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Experimental Design Technique on Removal of Hydrogen Sulfide using CaO-eggshells Dispersed onto Palm Kernel Shell Activated Carbon：Experiment,Optimization,Equilibrium and Kinetic Studies

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Journal of Wuhan University of Technology(Materials Science) 2017年第2期32卷 305-320页

作者： OMAR Abed Habecb RAMESH Kanthasamy GOMAA A. M. Ali rosli bin mohd yunus Faculty of Chemical & Natural Resources Engineering Universiti Malaysia Pahang Gambang 26300 Kuantan Malaysia Faculty of Industrial Sciences and Technology Universiti Malaysia Pahang Gambang 26300 Kuantan Malaysia Chemistry Department Faculty of Science Al-Azhar University Assiut 71524 Egypt Al-Azhar Center of Nanoscience and Applications (ACNA) Al-Azhar University Assiut 71524 Egypt.

This study presents the use of chicken eggshells waste utilizing palm kernel shell based activated carbon（PKSAC） through the modification of their surface to enhance the adsorption capacity of H2S. Response surface methodology technique was used to optimize the process conditions and they were found to be： 500 mg/L for H2S initial concentration, 540 min for contact time and 1 g for adsorbent mass. The impacts of three arrangement factors（calcination temperature of impregnated activated carbon（IAC）, the calcium solution concentration and contact time of calcination） on the H2S removal efficiency and impregnated AC yield were investigated. Both responses IAC yield（IACY, %） and removal efficiency（RE, %） were maximized to optimize the IAC preparation conditions. The optimum preparation conditions for IACY and RE were found as follows： calcination temperature of IAC of 880 ℃, calcium solution concentration of 49.3% and calcination contact time of 57.6 min, which resulted in 35.8% of IACY and 98.2% RE. In addition, the equilibrium and kinetics of the process were investigated. The adsorbent was characterized using TGA, XRD, FTIR, SEM/EDX, and BET. The maximum monolayer adsorption capacity was found to be 543.47 mg/g. The results recommended that the composite of PKSAC and Ca O could be a useful material for H2S containing wastewater treatment.

关键词： water treatment hydrogen sulfide response surface methodology optimization activated carbon adsorption isotherm kinetics calcium oxide

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Comparative Analysis of Polyphenolic and Antioxidant Constituents in Dried Seedlings and Seedless Acacia nilotica Fruits

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Journal of Analysis and Testing 2018年第4期2卷 352-355页

作者： Amani AbdErahman Olalere Olusegun Abayomi AbdElhafiz Eltahir Ahmed Abdurahman Hamid Nour rosli bin mohd yunus Ghada Mohamed Ibrahim Nassereldeen Ahmed Kabbashi Faculty of Science and Technology Omdurman Islamic UniversityOmdurmanSudan Faculty of Chemical and Natural Resources Engineering Universiti Malaysia PahangGambangMalaysia Faculty of Animal Production Bahri UniversityBahriSudan International Islamic University Malaysia MalaysiaKOEBTE EngineeringKuala LumpurMalaysia

The phenolic and antioxidant constituents in Acacia nilotica fruits have become an important source of medicinal and thera-peutic benefit with powerful biological *** study investigated the phenolic content and antioxidant capacity of powdered Acacia fruits with seeds and without *** phenolic content and antioxidant capacities in them were deter-mined using Folin-Ciocalteu and DPPH free radical-scavenging *** total phenolic and antioxidants of *** with seeds were spectrophotometrically determined to be 47.61 and 6.18%greater than when the seeds were removed from the dried fruits,*** LC-MS/QTOF analysis shows the presence of 282 and 214 phenolic compounds in the methanol extracts of *** with seeds and without seeds,*** present study,therefore,revealed that dried *** fruits with seeds have higher total phenolic content,antioxidant capacity,and bioactive constituents,which indi-cated that they have more medicinal value than fruits without seeds.

关键词： Acacia nilotica Liquid chromatography-mass spectrometry Total phenolic content DPPH antioxidant capacity

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Extraction of Keratin Protein from Chicken Feather

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Journal of Chemistry and Chemical Engineering 2012年第8期6卷 732-737页

作者： Arun Gupta Nuruldiyanah Bimi Kamarudin Chua Yeo Gek Kee rosli Bin mohd yunus Faculty of Chemical and Natural Resources Engineering University Malaysia Pahang Gambang Campus Pahang 25100 Malaysia

The present research was conducted to extract keratin protein from chicken feathers. Protein is an important nutrient needed by our body to maintain body structures and is an important ingredient for cosmetic products. Chicken feathers have high level of keratin protein content and can become a suitable protein source. The main processes involved are first dissolving chicken feathers using different reducing agents and later on separating the protein from chemicals. Reducing agents used are potassium cyanide, thioglycolic acid and sodium sulphide. Once the feathers are dissolved using reducing agents, ammonium sulfate solution is added to the solution for the precipitation of protein. The precipitated protein is washed with water several times and sodium hydroxide solution is used to obtain protein back in the solution form. Out of three different reducing agents used, sodium sulfide gives the highest efficiency in dissolving chicken feathers since the feathers are dissolved in a very short period of time. The percentage of keratin protein is evaluated by means of biuret test and FTIR analysis. The analysis by FTIR confirmed the presence of carboxyl acid and amino groups in the protein solution. The biuret test helps in determining the concentration of protein obtained from different methods. Thus these two tests confirm the presence of protein in the solution. From this research, it can be concluded that protein can be extracted from chicken feathers. The keratin protein solution can be used for several purposes such as anti-aging cream, shampoo, and conditioner and for medical purposes such as bone replacement and bone graft.

关键词： Chicken feather reducing agents protein precipitation analysis.

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<i>In-Situ</i>Impregnation of Copper Nanoparticles on Palm Empty Fruit Bunch Powder

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Advances in Nanoparticles 2014年第3期3卷 65-71页

作者： Ridzuan Ramli Md. Maksudur Rahman Khan rosli mohd yunus Huei Ruey Ong Rohaya Mohamed Halim Astimar Abdul Aziz Zawawi Ibrahim Nahrul Hayawin Zainal Faculty of Chemical and Natural Resources Engineering Universiti Malaysia Pahang Kuantan Malaysia Malaysian Palm Oil Board (MPOB) No. 6 Persiaran Institusi Kajang Malaysia Malaysian Palm Oil Board (MPOB) No. 6 Persiaran Institusi Kajang Malaysia Faculty of Chemical and Natural Resources Engineering Universiti Malaysia Pahang Kuantan Malaysia

Copper nanoparticles were impregnated onto oil palm empty fruit bunch (EFB) powders via in-situ sol-gel method. The impregnation and interfacial interaction of copper nanoparticles with EFB were analysed by fourier transformed infrared spectroscopy (FTIR), X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), energy dispersive X-ray (EDX) and atomic force microscopy (AFM). The interaction of copper nanoparticles with the surface functional groups of EFB powders was identified by FTIR analysis. The peak shift of O-H and C-O functional groups indicated the interaction between EFB and copper nanoparticles. Besides that, XRD and EDX analysis confirmed the formation of copper nanoparticles on EFB powder. Due to the copper impregnation, the crystallinity of the EFB was increased as shown by XRD. The particles size of nanoparticles was analysed via TEM and AFM where the sizes were in the range of 60 - 100 nm. These findings strongly suggest that, copper nanoparticles impregnated EFB powders can be synthesized via in- situ sol gel method.

关键词： Copper Nanoparticles In-Situ Empty Fruit Bunch Sol-Gel

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Comparative study of ethanol foamed asphalt binders and mixtures prepared via manual injection and laboratory foaming device

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Journal of Traffic and Transportation Engineering(English Edition) 2019年第4期6卷 383-395页

作者： mohd rosli mohd Hasan Zhanping You School of Civil Engineering Universiti Sains MalaysiaNibong Tebal 14300Pulau PinangMalaysia Department of Civil and Environmental Engineering Michigan Technological UniversityHoughtonMI 49931USA

The consistency of the ethanol foamed binders and mixtures prepared using asphalt binders foamed by the manual injection technique and laboratory foaming device were evaluated and compared in this study. The asphalt binders foamed using both methods was prepared at 120℃, 130℃ and 140℃. The performance of ethanol-foamed binders was evaluated in terms of rotational viscosity, expansion ratio, and low temperature ***, the performance of foamed WMA mixtures was tested using semi-circular bending(SCB), disk-shaped compact tension(DCT), and tensile strength ratio(TSR) tests. In order to conduct the TSR test, the samples were conditioned using the Moisture Induced Stress Tester(MIST) to simulate the pore pressure and scouring effects due to a tire passing over wet pavement. The foamed WMA mixtures were produced using pre-heated aggregates at 80℃ and 100℃ and foamed asphalt binders produced at 130℃. The nano-hydrated lime was used as the filler and anti-stripping agent. Overall, the properties of ethanol-foamed binders and WMA mixtures produced via both methods are significantly comparable, except the resistance to moisture damage test result. However, the findings indicate that the ethanol-foamed WMA mixtures prepared using both techniques are having good resistance to moisture damage, based on the TSR values more than 0.8. The foamed WMA mixtures also exhibited a better resistance to cracking, as indicated by a higher tensile strength compared to the control HMA. Additionally, the WMA specimen prepared at 100℃ was less susceptible to rutting than the samples produced at 80℃.

关键词： Warm mix asphalt Foaming technique Rheological Foam quality Mixture performance

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Preparation process of bio-oil and bio-asphalt,their performance,and the application of bio-asphalt:A comprehensive review

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Journal of Traffic and Transportation Engineering(English Edition) 2020年第2期7卷 137-151页

作者： Hainian Wang Ziye Ma Xi Chen mohd rosli mohd Hasan School of Highway Chang'an UniversityXi'an 710064China School of Civil Engineering Universiti Sains MalaysiaNibong Tebal 14300Pulau PinangMalaysia

The objective of this paper is to establish the state of knowledge on fast pyrolysis of bio-oil and bio-asphalt binder and to facilitate efforts in improving the overall perform ance of bioasphalt and maximizing its road *** the basis of reviewing the relevant literature recently,the fast pyrolysis(FasP) preparation process of bio-oil and its main properties,the preparation process of bio-asphalt and its performance and the application of bio-asphalt have been *** to the variations in raw materials,the adopted methods of FasP to prepare bio-oil could be different,and the properties of bio-oil from different sources are also *** present,the plant-based bio-oil(mainly derived from wood waste and sawdust) has been widely used to prepare the *** on the low-temperature flexibility,high-temperature rheology,workability and other performance of biological asphalt showed that the workability and high-temperature performance of most asphalt are improved after adding ***,the low-temperature performance is found to relatively ***,with regards to its application as a rejuvenator,bio-oil can considerably rejuvenate the aged asphalt’s mixture *** far,most of research on bio-asphalt is still focused on the performance of bio-asphalt binder in the laboratory;its application in practical road engineering is still to be *** review also provides an outlook for the future,for example,establishing an integrated preparation process from bio-oil to bio-asphalt,and evaluating the properties of bioasphalt by new standards.

关键词： Road engineering Bio-oil Bio-asphalt Preparation process Performance Application of bio-asphalt

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Recent development,utilization,treatment and performance of solid wastes additives in asphaltic concrete worldwide:A review

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Journal of Traffic and Transportation Engineering(English Edition) 2022年第5期9卷 693-724页

作者： Tracy Leh Xin Wong mohd rosli mohd Hasan Leo Choe Peng School of Civil Engineering Universiti Sains Malaysia14300 Nibong TebalPinangMalaysia School of Chemical Engineering Universiti Sains Malaysia14300 Nibong TebalPinangMalaysia

Asphalt modifications either involved commercial or recycled waste materials modifiers help optimise and improve the deficient properties of asphalt mixtures relative to current *** manuscript reviews the recycling of waste materials generated from various sources such as household,agricultural and industrial to minimise natural resources exploitation,lower energy demand,and enhance overall pavement *** actual development and implementation of recycled asphalt pavement in numerous countries in Asia,North America,South America,Europe and Africa are emphasised,and their influence on the performance of asphalt pavements is *** pavement showed satisfying performance for years as maintenance and restoration are not ***,solid wastes are required to undergo pre-requisite treatments via mechanical,biological stabilization,thermal or chemical methods before the implementation as asphalt modifiers to ease the handling *** damage issues have been spotted in the implementation of several types of solid wastes and consequently reduced the strength and durability of ***,potential hydrophobic treatment can be adopted to improve the quality of asphalt mixtures by modifying the hydrophilic characteristics that are contributed by the hydroxyl groups on the cellulose nanocrystals(CNCs)or providing a superhydrophobic coating onto the *** treatments greatly weakened the moisture sensitivity of modified materials by reducing their water absorption and increasing their water contact *** modified mixtures are necessary to have identical or enhanced pavement performance to the conventional ***,future researchers are encouraged to broaden the research field in pavement engineering by considering chemical treatments in improving material properties to achieve cost-saving,efficient waste management,and higher commercial *** implementing any virgin materials,waste material

关键词： Sustainable pavement Industrial waste Cleaner environment Resources preservation Hydrophobic treatments Mechanical performances

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Ethanol based foamed asphalt as potential alternative for low emission asphalt technology

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Journal of Traffic and Transportation Engineering(English Edition) 2016年第2期3卷 116-126页

作者： mohd rosli mohd Hasan Zhanping You Department of Civil and Environmental Engineering Michigan Technological University School of Civil Engineering Universiti Sains Malaysia

Foamed asphalt typically relies on water as a foaming agent because water becomes gaseous at elevated temperatures, generating numerous tiny bubbles in the asphalt and causing spontaneous foaming. In this study, ethanol was used as a potential alternative to water as a foaming agent. Ethanol is expected to be a physical blowing agent in the same manner as water, except it requires less energy to foam due to its 78 ℃ boiling point. This study compares the performance of water and ethanol as foaming agents through the measurements of rotational viscosity, the reduction in temperature during foaming, and volatile loss. The ethanol-foamed asphalt binders were prepared at 80 ~C and 100 ~C, while the water-foamed asphalt binders were prepared at 100 ~C and 120 ~＇C. Additionally, the rolling thin film oven （RTFO） was used to generate short-term aging of the foamed asphalt binders. A rotational viscometer was used to determine the viscosity of the asphalt binders at 80 ~C, 100 ~C, 120 ~C, 140 ~C, and 160 ~C. Overall, ethanol can function in the same manner as water but requires less energy to foam. It is proven based on the smaller drop in temperature of the asphalt binder foamed using ethanol compared with that prepared with water. This is due to the lower latent heat capacity of ethanol, which requires less energy to vaporize compared with water. Through the rotational viscometer test, ethanol performs better in lowering the viscosity of asphalt binders, which is essential in allowing produc- tion processes at low temperatures, as well as a better workability and aggregate coating. Ethanol can be expelled from the foamed asphalt binders at a higher rate due to its lower boiling point and latent heat.

关键词： Warm mix asphalt Foaming agent Ethanol-based foaming Expulsion rate Aging factor

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Review of sustainability, pretreatment, and engineering considerations of asphalt modifiers from the industrial solid wastes

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Journal of Traffic and Transportation Engineering(English Edition) 2019年第3期6卷 209-244页

作者： mohd rosli mohd Hasan J-Wei Chew Ali Jamshidi Xu Yang Meor Othman Hamzah School of Civil Engineering Universiti Sains Malaysia Nibong Tebal 14300 Pulau Pinang Malaysia School of Highway Chang'an University Xi'an 710064 China School of Science and Engineering University of Sunshine Coast Sippy Downs Queensland 4556 Australia Department of Civil Engineering Monash University Melbourne Victoria 3168 Australia

The escalating mass of solid waste at an overwhelming sum requires a global attention to strive for efficient waste management and to outsource the ecological treatments. The asphalt pavement industry that consumes a vast scale of natural resources while contributing to thermal and greenhouse emissions is viewed as a high potential alternative for the application of solid waste as asphalt modifier and substantial waste reduction. In efforts to urge for cleaner and greener asphalt production, a growing trend towards usage of solid waste as a renewable material is paving a sustainable future for the asphalt pavement industry. The economic options of incorporating solid waste into the asphaltic mixture coupled with proven effective performances are a green and cost-effective alternative to mitigate various pavement distresses. Various options either as coarse or fine aggregates and as fillers in powder, ash, or fibre form are to stimulate further research interest to incorporate a diversified range of solid waste into the asphalt binder and asphalt mixture. Prior to incorporating solid waste into the asphaltic mixture through the selected options, prerequisite tests in addressing engineering limitations due to the unknown properties of solid waste are reviewed. The concerns on environmental impact are given heavy metals leaching possibilities into water sources are addressed by Toxicity Characterization Leaching Procedure test, to leverage further the systematic reuse of solid waste in steering towards the cleaner production of the asphalt mixture. The microcosmic traits of solid waste namely surface morphology, mineralogical composition and chemical composition are summarized based on the usage of Scanning Electron Microscope, X-Ray Diffraction, and X-Ray Fluorescence, respectively. This systematic review is an enactment and stimulus for researchers to have a general overview before incorporating solid waste into asphalt mixture.

关键词： Asphalt modifier Waste materials Clean production Energy Carbon footprint Green pavement

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Experimental assessments of methanol-based foaming agent in latex modified foamed binders and warm asphalt mixtures

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Journal of Road Engineering 2022年第1期2卷 84-97页

作者： mohd rosli mohd Hasan Tai Guo Hainian Wang Zul Fahmi Mohamed Jaafar Zhanping You School of Civil Engineering Universiti Sains Malaysia(Engineering Campus)Nibong Tebal 14300Pulau PinangMalaysia School of Highway Chang'an UniversityXi'an 710064China Department of Civil and Environmental Engineering Michigan Technological UniversityHoughtonMI 49931USA

Latex is one of the natural rubbers that is used to enhance the performance of asphalt pavement for the last few *** presence of latex,which is categorized as an elastomer,helps to improve pavement performance and ***,higher viscosity of latex modified asphalt binder increases the production-temperatures of asphalt mixture,thus consuming higher energy during asphalt mixture’s production *** this study,the effectiveness of methanol as an energy-efficient foaming agent was assessed to reduce the viscosity and enhance the workability of the modified asphalt *** basic and rheological properties of the asphalt binders were determined through multiple laboratory tests including expansion ratio and half-life,rotational viscosity,softening point,torsional recovery,and dynamic shear *** properties of asphalt mixtures were assessed through the service characteristics,mechanical performance,and moisture resistance *** was found that the presence of latex results in an approximately twofold higher expansion ratio and a lower half-life of the asphalt binder at about the same *** the rotational viscosity test,the application of methanol into asphalt binder decreased the viscosity and led to better workability,despite the addition of latex as an asphalt *** application of methanol into asphalt binder improved the workability of mixture samples and lowered the compaction energy of the compaction process,which are the crucial criteria for a better mixing and compaction *** foamed asphalt mixtures with latex show much higher resistance to moisture damage and stiffness than control sample even though they were prepared at a lower temperature.

关键词： Foaming agent Foaming technique Latex Lower energy Methanol Natural rubber

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