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Magnetic,thermal stability and dynamic mechanical properties of beta isotactic polypropylene/natural rubber blends reinforced by NiZn ferrite nanoparticles

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Defence Technology（防务技术） 2019年第6期15卷 958-963页

作者： Lih-Jiun Yu Sahrim Hj Ahmad Ing Kong Mouad ATarawneh shamsul bahri bin abd.razak Elango Natarajan Chun Kit Ang Department of Mechanical Engineering Faculty of EngineeringTechnology and Built EnvironmentUCSI UniversityNo 1Jalan Menara GadingUCSI Heights(Taman Connaught)Cheras56000Kuala LumpurMalaysia School of Applied Physics Faculty of Science and TechnologyUniversity Kebangsaan Malaysia43600BangiSelangor Darul EhsanMalaysia School of Engineering and Mathematical Sciences La Trobe UniversityBundooraVIC3086Australia Department of Physics College of ScienceAl-Hussein Bin Talal UniversityP.O Box 20Ma'anJordan Department of Food Science and Technology University Malaysia TerengganuKuala NerusTerengganuMalaysia

The dispersion of magnetic nanoparticles in matrix is crucial to ensure optimum performance of the *** difficulty level of achieving good dispersion is further increase when a multi-phases of matrix is present.A pre-coating technique of magnetic nanoparticles with polypropylene using ball-mill prior to melt-blending process was employed to prepare a multi-phases thermoplastic natural rubber *** effect of filler loading(2 wt%-10 wt%) on morphology,structure,magnetic properties,thermal stability and dynamic mechanical properties of the composites were *** was found that the NiZn ferrite nanoparticles act as nucleating agent to form beta isostatic polypropylene thermoplastic *** composites’ magnetic properties are directly dependent on the filler *** dispersion of magnetic fillers in polymer matrix plays role in affecting the magnetic properties and thermal *** preference of filler to locate at amorphous phase has distorted the chain orientation of natural rubber and ***,the polymorphism and crystallinity of the matrix varied as the filler loading increased,affecting the dynamic mechanical *** was found that 8 wt% NiZn nanocomposite exhibits highest E’ and tanδ,indicating the dynamic mechanical properties of NiZn nanocomposite are affected by β-phase degree.

关键词： Magnetic Thermoplastic natural rubber Nanoparticles Composites

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The Effects of Sintering Temperature on the Densification of Mechanically Alloyed W-Brass Composites

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Open Journal of Metal 2015年第3期5卷 19-26页

作者： Baba Gowon Kahtan S. Mohammed shamsul Baharin bin Jamaluddin Zuhailawati Hussain Polycarp Evarastics School of Materials Engineering Universiti Malaysia Perlis (UniMAP) D/A Pajabat Pos Besar Kangar Malaysia Department of Metallurgical and Materials Engineering Federal Polytechnic Idah Nigeria School of Materials and Mineral Resources Engineering Engineering Campus Universiti Sains Malaysia Nibong Tebal Malaysia

Prealloyed (PA) and premixed (PM) W-brass with the composition of 60 wt% W, 1 wt% Ni and 39 wt% brass was sintered at the temperature of 800°C, 920°C and 1000°C each. As a result of difficulties in the densification of W-Cu and W-Cu alloys, mechanical alloying (MA) and activated sintering were combined. The powders were mechanically alloyed for 13 hours to produce nanosized W grains embedded in brass. The microstructure and properties of these composites with increase in sintering temperature has been studied. Both prealloyed and premixed composites sintered at 800°C (solid state sintering) and 920°C (sub-solidus state sintering) have lower sintered densities and hardness. The densification rate in the premixed composites was observed to be higher than that of the prealloyed composites. Their densification and properties increased with the increase in the sintering temperature. Premixed composite sintered at 1000°C had 91.0% sintered density, 180 Hv microhardness against 76.0% and 133 Hv respectively for prealloyed composite at the same temperature. The values of electrical conductivity in both prealloyed and premixed composites increased with increase in temperature.

关键词： W-Brass Temperature Densification Prealloy Hardness

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Synthesis and Densification of Tungsten-Brass Composite by Mechanical Alloying

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Open Journal of Metal 2015年第3期5卷 27-36页

作者： Kahtan S. Mohammed Baba Gowon shamsul Baharin bin Jamaluddin Zuhailawati Hussain Polycarp Evarastics School of Materials Engineering Universiti Malaysia Perlis (UniMAP) D/A Pajabat Pos Besar Kangar Malaysia Department of Metallurgical and Materials Engineering Federal Polytechnic Idah Nigeria School of Materials and Mineral Resources Engineering Engineering Campus Universiti Sains Malaysia Nibong Tebal Malaysia

Fabrication of full-density W-brass composites is very difficult to achieve because of evaporation of zinc, insolubility of W and brass and compacts expansion. In this study, to achieve full-density W-brass composites, mechanical alloying (MA) and activated sintering process were utilized. Mechanical coating of W with Ni using high energy planetary ball mill was carried out. The milling was divided into two stages: to alloy and modify the surface of W with Ni for enhanced activation. The microstructure of the milled powders and sintered compacts, elemental composition and phases present were studied by using scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX) and X-ray diffraction (XRD) respectively. As-received powder compacts was also sintered under the same condition for comparison purpose. The effects of milling time on the microstructure, sinterability and the hardness of the composites were investigated. It was observed that the samples produced from 8 h milled powder had the highest relative sintered density (98% TD) and microhardness (234 Hv). On the other hand, the samples from the as-received powders expanded and had a relative sintered density of (67% TD) and microhardness as low as 24 Hv. The significance of this study is the possibility of producing W-brass composites as a cheaper alternative to W-Cu composites.

关键词： W-Brass Mechanical Alloying Microstructure Expansion Hardness

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Comparative Analysis of Polyphenolic and Antioxidant Constituents in Dried Seedlings and Seedless Acacia nilotica Fruits

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Journal of Analysis and Testing 2018年第4期2卷 352-355页

作者： Amani abdErahman Olalere Olusegun Abayomi abdElhafiz Eltahir Ahmed abdurahman Hamid Nour Rosli bin Mohd Yunus Ghada Mohamed Ibrahim Nassereldeen Ahmed Kabbashi Faculty of Science and Technology Omdurman Islamic UniversityOmdurmanSudan Faculty of Chemical and Natural Resources Engineering Universiti Malaysia PahangGambangMalaysia Faculty of Animal Production Bahri UniversityBahriSudan International Islamic University Malaysia MalaysiaKOEBTE EngineeringKuala LumpurMalaysia

The phenolic and antioxidant constituents in Acacia nilotica fruits have become an important source of medicinal and thera-peutic benefit with powerful biological *** study investigated the phenolic content and antioxidant capacity of powdered Acacia fruits with seeds and without *** phenolic content and antioxidant capacities in them were deter-mined using Folin-Ciocalteu and DPPH free radical-scavenging *** total phenolic and antioxidants of *** with seeds were spectrophotometrically determined to be 47.61 and 6.18%greater than when the seeds were removed from the dried fruits,*** LC-MS/QTOF analysis shows the presence of 282 and 214 phenolic compounds in the methanol extracts of *** with seeds and without seeds,*** present study,therefore,revealed that dried *** fruits with seeds have higher total phenolic content,antioxidant capacity,and bioactive constituents,which indi-cated that they have more medicinal value than fruits without seeds.

关键词： Acacia nilotica Liquid chromatography-mass spectrometry Total phenolic content DPPH antioxidant capacity

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