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Synthesis and characterization of lower generation broom molecules

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Chinese Chemical Letters 2008年第1期19卷 43-46页

作者： Jun Wang Cui Qin Li shu yan zhang Fang Sun Teng Jie Ge College of Chemistry and Chemical Engineering Daqing Petroleum Institute Daqing 163318 China Fine Chemical Laboratory Research Institute of Daqing Petrochemical Company Daqing 163714 China

Dendritic molecules with dodecyl groups as the hyperbranchs were synthesized in methanol by Michael addition with dodecylamine and methyl acrylate as raw materials. This new-type dendritic molecules were called vividly ＂broom molecules＂ in this report. The surface tension of the aqueous solution of broom molecule terminated amino group was measured by using the dropvolume method. The demulsification performance of the broom molecules for the oil/water （O/W） simulated crude oil emulsion was examined. The experimental results revealed that, as a new-type of surfactants, the broom molecules terminated amino groups showed demulsification for the O/W simulated crude oil emulsion. 2007 Jun Wang. Published by Elsevier B.V. on behalf of Chinese Chemical Society. All fights reserved.

关键词： Dendrimer Broom molecule Surface tension Demulsification

Microstructure and microhardness of Ti-48Al alloy prepared by rapid solidification

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China Foundry 2020年第6期17卷 429-434页

作者： Xiao-yu Chen Hong-ze Fang Qi Wang shu-yan zhang Rui-run Chen yan-qing Su School of Materials Science and Engineering Harbin Institute of TechnologyHarbin 150001China School of Electromechanic Engineering Qingdao UniversityQingdao 266071China Centre of Excellence for Advanced Materials Dongguan 523808China

To improve the microstructure and microhardness,Ti-48Al(at.%)alloy was rapidly solidified by melt spinning under different cooling *** microstructure and microhardness of rapidly solidified Ti-48Al alloy were systematically *** show that the average lamellar colony size of the alloy reduces from 60.6μm to 11μm as the cooling rate increases from 2.3×105 to 5.1×105 K·s-1,caused by the increase of nucleation rate at a higher cooling *** the high cooling rate of(4.3-5.1)×105 K·s-1,theαphase is the primary phase,and a few metastableαphases are reserved,which then transform intoα2 phase and subsequently lead to the formation ofα2 equiaxed *** lamellar spacing also decreases with the increase of cooling *** relationship between lamellar spacing(d)and cooling rate(v)is d=*** microhardness increases with the increase of cooling rate because the refined lamellar spacing and grain size can improve the microhardness.

关键词： cooling rate solidification path microstructure lamellar spacing microhardness

Heyingwuzi formulation alleviates diabetic retinopathy by promoting mitophagy via the HIF-1α/BNIP3/NIX axis

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World Journal of Diabetes 2024年第6期15卷 1317-1339页

作者： Jia-Jun Wu shu-yan zhang Lin Mu Zhi-Guo Dong Yin-Jian zhang Department of Ophthalmology Longhua Hospital Shanghai University of Traditional Chinese MedicineShanghai 200032China Department of Ophthalmology Eye and ENT HospitalFudan UniversityShanghai 200031China

BACKGROUND Diabetic retinopathy(DR)is the primary cause of visual problems in patients with *** Heyingwuzi formulation(HYWZF)is effective against *** To determine the HYWZF prevention mechanisms,especially those underlying *** Human retinal capillary endothelial cells(HRCECs)were treated with high glucose(hg),HYWZF serum,PX-478,or Mdivi-1 in ***,cell counting kit-8,transwell,and tube formation assays were used to evaluate HRCEC proliferation,invasion,and tube formation,*** electron microscopy was used to assess mitochondrial morphology,and Western blotting was used to determine the protein *** cytometry was used to assess cell apoptosis,reactive oxygen species(ROS)production,and mitochondrial membrane ***,C57BL/6 mice were established in vivo using streptozotocin and treated with HYWZF for four *** glucose levels and body weight were monitored *** in retinal characteristics were evaluated using hematoxylin and eosin,tar violet,and periodic acid-Schiff *** levels in retinal tissues were determined via Western blotting,immunohistochemistry,and *** HYWZF inhibited excessive ROS production,apoptosis,tube formation,and invasion in hg-induced HRCECs via mitochondrial autophagy in *** increased the mRNA expression levels of BCL2-interacting protein 3(BNIP3),FUN14 domain-containing 1,BNIP3-like(BNIP3L,also known as NIX),PARKIN,PTEN-induced kinase 1,and hypoxia-inducible factor(HIF)-1α.Moreover,it downregulated the protein levels of vascular endothelial cell growth factor and increased the light chain 3-II/I ***,PX-478 and Mdivi-1 reversed these ***,PX-478 and Mdivi-1 rescued the effects of HYWZF by decreasing oxidative stress and apoptosis and increasing *** intervention improved the symptoms of diabetes,tissue damage,number of acellular capillaries,and oxidative stress in ***,in vivo

关键词： Diabetic retinopathy HIF-1α/BNIP3/NIX axis Mitophagy Heyingwuzi formulation Traditional Chinese medicine

Microwave-assisted Regioselective 1-O-Deacylation of Peracylated Glycopyranoses on Alumina

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Chinese Chemical Letters 2003年第9期14卷 904-906页

作者： Jia Qiang DONG, shu Jia zhang, yan Guang WANG Department of Chemistry, Zhejiang University, Hangzhou 310027 Department of Chemistry Zhejiang University Hangzhou 310027

A facile, rapid and regioselective method for the 1-O-deacylation of peracylated glycopyranoses is described which occurs under mild conditions by absorption onto alumina using microwave irradiation.

关键词： Deacylation sugars regioselectivity microwave irradiation.

Synthesis of a New Aromatic Dianhydride Containing Pyridine Ring and Related Polyimide

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Chinese Chemical Letters 2006年第3期17卷 305-306页

作者： Xiao Long WANG shu Jiang zhang yan Feng LI Tao MA Yu SHAO Xin ZHAO State Key Laboratory of Applied Organic Chemistry College of Chemistry and Chemical Engineering Lanzhou University Lanzhou 730000

A new aromatic dianhydride monomer containing pyridine moiety, 2,6-bis[4＇-（3＂,4＂- dicarboxyphenoxy）benzoyl]-pyridine dianhydride （Md）, was synthesized in four steps, starting from 2,6-pyridinedicarboxyl chloride. A novel pyridine-containing polyimide was prepared via polycondensation of Md with ODA by two-step method. The resulting polyimide exhibits excellent solubility, film-forming capability and high thermal resistance.

关键词： Polyimides pyridine-containing monomer synthesis aromatic dianhydride.

D-serine reduces memory impairment and neuronal damage induced by chronic lead exposure

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Neural Regeneration Research 2021年第5期16卷 836-841页

作者： Jian-Zhu Bo Ling Xue shuang Li Jing-Wen Yin Zheng-Yao Li Xi Wang Jun-Feng Wang yan-shu zhang College of Public Health North China University of Science and TechnologyTangshanHebei ProvinceChina Laboratory Animal Center North China University of Science and TechnologyTangshanHebei ProvinceChina

Although exogenous D-serine has been applied as a neural regulatory intervention in many studies,the role played by D-serine in hippocampal injuries caused by lead exposure remains poorly *** models of chronic lead exposure were established through the administration of 0.05%lead acetate for 8 ***,rats were administered 30 or 60 mg/kg D-serine,intraperitoneally,twice a *** results showed that D-serine treatment shortened the escape latency from the Morris water maze,increased the number of times that mice crossed the original platform location,and alleviated the pathological damage experienced by hippocampal neurons in response to lead *** D-serine administration did not increase the expression levels of the N-methyl-D-aspartate receptor subtype 2B(NR2B)in the hippocampi of lead-exposed rats,60 mg/kg D-serine treatment restored the expression levels of NR2A,which are reduced by lead *** findings suggested that D-serine can alleviate learning and memory impairments induced by lead exposure and that the underlying mechanism is associated with the increased expression of NR2A in the *** study was approved by the Animal Ethics Committee of North China University of Science and Technology,China(approval ***2018155)on December 21,2018.

关键词： D-serine hippocampus lead neurological function N-methyl-D-aspartate poisoning protection repair

Microstructure characteristics and mechanical properties of NbMoTiVWSix refractory high-entropy alloys

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China Foundry 2022年第6期19卷 495-502页

作者： Qin Xu Qi Wang De-zhi Chen Yi-ang Fu Qing-sheng Shi Ya-jun Yin shu-yan zhang School of Mechanic and Electrical Engineering Henan University of TechnologyZhengzhou 450001China National Key Laboratory for Precision Hot Processing of Metals Harbin Institute of TechnologyHarbin 150001China State Key Laboratory of Materials Processing and Die&Mould Technology Huazhong University of Science&TechnologyWuhan 430074China Centre of Excellence for Advanced Materials Songshan LakeDongguan 523808GuangdongChina

Refractory high-entropy alloys are considered as potential structural materials for elevated temperature *** obtain refractory high-entropy alloys with high strength,different amounts of Si were added into the NbMoTiVW refractory high-entropy *** effects of Si on the phase constitution,microstructure characteristics and mechanical properties of NbMoTiVWSi_(x) alloys were *** show that when the addition of Si is 0,0.025 and 0.05(molar ratio),the alloys are consisted of primary BCC and secondary BCC in the intergranular *** the addition of Si is increased to 0.075 and 0.1,eutectic structure including silicide phase and secondary BCC phase is *** primary BCC phase shows dendritic morphology,and is refined by adding *** volume fraction of intergranular area is increased from 12.22%to 18.13%when the addition of Si increases from 0 to *** ultimate compressive strength of the NbMoTiVW alloy is improved from 2,242 MPa to 2,532 *** yield strength is also improved by the addition of Si,and the yield strength of NbMoTiVWSi_(0.1) reaches maximum of 2,298 ***,the fracture strain of the alloy is decreased from 15.31%to 12.02%.The fracture mechanism of the alloys is changed from mixed fracture of ductile and quasi-cleavage to cleavage fracture with increasing of *** strengthening of alloys is attributed to the refinement of primary BCC phase,volume fraction increment of secondary BCC phase,and formation of eutectic structure by addition of Si.

关键词： high-entropy alloy second phase microstructure refinement mechanical property strengthening

Electrochemical and Spectroelectrochemical studies of Mixed-Valence Heteropolyanion VMo_(12)O_(40)^(n-)(n=4,5,6) in Aprotic Media

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Chinese Chemical Letters 1997年第10期8卷 909-912页

作者： shu yan zhang Hao Ran SUN Ji Qing XU Tong shun SHl(Department of Chemistry, Jilin University, Changchun 130023) JILIN UNIV DEPT CHEMCHANGCHUN 130023PEOPLES R CHINA

The mixed-valence heteropolyanion VMo12O40 n-(where n=4,5,6) in aprotic media wasinvestigated by cyclic voltammatry and in-situ FTIR and UV-visible-near-lRspectroelectrochemical methods. The results indicate that the heteropolyanion VMo12O403-undergoes three reversible one electron transfer reductions and the mixed-valenceheteropolyanion VMo12O40n-(where n=4,5,6) was formed after electroreduction. The spectraof the aforementioned mixed-valence compounds were characterized by in-situspectroelectrochemical mathods

关键词： Media n=4,5,6 VM Figure n in Aprotic Media Electrochemical and Spectroelectrochemical studies of Mixed-Valence Heteropolyanion VMo

B2-CuZr reinforced amorphous alloy matrix composites:A review

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China Foundry 2025年第1期22卷 1-11页

作者： Wei Guo Run-hua Huang Zhen zhang Mi Zhao Jin-cheng Wang yan-qiang Qiao shu-lin Lü shu-sen Wu State Key Lab of Materials Processing and Die&Mould Technology School of Materials Science and EngineeringHuazhong University of Science and TechnologyWuhan 430074China State Key Laboratory of Solidification Processing Northwestern Polytechnical UniversityXi’an 710072China School of Aerospace Engineering Huazhong University of Science and TechnologyWuhan 430074China Research Institute of Huazhong University of Science and Technology in Shenzhen Shenzhen 518057GuangdongChina

B2-CuZr phase reinforced amorphous alloy matrix composites has become one of the research hotspots in the field of materials science due to the“transformation-induced plasticity”phenomenon,which makes the composites show better macroscopic plastic deformability and obvious work-hardening behavior compared to the conventional amorphous alloy matrix composites reinforced with ductile ***,the in-situ metastable B2-CuZr phase tends to undergo eutectoid decomposition during solidification,and the volume fraction,size,and distribution of B2-CuZr phase are difficult to control,which limits the development and application of these *** date,much efforts have been made to solve the above problems through composition optimization,casting parameter tailoring,and post-processing *** this study,a review was given based on relevant studies,focusing on the predictive approach,reinforcing mechanism,and microstructure tailoring methods of B2-CuZr phase reinforced amorphous alloy matrix *** research focus and future prospects were also given for the future development of the present composite system.

关键词： amorphous alloy matrix composite B2-CuZr phase plasticity microstructure tailoring