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Journal of Materials Science & Technology 2024年第2期169卷 235-242页

作者： H.X.Lu H.Liu Z.Z.Fu Y.Y.Chen H.q.Dai Z.Hu W.L.Zhang r.q.guo Institute for Electric Light Sources School of Information Science and TechnologyFudan UniversityShanghai 200433China Institute of Future Lighting Academy for Engineering and TechnologyFudan UniversityShanghai 200433China Yiwu research Institute of Fudan University YiwuZhejiang 322000China Zhongshan-Fudan Joint Innovation Center Zhongshan 528437China

In this study,a two-step method was used to synthesize highly luminescent AgGaS/ZnS/ZnS quantum dots(qDs).In the first step,an inner ZnS shell was formed via a one-pot method,which resulted in a smaller lattice mismatch between the AgGaS core and the outer ZnS shell,thereby facilitating the formation of a thick outer *** the two-step shelling process,the synthesized AgGaS/ZnS/ZnS qDs showed an excellent photoluminescence quantum yield(PLqY)of 96.4%with a peak wavelength of 508 nm,repre-senting the highest PLqY reported thus far for AgGaS ***,the effect of halogen ions in Zn precursors on the shelling process was *** was proposed that the capacity of halogen ions to coordinate with the qDs influenced the balance between Zn cation diffusion and ZnS shelling ***,the ZnS shelling reaction was dominant when ZnCl_(2)was employed,while Zn cation diffusion was the dominant process under the I^(−)-rich *** work provides insights into the interfacial restructuring during the ZnS shelling and offers a clear map for the tailored synthesis of core/shell qDs.

关键词： AgGaS quantum dots Photoluminescence Core/shell Alloyed core/shell interface

Multiple Tin Compounds Modified Carbon Fibers to Construct Heterogeneous Interfaces for Corrosion Prevention and Electromagnetic Wave Absorption

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Nano-Micro Letters 2025年第1期17卷 507-527页

作者： Zhiqiang guo Di Lan Zirui Jia Zhenguo Gao Xuetao Shi Mukun He Hua guo Guanglei Wu Pengfei Yin College of Science Sichuan Agricultural UniversityYa’an 625014People’s Republic of China School of Materials Science and Engineering Hubei University of Automotive TechnologyShiyan 442002People’s Republic of China Institute of Materials for Energy and Environment State Key Laboratory of Bio‑Fibers and Eco‑TextilesCollege of Materials Science and EngineeringQingdao UniversityQingdao 266071People’s Republic of China Shaanxi Key Laboratory of Macromolecular Science and Technology School of Chemistry and Chemical EngineeringNorthwestern Polytechnical UniversityXi’anShaanxi 710072People’s Republic of China

Currently,the demand for electromagnetic wave(EMW)absorbing materials with specific functions and capable of withstanding harsh environments is becoming increasingly ***-component interface engineering is considered an effective means to achieve high-efficiency EMW ***,interface modulation engineering has not been fully discussed and has great potential in the field of EMW *** this study,multi-component tin compound fiber composites based on carbon fiber(CF)substrate were prepared by electrospinning,hydrothermal synthesis,and high-temperature thermal *** utilizing the different properties of different substances,rich heterogeneous interfaces are *** effectively promotes charge transfer and enhances interfacial polarization and conduction *** prepared SnS/SnS_(2)/SnO_(2)/CF composites with abundant heterogeneous interfaces have and exhibit excellent EMW absorption properties at a loading of 50 wt%in epoxy *** minimum reflection loss(rL)is−46.74 dB and the maximum effective absorption bandwidth is 5.28 ***,SnS/SnS_(2)/SnO_(2)/CF epoxy composite coatings exhibited long-term corrosion resistance on q235 steel ***,this study provides an effective strategy for the design of high-efficiency EMW absorbing materials in complex and harsh environments.

关键词： Electrostatic spinning Component regulation Heterogeneous interfaces Electromagnetic wave absorption Corrosion protection

Viscosity and structure relationship with equimolar substitution of CaO with MgO in the CaO–MgO–Al_(2)O_(3)–SiO_(2)slag melts

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International Journal of Minerals,Metallurgy and Materials 2025年第1期32卷 70-79页

作者： Yong Hou Shuo Zhang Jie Dang Jia guo Hanghang Zhou Xuewei Lü College of Materials Science and Engineering Chongqing UniversityChongqing 400044China Chongqing Key Laboratory of Vanadium-Titanium Metallurgy and New Materials Chongqing UniversityChongqing 400044China

Currently,the Al_(2)O_(3)content in the high-alumina slag systems within blast furnaces is generally limited to 16wt%–18.5wt%,making it challenging to overcome this *** most studies that concentrated on managing the MgO/Al_(2)O_(3)ratio or basicity,this paper explored the effect of equimolar substitution of MgO for CaO on the viscosity and structure of a high-alumina CaO-MgO-Al_(2)O_(3)-SiO_(2)slag system,providing theoretical guidance and data to facilitate the application of high-alumina *** results revealed that the viscosity first decreased and then increased with higher MgO substitution,reaching a minimum at 15mol%MgO *** transform infrared spectroscopy(FTIr)results found that the depths of the troughs representing[SiO_(4)]tetrahedra,[AlO_(4)]tetrahedra,and Si-O-Al bending became progressively deeper with increased MgO *** of the raman spectra showed that the average number of bridging oxygens per Si atom and the X_(q^(3))/X_(q^(2))(X_(q^(i))is the molar fraction of q^(i) unit,and i is the number of bridging oxygens in a[SiO_(4)]tetrahedral unit)ratio increased from 2.30 and 1.02 to 2.52 and 2.14,respectively,indicating a progressive polymerization of the silicate structure.X-ray photoelectron spectroscopy(XPS)results highlighted that non-bridging oxygen content decreased from 77.97mol% to 63.41mol% with increasing MgO concentration,whereas bridging oxygen and free oxygen contents *** analysis demonstrated a gradual increase in the polymerization degree of the tetrahedral structure with the increase in MgO ***,bond strength is another important factor affecting the slag *** occurrence of a viscosity minimum can be attributed to the complex evolution of bond strengths of non-bridging oxygens generated during depolymerization of the[SiO_(4)]and[AlO_(4)]tetrahedral structures by CaO and MgO.

关键词： aluminosilicate viscosity structure spectroscopy

Novel transcatheter aortic heart valves exhibiting excellent hemodynamic performance and low-fouling property

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Journal of Materials Science & Technology 2019年第1期35卷 207-215页

作者： F.guo K.Jiao Y.Bai J.guo q.Chen r.Yang X.Zhang Shenyang National Laboratory for Materials Science Institute of Metal Research Chinese Academy of Sciences School of Materials Science and Engineering University of Science and Technology of China School of Textile and Material Engineering Dalian Polytechnic University Lumenous Peiertech

Transcatheter aortic heart valves(TAHVs) have been widely used for aortic valve replacements, with less trauma and lower clinical risk compared with traditional surgical heart valve replacements. In the present study, composites of poly(ethylene glycol) diacrylate(PEGDA) hydrogels and anisotropic highshrinkage polyethylene terephthalate/polyamide6(PET-PA6) fabric(PEGDA/PET-PA6) were fabricated as artificial heart valve leaflets. Dynamic mechanical analyses(DMA) indicated that PEGDA/PET-PA6 composites possessed anisotropic mechanical properties(i.e., storage moduli ~23.30 ± 1.36 MPa parallel to the aligned fabric fibers and ~9.68 ± 0.90 MPa perpendicular to the aligned fibers at 1 Hz) that were comparable to aortic valve leaflets. The PEGDA/PET-PA6 composites with smooth surfaces were highly hydrophilic(contact angle ~41.6°± 3.8°) and had low-fouling properties without platelet adhesion,suggesting a low risk of thrombogenicity when they interacted with blood. Furthermore, transcatheter aortic heart valves were fabricated using nitinol self-expanding frames and PEGDA/PET-PA6 composites as artificial leaflets, which presented excellent hemodynamic performance with a large orifice area(1.75cm2) and low regurgitation(3.41%), thus meeting the requirements of ISO 5840-3 standard. Therefore,PEGDA/PET-PA6 composites had suitable mechanical properties, good biocompatibility, and low-fouling properties, indicating that they might be used for TAHVs in the future.

关键词： Transcatheter aortic heart valve Textile fabric Poly(ethylene glycol)diacrylate Anti-fouling

A Geometric Distortion Solution Specifically for Historical Observations and its Implementation

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research in Astronomy and Astrophysics 2024年第11期24卷 85-94页

作者： F.r.Lin q.Y.Peng Z.J.Zheng B.F.guo School of Software Jiangxi Normal UniversityNanchang 330022China Sino-French Joint Laboratory for Astrometry Dynamics and Space ScienceJinan UniversityGuangzhou 510632China Department of Computer Science Jinan UniversityGuangzhou 510632China Guangdong Ocean University Zhanjiang 524000China

Geometric distortion(GD)critically constrains the precision of *** well-established methods to correct GD requires calibration observations,which can only be obtained using a special dithering strategy during the observation ***,this special observation mode is not often used,especially for historical observations before those GD correction methods were *** a result,some telescopes have no GD calibration observations for a long period,making it impossible to accurately determine the GD *** limits the value of the telescope observations in certain astrometric scenarios,such as using historical observations of moving targets in the solar system to improve their *** investigated a method for handling GD that does not rely on the calibration *** this advantage,it can be used to solve the GD models of telescopes which were intractable in the *** method was implemented in Python and released on *** was then applied to solve GD in the observations taken with the 1 m and 2.4 m telescopes at Yunnan *** resulting GD models were compared with those obtained using well-established methods to demonstrate the ***,the method was applied in the reduction of observations for two targets,the moon of Jupiter(Himalia)and binary GSC 2038-0293,to show its *** GD correction,the astrometric results for both targets show ***,the mean residual between the observed and computed position(O-C)for binary GSC 2038-0293 decreased from 36 to 5 mas.

关键词： astrometry-methods data analysis-techniques image processing

Experimental methods for determination of mechanical behaviors of materials at high temperatures via the split Hopkinson bars

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Acta Mechanica Sinica 2020年第6期36卷 1275-1293,I0003页

作者： q.B.Dou K.r.Wu T.Suo C.Zhang X.guo Y.Z.guo W.G.guo Y.L.Li School of Aeronautics Northwestern Polytechnical UniversityXi’an710072China Joint International research Laboratory of Impact Dynamics and its Engineering Application Xi’an710072China Shaanxi Key Laboratory of Impact Dynamics and its Engineering Application Xi’an710072China State Key Laboratory for Strength and Vibration of Mechanical Structures School of AerospaceXi’an Jiaotong UniversityXi’an710049China

Full understanding of the thermomechanical behaviors of materials at high strain rates and high temperatures are of great importance from not only scientific meaning but also practical value in engineering structure design and safety *** efforts have been made for abilities of operation the split Hopkinson bars,the most popular technique for experimental determination of mechanical behaviors of materials over the strain rates from 10^2 to 10^4 s^−1 over the past 70 years,at high temperatures since 1960s.A review of experiment work is presented in this paper to give an overview of the development of experimental techniques at high temperatures based on Hopkinson bar *** principles of the split Hopkinson bar requires the loading bars avoiding temperature gradient or keeping relatively low temperature when performing high temperature *** such as performing temperature gradient corrections,rapid heating or using special designed automatically assembled systems were proposed by researchers to enable the operation of the split Hopkinson bars at temperature as high as ***,to the application of high speed photographic technique for capturing the dynamic deformation process of the specimen in high temperature Hopkinson bar testing,some key issues of eliminating the strong thermal radiation induced lights oversaturation and de-blurring of images due to insufficient exposure at high temperature and high strain rate condition,as well as fabrication of high contrast speckle pattern for high temperature digital image correlation measurement were also *** technique can now enable the split Hopkinson bar testing to be performed at high temperature up to 1873 K under the loading conditions of compression or tension with the in situ observation and full field measurement of deformation as *** paper concludes with summaries of the most important achievements and highlighting of the prospects,trends and remaining challenge

关键词： Mechanical behaviors Split Hopkinson bar High strain rate High temperature

Fluid-structure interaction in Z-shaped pipe with different supports

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Acta Mechanica Sinica 2020年第2期36卷 513-523页

作者： q.guo J.X.Zhou X.L.Guan College of Water Conservancy and Hydropower Engineering Hohai UniversityNanjing 210098China Highway Science and Technology research Institute Xinjiang Production and Construction Corpsürümqi 830002China

Fluid-structure interaction(FSI)has a strong relation with layout of fluid delivery *** is liable to cause local ***,FSI analysis is necessary in many cases,especially for flexible pipe *** modeling consists of eight governing equations and then completely solved via the finite volume method(FVM).Friction,Poisson and joint couplings were discussed in detail to reveal the influence of a Z-shaped pipe with different supports and elbows on *** the feasibility of solving FSI by FVM was verified,the different effects of free,fixed and elastic supports on FSI in the commonly used and simplified Z-shaped pipe were further *** indicated that different support stiffness lead to various FSI *** coupling occurs at the elbow and less support is considered,then the pipe has a relatively large amplitude and complex pressure fluctuation.

关键词： Fluid-structure interaction Finite volume method Z-shaped pipe Support stiffness

HIGH－PErFOrMANCE　CAPILLArY　ELECTrOPHOrESIS　OF　rEDUCING　OLIGOSACCHArIDES　AS　THEIr　ETHYL　P－AMINOBENZOATE　DErIVATIVES

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Chinese Chemical Letters 1996年第2期7卷 159-160页

作者： Chang, LW guo, q Yu, ZL Chen, Y Zhu, A ACAD SINICA INST CHEMBEIJING 100080PEOPLES R CHINA

A modified method for the separation of oligosaccharides derivatized with p-aminoben-zoate ethyl ester by high performance capillary electrophoresis (HPCE) is described. The isomers of larger oligosaccharides up to 10... 详细信息

关键词： AS OLIGOSACCHArIDES THEIr ETHYL CAPILLArY AMINOBENZOATE

Twisted fiber microfluidics:a cutting-edge approach to 3D spiral devices

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Microsystems & Nanoengineering 2024年第1期10卷 193-202页

作者： Shunsuke Kato Daniel W.Carlson Amy q.Shen Yuanyuan guo Department of Electrical Information and Physics EngineeringSchool of EngineeringTohoku UniversityAoba-kuSendai 980-8579 MiyagiJapan Micro/Bio/Nanofluidics Unit Okinawa Institute of Science and TechnologyOnnaKunigami-gun 904-0495 OkinawaJapan Frontier research Institute for Interdisciplinary Sciences(FrIS) Tohoku UniversityAoba-kuSendai 980-0845 MiyagiJapan Graduate School of Biomedical Engineering Tohoku UniversityAoba-kuSendai 980-8579 MiyagiJapan Department of Physiology Graduate School of MedicineTohoku UniversityAoba-kuSendai 980-8575 MiyagiJapan

The development of 3D spiral microfluidics has opened new avenues for leveraging inertial focusing to analyze small fluid volumes,thereby advancing research across chemical,physical,and biological *** traditional straight microchannels rely solely on inertial lift forces,the novel spiral geometry generates Dean drag forces,eliminating the necessity for external fields in fluid ***,fabricating 3D spiral microfluidics remains a labor-intensive and costly endeavor,hindering its widespread ***,conventional lithographic methods primarily yield 2D planar devices,thereby limiting the selection of materials and geometrical *** address these challenges,this work introduces a streamlined fabrication method for 3D spiral microfluidic devices,employing rotational force within a miniaturized thermal drawing process,termed as *** innovation allows for rapid prototyping of twisted fiber-based microfluidics featuring versatility in material selection and heightened geometric *** validate the performance of these devices,we combined computational modeling with microtomographic particle image velocimetry(uTPiM)to comprehensively characterize the 3D flow *** results corroborate the presence of a steady secondary flow,underscoring the effectiveness of our *** 3D spiral microfluidics platform paves the way for exploring intricate microflow dynamics,with promising applications in areas such as drug delivery,diagnostics,and lab-on-a-chip systems.

关键词： thereby straight twisted

On the mechanism of Si-promoted destabilization of TiC_(x)particles in Al alloys

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Journal of Materials Science & Technology 2023年第34期165卷 17-26页

作者： H.Dong Y.C.guo Y.Z.Chen F.Xia q.q.guo q.Chen G.L.Li J.Y.Zhao Y.Zhong J.P.Li School of Materials and Chemical Engineering Xi’an Technological UniversityXi’an 710021China State Key Lab.of Solidification Processing Northwestern Polytechnical UniversityXi’an 710072China School of Science Xi’an University of Science and TechnologyXi’an 710054China

TiC_(x)is an excellent composite strengthening particle and grain refiner for Al ***,the stability of TiC_(x)is poor when solute Si exists in Al alloy melts,which significantly depresses its strengthening and grain refining *** this work,the destabilization mechanisms of the TiC_(x)particles in Al-Si alloy melt with a composition of Al-7Si-7.5TiC were explored via experiments,first-principles calculations and thermodynamic *** experimental results show that Si atoms diffuse into TiC_(x)and Ti atoms are released into the Al melt to form a Ti-rich transition zone during the insulation of TiC_(x)in Al-Si melt,and the TiAlySiz and Al_(4)C_(3)phases are solidified in the Ti-rich zone and at Ti-rich zone/TiC_(x)interface,*** first principles calculations show that the low formation energy of C vacancies facilitates the rapid diffusion of Si atoms in TiC_(x),while the doping of Si atoms reduces the energy barrier of diffusion of Ti atoms in TiC_(x)and promotes the formation of Ti-rich *** thermodynamic calculations show that the wide crystallization temperature range of the destabilized product TiAlySiz phase is the key to continuous decomposition of TiC_(x)*** addition,the driving force of the main destabilization reaction of TiC_(x)in the Al-Si alloys is about 44 times higher than that in the Al alloys without Si *** indicates that the presence of solute Si remarkably promotes the subsequent decomposition process of TiC_(x)in the Al-Si alloy melts.

关键词： Al-Si alloy TiC_(x)particles Destabilization First principles calculations Thermodynamics