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Journal of Pharmaceutical Analysis 2022年第2期12卷 253-262页

作者： Abir Chamandy Minjie Zhao Hassan Rammal saïd.ennahar Analytical Chemistry of Bioactive Molecules and Pharmacognosy Team(CAMBAP) Hubert Curien Multidisciplinary Institute(IPHC)National Center for Scientific Research(CNRS)Faculty of PharmacyUniversity of StrasbourgIllkirch67400France Research Platform of Analysis and Environmental Science(PRASE) Lebanese UniversityHadath005Lebanon Faculty of Agronomy Lebanese UniversityDekwaneh005Lebanon

The compounds in leaf and stem extracts of Astragalus emarginatus Labill.(AEL),a plant species used in traditional Lebanese medicine,were investigated for antioxidant ***,the activity of various extracts was assessed using the Trolox equivalent antioxidant capacity,oxygen radical absorption capacity,and 2,2-diphenyl-1-picryl-hydrazyl-hydrate *** extract obtained using 30%ethanol showed the greatest *** antioxidant compounds in this extract were screened using a hyphenated high-performance liquid chromatography-2,2-azinobis-(3-ethylbenzothiazoline-6-sulfonate)radical(ABTS$t)system before being separated by ultra-high-performance liquid chromatography and identified using high-resolution mass spectrometry and ultra-violet-visible diode array *** 40 compounds were ***(caffeic,ferulic,and p-coumaric acid derivatives)and flavonoids(quercetin,luteolin,apigenin,and isorhamnetin derivatives)were the two main categories of the identified *** active compounds were identified as caffeic acid derivatives and quercetin *** addition,the catechol moiety was shown to be key to antioxidant *** study showed that AEL is a source of natural antioxidants,which may explain its medicinal use.

关键词： Antioxidant Astragalus emarginatus Catechol Flavonoids Hydroxycinnamates Caffeic acid Quercetin

Effects of human disturbance on nest placement of the woodpigeon (Columba palumbus): a case study from the Middle Atlas, Morocco

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Integrative Zoology 2014年第3期9卷 349-359页

作者： saâd HANANE Forest Research Center High Commissariat for WaterForests and Desertification ControlRabat-AgdalMorocco

The woodpigeon(Columba palumbus)is a common and widespread bird in Morocco(North Africa).I examined,over 2 years(2010 and 2011),the breeding density and nest placement of this game species in relation to nest site habitat and degree of human *** study area was in the Middle Atlas Tighboula mountain forest,Morocco,in a disturbed and an undisturbed *** data collected in the 2 study sites,I aimed to identify the factors influencing the placement of nests within holm oak trees(Quercus rotundifolia)and their densities.I found that habitat structures,influenced by grazing disturbance,have affected nesting density and the location of nests of this *** place their nests in a higher position(3.42±0.19 m)when disturbance intensity is high and lower(1.68±0.1 m)when disturbance intensity is low,and show higher nesting density in less disturbed zone(3.1±0.4 nests/ha)than in highly disturbed zones(1.4±0.2 nests/ha).Grazing disturbance could pose a threat to population persistence at a broader scale and could potentially reduce the abundance of this species by altering the composition and the structure of the forest nesting *** multi-scale studies are needed to assess the effects of different levels of grazing disturbance on woodpigeon nest density and placement,and to enhance our knowledge of the breeding behavior of this game species under variable environments.

关键词： breeding density Columba palumbus holm oak Middle Atlas Morocco nest location woodpigeon

PYRIdINATION OF POLY(VINYL CHLORIdE) via A HOMOLYTIC PATHWAY

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Chinese Journal of Polymer Science 2007年第3期25卷 297-302页

作者： sad Moulay Zakia Zeffouni Laboratoire de Chimie-Physique Moléculaire et Macromoléculaire Faculté des Sciences de l'Ingénieur Département de Chimie IndustrielleUniversité Sad Dahlab de BlidaRoute de SoumaB. P. 270Blida 09000Algeria

PVC was subjected to a chemical modification aiming at replacing the chlorine atoms by pyridine groups via a homolytic route. Pyridine groups were peculiarly affixed to the PVC matrix via a carbon-carbon bond rather than a carbonnitrogen one. PVC was first iodinated using the Conant-Finkelstein reaction, followed by the application of the homolytic conditions of Minisci to generate pyridinated PVC with a varying degree of substitution. The extent of substitution was not high; the reaction on 30% iodinated PVC afforded a degree of modification no greater than 3%.

关键词： Conditions of Minisci Iodinated PVC Pyridinated PVC

HALOMETHYLATION OF POLYSTYRENE ANd SUBSEQUENT PYRIdINATION VIA A HOMOLYTIC PATHWAY

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Chinese Journal of Polymer Science 2006年第6期24卷 627-635页

作者： sad Moulay Nadia Mehdi Laboratoire de Chimie-Physique Moléculaire et Macromoléculaire Faculté des Sciences de l'Ingénieur Departement de Chimie IndustrielleUniversité de BlidaRoute de SoumaB. P. 270Blida 09000Algeria

Chloromethylation of polystyrene （PS） with two different chloromethylating systems methylal/thionyl chloride and paraformaldehyde/trimethylchlorosilane was studied. Soluble chloromethylated polystyrene with a degree of substitution of 89% was obtained. The Conant-Finkelstein reaction on the chloromethylated PS afforded soluble iodomethylated polystyrene with a degree of substitution as high as 96%. The reaction conditions of Minisci were employed to radically pyridinate PS via its iodomethylated derivative. Polyelectrolytes were formed which could be converted to normal polymers by treatment with a 20% aqueous solution of NaOH.

关键词： Chloromethylated polystyrene Conditions of Minisci Iodomethylated polystyrene Pyridinated polystyrene.

A location-based fog computing optimization of energy management in smart buildings:dEVS modeling and design of connected objects

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Frontiers of Computer Science 2023年第2期17卷 179-195页

作者： Abdelfettah MAATOUG Ghalem BELALEM saïd MAHMOUdI Computer Science department Faculty of Exact and Applied SciencesUniversity of Oran 1 Ahmed Ben BellaOran 31000Algeria Science and Technology department Faculty of Science and TechnologyUniversity of TIARETTiaret 14000Algeria Computer Science department Faculty of EngineeringUniversity of MonsMons 7000Belgium

Nowadays,smart buildings rely on Internet of things(loT)technology derived from the cloud and fog computing paradigms to coordinate and collaborate between connected *** is characterized by low latency with a wider spread and geographically distributed nodes to support mobility,real-time interaction,and location-based *** provide optimum quality of user life in moderm buildings,we rely on a holistic Framework,designed in a way that decreases latency and improves energy saving and services efficiency with different *** EVent system Specification(dEVS)is a formalism used to describe simulation models in a modular *** this work,the sub-models of connected objects in the building are accurately and independently designed,and after installing them together,we easily get an integrated model which is subject to the fog computing *** results show that this new approach significantly,improves energy efficiency of buildings and reduces ***,with dEVS,we can easily add or remove sub-models to or from the overall model,allowing us to continually improve our designs.

关键词： smart building energy consumption IoT fog computing Framework dEVS simulation models

SYNTHESIS OF SOLUBLE POLY(3,4-dIHYdROXY-o-TOLYLENE):REdOX POLYMER

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Chinese Journal of Polymer Science 2006年第1期24卷 41-46页

作者： sad Moulay Fatima M'zyène Laboratoire de Chimie-Physique Moléculaire et Macromoléculaire Faculté des Sciences de l'Ingénieur département de Chimie Industrielle Université de BlidaRoute de SoumèaB.P.270Blida 09000Algeria. Laboratoire de Chimie-Physique Moléculaire et Macromoléculaire Faculté des Sciences de l'Ingénieur département de Chimie Industrielle Université de BlidaRoute de SoumaB.P.270Blida 09000Algeria.

Conventional chloromethylation, paraformaldehyde/hydrogen chloride in acetic acid medium, was applied to 1,2- dimethoxybenzene. Chloroform-soluble poly（3,4-dimethoxy-o-tolylene） was obtained with an intrinsic viscosity of 0.034 dL g^-1. The polymer was evaluated as a condensation redox polymer precursor formed by a Friedel-Crafts reaction. Cleavage of the methoxy groups present in this polymer resulted in poly（3,4-dihydroxy-o-tolylene） which manifested a great air-oxidation resistance. The redox property of the latter polymer was found to be 1017 mV by potentiometric titration with 0.05 N ceric ammonium nitrate at 25℃. This midpotential was compared to that of catechol, a monomeric analogue, under the same titration conditions.

关键词： Poly(3,4-dimethoxy-o-tolylene) Poly(3,4-dihydroxy-o-tolylene) Redox polymer.

Seasonal variability in CdOM absorption and fluorescence properties in the Barataria Basin,Louisiana,Usa

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Journal of Environmental Sciences 2010年第10期22卷 1481-1490页

作者： Shatrughan Singh Eurico d'sa Erick Swenson department of Oceanography and Coastal Sciences Louisiana State University

Absorption and fluorescence properties of chromophoric dissolved organic matter （CdOM） along a 124 km transect in the Barataria Basin, a large estuary located in Louisiana, Usa, were investigated during high and low flow periods of the Mississippi River in the spring and winter of 2008-2009. Mean CdOM absorption at 355 nm from the marine to the freshwater end member stations ranged from （3.25 ± 0.56） to （20.76 ± 2.43） m^-1 for the three month high flow period whereas it varied from （1.48 ± 1.08） to （25.45 ± 7.03） m^-1 for the same stations during low flow period. Corresponding salinity values at these stations indicated the influence of river and shelf exchanges in the lower basin and precipitation and runoff in the upper basin. An inverse relationship of CdOM absorbance and fluorescence with salinity observed in the basin could he a useful indicator of salinity. CdOM fluorescence also varied over a large range showing an approximately 8 to 12-fold increase between the marine and freshwater end members for the two flow seasons. Excitation-emission matrix spectral plots indicated the presence of various fluorescence components with highest being the A-peak, lowest the T-peak, and the C and M-peaks showing similar trends along the transect. during low flow season the A/C ratio were well correlated with station locations indicating increased terrestrial influence towards the upper basin. CdOM absorption and fluorescence at 355 nm were highly correlated and independent of CdOM sources suggesting that fluorescence could be used to characterize CdOM in the basin.

关键词： Barataria Basin chromophoric dissolved organic matter CdOM fluorescence excitation-emission matrix

Biochemical dissection of STAT3 signaling in amyotrophic lateral sclerosis

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Neural Regeneration Research 2025年第11期20卷 3229-3230页

作者： savina Apolloni Nadia d’Ambrosi department of Biology University of Rome Tor VergataRomeItaly

Amyotrophic lateral sclerosis(ALS)is a progressive neurodegenerative disease characterized by the loss of upper and lower motor neurons,clinically marked by muscle atrophy and *** the clinical course is highly variable,the average time from the onset of symptoms to the need for respiratory support or death is 3-5 *** is the most prevalent motor neuron disease in adults,occurring at a rate of 2 per 100,000 individuals and affecting 5.4 per 100,000 individuals overall.

关键词： STAT3 dissection sclerosis

Quaternionic Monge–Ampère Measure on Pluripolar Set

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Acta Mathematica Sinica,English Series 2024年第6期40卷 1431-1457页

作者： Hichame AMAL saïd ASSERdA Fadoua BOUKHARI department of Mathematics Laboratory LaREAMIRegional Centre of Trades of Education and TrainingKenitraMorocco Ibn Tofail University Faculty of SciencesDepartment of MathematicsPO 242 KenitraMorroco

In this paper, we prove that in a hyperconvex domain Ω in H^(n), if a non-negative Borel measure is dominated by a quaternionic Monge–Ampère measure, then it is a quaternionic Monge–Ampère measure of a function i... 详细信息

关键词： Quaternion space Monge-Amp`ere operator plurisubharmonic function

Analysis and optimal synthesis of single loop spatial mechanisms

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Journal of Zhejiang University-Science A(Applied Physics & Engineering) 2011年第9期12卷 665-679页

作者： Med Amine LARIBI Lotfi ROMdHANE sad ZEGHLOUL Laboratoire de Génie Mécanique LAB-MA-05 Ecole Nationale d'Ingénieurs de Sousse Institut Pprime-UPR 3346 CNRS-Université de Poitiers-ENSMA Département Génie Mécanique et Systémes Complexes SP2MIBP30179 86962 Futuroscope France

In this work, a systematic approach is presented to obtain the input-output equations of a single loop 4-bar spatial mechanisms. The dialytic method along with denavit-Hartenberg parameters can be used to obtain these equations efficiently. A genetic algorithm （GA） has been used to solve the problem of spatial mechanisms synthesis. Two types of mechanisms, e.g., RSCR and RSPC （R： revolute; S： spherical; C： cylindrical; P： prismatic）, have illustrated the application of the GA to solve the problem of function generation and path generation. In some cases, the GA method becomes trapped in a local minimum. A combined GA-fuzzy logic （GA-FL） method is then used to improve the final result. The results show that GAs, combined with an adequate description of the mechanism, are well suited for spatial mechanism synthesis problems and have neither difficulties inherent to the choice of the initial feasible guess, nor a problem of convergence, as it is the case for deterministic methods.

关键词： Spatial mechanisms Genetic algorithm-fuzzy logic (GA-FL) method denevit-Hartenberg parameters Mechanism synthesis