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Kinetics of electroless Ni-Cu-P deposits on silicon in a basic hypophosphite-type bath

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International Journal of Minerals,Metallurgy and Materials 2009年第2期16卷 197-202页

作者： shu-huei hsieh Wen-Jauh Chen Department of Materials Science and Engineering Formosa UniversityHuweiYunlin 632China Taipei Graduate School of Materials Science Yunlin University of Science and TechnologyYunlin 640China Taipei

Electroless Ni-Cu-P deposits were deposited on the Si substrate in a basic hypophosphite-type plating bath. The effects of pH value and the metal source composition,Ni and Cu,in the plating bath on the kinetics of the Ni-Cu-P deposition were studied. The electroless Ni-Cu-P deposits were characterized by a scanning electron microscope,a transmission electron microscope,an energy dispersive X-ray spectroscope,and an X-ray diffractometer. The results showed that the pH value of the plating bath had no ob-vious effect on the morphology and composition of electroless Ni-Cu-P deposits. However,the composition of the metal source,Ni and Cu,in the plating bath had great effect on the kinetics of electroless Ni-Cu-P deposition.

关键词： electroless deposition Ni-Cu-P silicon substrate kinetics activation energy

Synthesis of the CuInSe_2 thin film for solar cells using the electrodeposition technique and Taguchi method

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International Journal of Minerals,Metallurgy and Materials 2009年第1期16卷 101-107页

作者： Wei-long Liu shu-huei hsieh Wen-jauh Chen Pei-i Wei Jing-herng Lee Department of Materials Science and Engineering Huwei Institute of Technology Yunlin China Taipei Graduate Institute of Materials Science Yunlin University of Science and Technology Yunlin China Taipei

The Taguchi method was used to obtain the optimum electrodeposition parameters for the synthesis of the CuInSe2 thin film for solar cells. The parameters consist of annealing temperature, current density, CuCl2 concentration, FeCl3 concentration, H2SeO3 concentration, TEA amount, pH value, and deposition time. The experiments were carried out according to an L18（2^13^7） table An X-ray diffractometer （XRD） and a scanning electron microscope （SEM） were respectively used to analyze the phases and observe the microstructure and the grain size of the CuInSe2 film before and after annealing treatment. The results showed that the CuInSe2 phase was deposited with a preferred plane （112） parallel to the substrate surface. The optimum parameters are as follows： current density, 7 mA/cm^2; CuCl2 concentration, 10 mM; FeCl3 concentration, 50 mM; H2SeO3 concentration, 15 mM; TEA amount, 0 mL; pH value, 1.65; deposition time, 10 min; and annealing temperature, 500℃.

关键词： CuInSe2 (CIS) thin film solar cell electrodeposition Taguchi method

Interface structure between epitaxial NiSi_2 and Si

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Journal of University of Science and Technology Beijing 2006年第6期13卷 558-563页

作者： Wei-Long Liu Wen-Jauh Chen Ting-Kan Tsai Hsun-Heng Tsai shu-huei hsieh Department of Materials Engineering Formosa University Yunlin China Taipei Graduate Institute of Materials Engineering Pingtung University of Science and Technology 1 Pingtung China Taipei Department of Biosystems Engineering Pingtung University of Science and Technology 1 Pingtung China Taipei

The interface structure between the Si and NiSi2 epitaxially grown on the （112） Si substrate was studied using high resolution transmission electron microscopy and computer image simulation. The results showed that the interface between Si and NiSi2 epitaxially grown on the （ 112 ） Si substrate has six different types： type A NiSi2 （111 ）/（ 111 ） Si, type A NiSi2 （001）/（001） Si, type B NiSi2 （ 111 ）/（ 111） Si, type B NiSi2 （ 112 ）/（ 1 12 ） Si, type B NiSi2 （ 271 ）/（001） Si, and type B NiSi2 （ 114 ）/（ 110 ） Si. And there are one or more different atomic structures for one type of interface.

关键词： nickel silicide interface high resolution image simulation atomic structure

Growth behavior of electroless copper on silicon substrate

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Journal of University of Science and Technology Beijing 2007年第1期14卷 67-71页

作者： Shin-Shyan Wu Wei-Long Liu Ting-Kan Tsai shu-huei hsieh Wen-Jauh Chen Institute of Electro-Optical and Materials Science Formosa University Yunlin China Taipei Department of Materials Science and Engineering Formosa University Yunlin China Taipei Graduate Institute of Materials Engineering Pingtung University of Science and Technology Pingtung China Taipei

The growth behavior containing deposit morphology, growth rate, activation energy, and growth mechanism of copper on silicon substrate, especially at the initial stage, in the electroless plating process was studied. Copper was deposited on the surface of the silicon substrate in an electloless plating bath containing formalin （CH2O 37vol%） as a reducing agent at a pH value of 12.5 and a temperature of 50-75℃. The copper deposit was characterized using a field emission scanning electron microscope and transmission electron microscope. The results showed that after the activation process, nanoscale Pd particles were distributed evenly on the surface of the silicon; in the deposition process, copper first nucleated at locations not only near the Pd particles but also between the Pd particles; the growth rate of electroless Cu ranged from 0.517 nm/s at 50℃ to 1.929 nm/s at 75℃. The activation energy of electroless Cu on Si was 52.97 kJ/mol.

关键词： electroless copper silicon substrate activation energy growth mechanism

Automated and miniaturized screening of antibiotic combinations via robotic-printed combinatorial droplet platform

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Acta Pharmaceutica Sinica B 2024年第4期14卷 1801-1813页

作者： Fangchi Shao Hui Li Kuangwen hsieh Pengfei Zhang Sixuan Li Tza-huei Wang Department of Biomedical Engineering Johns Hopkins UniversityBaltimoreMD 21218USA Department of Mechanical Engineering Johns Hopkins UniversityBaltimoreMD 21218USA

Antimicrobial resistance(AMR)has become a global health crisis in need of novel *** this end,antibiotic combination therapies,which combine multiple antibiotics for treatment,have at-tracted significant attention as a potential approach for combating *** facilitate advances in anti-biotic combination therapies,most notably in investigating antibiotic interactions and identifying synergistic antibiotic combinations however,there remains a need for automated high-throughput plat-forms that can create and examine antibiotic combinations on-demand,at scale,and with minimal reagent *** address these challenges,we have developed a Robotic-Printed Combinatorial Droplet(RoboDrop)platform by integrating a programmable droplet microfuidic device that generates antibiotic combinations in nanoliter droplets in automation,a robotic arm that arranges the droplets in an array,and a camera that images the array of thousands of droplets in *** further implement a resazurin-based bacterial viability assay to accelerate our antibiotic combination *** a demonstration,we use RoboDrop to corroborate two pairs of antibiotics with known interactions and subsequently identify a new synergistic combination of cefsulodin,penicillin,and oxacillin against a model *** *** therefore envision RoboDrop becoming a useful tool to efficiently identify new synergistic antibiotic combinations toward combating AMR.

关键词： Droplet microfluidics Antimicrobial resistance Antibiotic combinatorial screening Contact printing Robotics Pharmaceutical analysis High-throughput Antibiotic interactions

Effect of Fe metal on the growth of silicon oxide nanowires

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International Journal of Minerals,Metallurgy and Materials 2009年第3期16卷 317-321页

作者： Wei-long Liu1), shu-huei hsieh1), Ching He Chen2), and Wen-jauh Chen3) 1) Department of Materials Science and Engineering, Formosa University, Yunlin 632, China Taipei 2) Department of Materials Engineering, Pingtung University of Science and Technology, Pingtung 912, China Taipei 3) Graduate School of Materials Science, Yunlin University of Science and Technology, Yunlin 632, China Taipei Department of Materials Science and Engineering Formosa University Yunlin 632 China Taipei Department of Materials Engineering Pingtung University of Science and Technology Pingtung 912 China Taipei Graduate School of Materials Science Yunlin University of Science and Technology Yunlin 632 China Taipei

Silicon oxide (SiOx) nanowires are generally grown on Si substrate under the catalysis of Au in N2 atmosphere at elevated temperatures. Because the price of Au metal is quite high, Fe metal is then used to replace a part of Au for catalyzing the growth of SiOx nanowires. The results show that the Fe film can be used as the diffusion barrier of Au. SiOx nanowires are grown on Au/Fe/Si substrate at 1030°C. Under the catalysis of Fe/Au, the efficiency for the growth of SiOx nanowires is promoted.

关键词： silicon oxide nanowires Au catalyst Fe substitution Si substrate

Concise extraction and characterization of the pore-throat network in unconventional hydrocarbon reservoirs: A new perspective

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Petroleum Science 2024年第3期21卷 1474-1487页

作者： shu-Heng Du Yong-Min Shi State Key Laboratory of Nonlinear Mechanics Institute of MechanicsChinese Academy of SciencesBeijing100190China School of Engineering Science University of Chinese Academy of SciencesBeijing100049China School of Earth and Space Sciences Peking UniversityBeijing100871China

In this study,a new image-based method for the extraction and characterization of pore-throat network for unconventional hydrocarbon storage and exploitation is proposed.“Pore-throat solidity”,which is analogous to particle solidity,and a new method for automatic identification of pores and throats in tight sandstone oil reservoirs are ***,the“pore-throat combination”and“pure pore”are defined and distinguished by drawing the cumulative probability curve of the pore-throat solidity and by selecting an appropriate cutoff *** the discrete grid set is recognized as a pore-throat combination,Legendre ellipse fitting and minimum Feret diameter are *** the pore and throat grid sets are identified as pure pores,the pore diameter can be directly *** the new method,the analytical results for the physical parameters and pore radius agree well with most prior *** results comparing the maximum ball and the new model could also prove the accuracy of the latter's in micro and nano *** new model provides a more practical theoretical basis and a new calculation method for the rapid and accurate evaluation of the complex processes of oil migration.

关键词： Hydrocarbon exploitation Pore Throat Porous media Identification

Origins of perturbations in dayside equatorial ground magnetograms

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Earth and Planetary Physics 2024年第1期8卷 215-221页

作者： Syau-Yun W.hsieh David G.Sibeck The Johns Hopkins University Applied Physics Laboratory LaurelMarylandUSA NASA Goddard Space Flight Center GreenbeltMarylandUSA

To determine the cause(s)of perturbations seen in dayside equatorial ground magnetograms,we conducted a systematic survey of simultaneous ground-based and geosynchronous satellite-based observations during the 90-day period from December 1,2020 to February 28,*** examined Huancayo ground magnetometer observations from 14:00:00 to 20:00:00 UT each day,during which Huancayo passed through local *** those data we chose perturbation events selected on the basis of large(>20 nT)event amplitude and classified the selected events as responding primarily to solar wind pressure,or to variations in the north/south component of the interplanetary magnetic field(IMF Bz),or perhaps in part to *** results show that an equivalent number of events were identified for each model during this 90-day *** in the lagged solar wind dynamic pressure routinely correspond to nearly simultaneous sudden impulses recorded at both geosynchronous orbit and on the *** in IMF Bz produce erosion signatures at geosynchronous orbit and can correspond to ground events if lag times for reconnection to enhance convection in the magnetosphere are taken into account.

关键词： dayside magnetosphere dayside equatorial ionosphere geosynchronous magnetic field

Cu-substituted nickel hexacyanoferrate with tunable reaction potentials for superior ammonium ion storage

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Journal of Materials Science & Technology 2024年第2期169卷 19-27页

作者： Leiyu Fan Guangchang shu Yiwen Liu Haoxiang Yu Lei Yan Liyuan Zhang Jie shu School of Materials Science and Chemical Engineering Ningbo UniversityNingbo 315211China

In this work,a variety of Cu_(x)Ni_(2-x)Fe(CN)_(6)(x=0,0.4,0.8,1.2,1.6,2)cathodes for ammonium ion batteries are prepared and their electrochemical performances are *** the introduction of copper in nickel hexacyanoferrate,the electrochemical performance varies without changing the structure of nickel *** increase of Cu content in nickel hexacyanoferrate leads to the enhancement of reaction potential and *** results suggest that the substitution of Cu for Ni has a positive effect on improving the cycling stability and rate capacity of nickel hexacyanoferrate when x in Cu_(x)Ni_(2-x)Fe(CN)_(6)is less than ***,Cu_(0.4)Ni_(1.6)Fe(CN)_(6)exhibits the best cycling per-formance(capacity retention of 97.54%at 0.3 C)and the highest rate capacity(41.4 mAh g^(-1)at 10 C)in Cu_(x)Ni_(2-x)Fe(CN)_(6).Additionally,the X-ray diffraction(XRD)and X-ray photoelectron spectroscopy(XPS)tests also reveal that the structural evolution of Cu_(0.4)Ni_(1.6)Fe(CN)_(6)is highly reversible upon NH_(4)^(+)***,this work proposes a candidate material for ammoniumion batteries and offers a novel avenue for adjusting the operating potential of the material.

关键词： Nickel hexacyanoferrate Copper hexacyanoferrate NH_(4)^(+)storage Ammonium ion batteries Aqueous batteries