuous Galerkin Methods with Decoupled Implicit-Explicit Time Marching for the Growth-Mediated Autochemotactic Pattern Formation Model

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Advances in Applied Mathematics and Mechanics 2024年第1期16卷 208-236页

作者： hui Wang hui Guo Jiansong zhang Lulu tian College of Science China University of PetroleumQingdaoShandong 266580China

In this paper,two fully-discrete local discontinuous Galerkin(LDG)methods are applied to the growth-mediated autochemotactic pattern formation model in self-propelling *** numerical methods are linear and decoupled,which greatly improve the computational *** order to resolve the time level mismatch of the discretization process,a special time marching method with high-order accuracy is *** the condition of slight time step constraints,the optimal error estimates of this method are ***,the theoretical results are verified by numerical *** simulations show the patterns of spots,rings,stripes as well as inverted spots because of the interplay of chemotactic drift and growth rate of the cells.

关键词： Local discontinuous Galerkin methods implicit-explicit time-marching scheme error estimate growth-mediated autochemotactic pattern formation model

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Ultralow-phase-noise and broadband frequency-hopping coupled optoelectronic oscillator under quiet point operation

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Photonics Research 2024年第8期12卷 1785-1793页

作者： hui LIU MINGYang GUO tian zhang JIAN DAI KUN XU State Key Laboratory of Information Photonics and Optical Communications Beijing University of Posts and TelecommunicationsBeijing 100876China School of Electronic Engineering Beijing University of Posts and TelecommunicationsBeijing 100876China

Advancements in microwave photonics have yielded novel approaches for generating high-purity microwave *** these,optoelectronic oscillators(OEOs)and coupled optoelectronic oscillators(COEOs)have demonstrated the capability to generate frequency-independent microwaves with exceptionally low phase ***,the tunability of the oscillators is rather limited due to the necessity for narrowband electronic bandpass filters,presenting challenges in achieving both wide and rapid tuning ***,we present a COEO featuring ultralow phase noise,flexible tuning capability,and high *** is achieved through a quiet point(QP)-operated harmonic mode-locked fiber laser,which effectively mitigates optical amplifier noise and supermode competition,thus significantly diminishing the necessity for ultra-narrow electronic *** to the liberated tuning ability,we present an oscillator that can be tuned from 2 GHz to 18 GHz,with phase noise as low as-140 d Bc/Hz at 10 k Hz under the QP *** then illustrate the practical application of the proposed oscillator in generating frequency-hopping signals with consistent spurious modes less than-85 d Bc,absolute phase noise below-135 d Bc/Hz at 10 k Hz,hopping resolution of 1.25 MHz,and fractional frequency stability below 6.1×10^(-12)at 1 s averaging time when locked to a *** presented COEO structure emerges as a compelling solution for agile and low-noise microwave sources in advanced wireless communication and radar systems.

关键词： optoelectronic tuning amplifier

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Dual-filler reinforced PVDF-HFP based polymer electrolyte enabling high-safety design of lithium metal batteries

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Nano Research 2024年第6期17卷 5251-5260页

作者： Chang Fang Kangsheng Huang Jing Zhao Shiqi tian hui Dou Xiaogang zhang Jiangsu Key Laboratory of Electrochemical Energy Storage Technologies College of Materials Science and TechnologyNanjing University of Aeronautics and AstronauticsNanjing 210016China

Despite the high energy density of lithium metal batteries(LMBs),their application in rechargeable batteries is still hampered due to insufficient ***,we present a novel flame-retardant solid-state electrolyte based on polyvinylidene fluoride-hexafluoropropylene(PVDF-HFP)with nano SiO_(2)aerogel as an inert filler but Li_(6.4)La_(3)Zr_(1.4)Ta_(0.6)O_(12)(LLZTO)as an auxiliary component to enhance the ion *** introduction of SiO_(2)aerogels imparts the polymer electrolyte with exceptional thermal stability and flame ***,the interaction between hydroxyl groups of SiO_(2)particles and PVDF-HFP creates a strong cross-linking structure,enhancing the mechanical strength and stability of the ***,the presence of SiO_(2)aerogel and LLZTO facilitates the dissociation of lithium salts through Lewis acid-base interactions,resulting in a high ionic conductivity of 1.01×10^(−3)S·cm^(−1)and a wide electrochemical window of~5.0 V at room temperature for the prepared ***,the assembled Li|Li cell demonstrates the excellent resistance to lithium dendrite and runs stablly for over 1500 h at a current density of 0.25 mA·cm^(−2).Thus,we prepare a pouch cell with high safety,which can work normally after short-circuiting under the external folding and cutting.

关键词： polymer electrolyte SiO_(2)/Li_(6.4)La_(3)Zr_(1.4)Ta_(0.6)O_(12)(LLZTO)dual-filler non-flammable long cycle life lithium metal battery

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Quantum weak force sensing with squeezed magnomechanics

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Science China(Physics,Mechanics & Astronomy) 2024年第10期67卷 23-32页

作者： Qian zhang Jie Wang tian-Xiang Lu Ran Huang Franco Nori hui Jing Key Laboratory of Low-Dimensional Quantum Structures and Quantum Control of Ministry of Education Department of Physics and Synergetic Innovation Center for Quantum Effects and ApplicationsHunan Normal UniversityChangsha 410081China Theoretical Quantum Physics Laboratory Cluster for Pioneering ResearchRIKENWako-shi 351-0198Japan Center for Quantum Computing RIKENWako-shi 351-0198Japan Department of Physics University of MichiganAnn Arbor 48109-1040USA College of Physics and Electronic Information Gannan Normal UniversityGanzhou 341000China Academy for Quantum Science and Technology Zhengzhou University of Light IndustryZhengzhou 450002China

Cavity magnomechanics,exhibiting remarkable experimental tunability,rich magnonic nonlinearities,and compatibility with various quantum systems,has witnessed considerable advances in recent ***,the potential benefits of using cavity magnomechanical(CMM)systems in further improving the performance of quantum-enhanced sensing for weak forces remain largely *** we show that,by squeezing the magnons,the performance of a quantum CMM sensor can be significantly enhanced beyond the standard quantum limit(SQL).We find that,for comparable parameters,two orders of magnitude enhancement in the force sensitivity can be achieved in comparison with the case without magnon ***,we obtain the optimal parameter regimes of homodyne angle for minimizing the added quantum *** findings provide a promising approach for highly tunable and compatible quantum force sensing using hybrid CMM devices,with potential applications ranging from quantum precision measurements to quantum information processing.

关键词： quantum force sensing cavity magnomechanics magnon Kerr effect

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Effects of surface morphology on tribological properties of Arapaima gigas scales

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Friction 2024年第7期12卷 1469-1482页

作者： Shuaijun zhang Pengpeng BAI Xiangli WEN Chengwei WEN hui CAO Wanyou Yang Yu tian State Key Laboratory of Tribology in Advanced Equipment Department of Mechanical EngineeringTsinghua UniversityBeijing 100084China Key Laboratory of Bionic Engineering(Ministry of Education China)Jilin UniversityChangchun 130022China

The remarkable mechanical adaptability of arapaima(Arapaima gigas)scales has made them an important subject of ***,no research has been conducted into their tribological properties,which are crucial for the protectability and flexibility of *** this study,by combining morphological characterizations,friction experiments,and theoretical analyses,the relationship between the surface morphology and tribological properties of arapaima scales is *** results indicate that arapaima scales exhibit varying surface morphologies in different *** specifically,the exposed regions of scales feature grooves and a circulus,whereas the covered regions exhibit *** specific surface morphology of arapaima scales produces varying tribological properties across different regions and sliding *** unique tribological properties of arapaima scales influence the forces received from predator attacks and neighboring scales,directly influencing the arapaima’s protective *** study provides new insights into the mechanisms of natural flexible dermal armors,and it has potential applications in personal protective systems.

关键词： arapaima scales surface morphology tribological properties protectability

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Spectral Index Distribution of Various Scale Components in Supernova Remnant Cassiopeia A

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Research in Astronomy and Astrophysics 2024年第5期24卷 211-217页

作者： Xianhuan Lei hui Zhu Zongyao Yin Haiyan zhang Wenwu tian Xianchuan Yu Key Laboratory of Radio Astronomy and Technology National Astronomical ObservatoriesChinese Academy of SciencesBeijing 100101China University of Chinese Academy of Sciences Beijing 101408China School of Artiﬁcial Intelligence Beijing Normal UniversityBeijing 100875China

Cassiopeia A(Cas A) is a well-known candidate for studying cosmic-ray acceleration, in which compact features of various scales have attracted much attention. Based on observations by the Very Large Array of Cas A at 6 cm and 21 cm, we measure the spectral index distribution of various scale components using the observation of the 1998 epoch. We decompose its total density image into nine scale components, and map the temperature spectral index distribution of each component, which ranges from-2.48 ± 0.01 to-2.91 ± 0.05. We find that the spectral indices increase from the small scale to large scale components. A damped post-shock magnetic field model with a strength larger than ~200 μG and a damping length scale less than ~10% of the remnant radius can account for the spectral index variation naturally.

关键词： ISM supernova remnants-(ISM:)cosmic rays-radio continuum ISM

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Regio-and Stereoselective Polymerization of Bio-based Ocimene by Rare-Earth Metal Catalysts

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Chinese Journal of Polymer Science 2024年第2期42卷 223-229,I0008页

作者： Qi-Yuan Wang Li-Peng Sang Zhen zhang Yang Jiang hui tian Xia Zhao Xiang Guo Shi-hui Li State Key Laboratory of Polymer Physics and Chemistry Changchun Institute of Applied ChemistryChinese Academy of SciencesChangchun130022China School of Applied Chemistry and Engineering University of Science and Technology of ChinaHefei230026China Science and Technology on Aerospace Chemical Power Laboratory Hubei Institute of Aerospace ChemotechonologyXiangyang441003China Shanxi Coal Chemical Industry Technology Research Institute Xi’an710000China Hubei Institute of Aerospace Chemotechonology Xiangyang441003China

Coordination polymerization of renewable β-ocimene has been investigated using asymmetric diiminophosphinate lutetium complex1, β-diketiminate yttrium complex 2, bis(phosphino)carbazolide yttrium complex 3, half-sandwich benzyl fluorenyl scandium complex 4 and pyridyl-methylene-fluorenyl rare-metal complexes 5a–5c. Complexes 1, 4 and 5a–5c show trans-1,2-regioselectivities and high activities, of which 5c exhibits excellent isoselectivity(mmmm>99%). Conversely, complexes 2 and 3 promote β-ocimene polymerization to produce isotactic cis-1,4-polyocimenes(cis-1,4>99%, mm>95%). Diblock copolymers cis-1,4-PIP-block-cis-1,4-POc and cis-1,4-PBD-block-cis-1,4-POc are obtained in one-pot reactions of β-ocimene with isoprene and butadiene using complex 3. Epoxidation and hydroxylation of polyocimene afford functionalized polyolefins with enhanced T_(g)(from-20 ℃ to 79 ℃ and 74 ℃) and hydrophilicity.

关键词： Biobased monomer Terpenes Ocimene Rare-earths Polymerization Regio/stereoselectivity Elastomer

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Phase transfer-based high-efficiency recycling of precious metal electrocatalysts

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Green Chemical Engineering 2024年第1期5卷 68-74页

作者： Qing Zeng Shaonan tian Yu zhang hui Liu Dong Chen Xinlong tian Chaoquan Hu Jun Yang State Key Laboratory of Multiphase Complex Systems Institute of Process EngineeringChinese Academy of SciencesBeijing100190China State Key Laboratory of Marine Resource Utilization in South China Sea Hainan Provincial Key Lab of Fine ChemistrySchool of Chemical Engineering and TechnologyHainan UniversityHaikou570228China Nanjing IPE Institute of Green Manufacturing Industry Nanjing211100China Center of Materials Science and Optoelectronics Engineering University of Chinese Academy of SciencesBeijing100049China

Recycling precious metals with high-efficiency is undoubtedly beneficial to optimize resource utilization for environmental remediation and sustainable ***,we report an efficient route to recycle the palladium(Pd)and platinum(Pt)electrocatalysts using a phase transfer *** strategy involves acidic dissolution of deactivated precious metal(Pd/Pt)electrocatalysts from their loading substrates,mixing with an ethanolic solution of dodecylamine(DDA),subsequent extraction of metal ions into a non-polar organic phase,and final reduction by sodium borohydride to reproduce high-performance electrocatalysts towards typical electrochemical reactions,e.g.,oxygen reduction reaction(ORR)and ethanol oxidation reaction(EOR).In specific,the transfer efficiencies are up to 98%and the final recovery rate is over 85%for Pd and Pt electrocatalysts in each *** approach symbolizes a facile and efficient way to recover precious metals,which might be applied to recycling a wide range of metals in various realms after appropriate modifications.

关键词： Precious metal Phase transfer Extraction Recovery Electrocatalyst

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