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rapid prototyping of a polymer MEMS dropletdispenser by laser-assisted 3D printing

microsystems & Nanoengineering 2023年第4期9卷 211-221页

作者： rémi courson Oleksii Bratash Ali Maziz CloéDesmet ricardo Alvarado Meza Loïc Leroy Elodie Engel Arnaud Buhot Laurent Malaquin Thierry Leïchlé LAAS-CNrS Universitéde ToulouseCNRS31400 ToulouseFrance UniversitéGrenoble Alpes CNRSCEAIRIGSyMMES38000 GrenobleFrance Georgia Tech−CNrS International research Laboratory AtlantaGA 30332USA

In this work, we introduce a polymer version of a previously developed silicon MEMS drop deposition tool for surfacefunctionalization that consists of a microcantilever integrating an open fluidic channel and a reservoir. The device isfabricated by laser stereolithography, which offers the advantages of low-cost and fast prototyping. Additionally,thanks to the ability to process multiple materials, a magnetic base is incorporated into the cantilever for convenienthandling and attachment to the holder of a robotized stage used for spotting. Droplets with diameters ranging from∼50 μm to ∼300 μm are printed upon direct contact of the cantilever tip with the surface to pattern. Liquid loading isachieved by fully immersing the cantilever into a reservoir drop, where a single load results in the deposition of morethan 200 droplets. The influences of the size and shape of the cantilever tip and the reservoir on the printing outcomeare studied. As a proof-of-concept of the biofunctionalization capability of this 3D printed droplet dispenser,microarrays of oligonucleotides and antibodies displaying high specificity and no cross-contamination are fabricated,and droplets are deposited at the tip of an optical fiber bundle.

关键词： cantilever reservoir printing

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Sliding walls: a new paradigm for fluidic actuation and protocol implementation in microfluidics

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microsystems & Nanoengineering 2020年第1期6卷 1093-1102页

作者： Bastien Venzac Yang Liu Ivan Ferrante Pablo Vargas Ayako Yamada remi courson Marine Verhulsel Laurent Malaquin Jean-Louis Viovy Stephanie Descroix Laboratoire Physico Chimie Curie Institut CuriePSL Research UniversityCNRS UMR16875005 ParisFrance Sorbonne Universites UPMC Univ Paris 0675005 ParisFrance Institut Pierre-Gilles de Gennes PSL Research University75005 ParisFrance Institut Curie PSL Research UniversityCNRS UMR 14475005 ParisFrance LAAS-CNrS Universitéde ToulouseCNRS31400 ToulouseFrance

Currently,fluidic control in microdevices is mainly achieved either by external pumps and valves,which are expensive and bulky,or by valves integrated in the *** types of internal valves or actuation methods have been proposed,but they generally impose difficult compromises between performance and fabrication *** propose here a new paradigm for actuation in microfluidic devices based on rigid or semi-rigid walls with transversal dimensions of hundreds of micrometres that are able to slide within a microfluidic chip and to intersect microchannels with hand-driven or translation stage-based *** this new concept for reconfigurable microfluidics,the implementation of a wide range of functionalities was facilitated and allowed for no or limited dead volume,low cost and low *** demonstrate here several fluidic operations,including on/off or switch valving,where channels are blocked or reconfigured depending on the sliding wall *** valves sustain pressures up to *** and reversible compartmentalisation of large microfluidic chambers were also *** last possibility was applied to a“4D”migration assay of dendritic cells in a collagen ***,sliding walls containing a hydrogel-based membrane were developed and used to concentrate,purify and transport biomolecules from one channel to another,such functionality involving complex fluidic transport patterns not possible in earlier microfluidic ***,this toolbox is compatible with“soft lithography”technology,allowing easy implementation within usual fabrication workflows for polydimethylsiloxane *** new technology opens the route to a variety of microfluidic applications,with a focus on simple,hand-driven devices for point-of-care or biological laboratories with low or limited equipment and resources.

关键词： walls hundreds operations

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Fe-doped olivine and char for in-bed elimination of gasification tars in an air-blown fluidised bed reactor coupled with oxidative hot gas filtration

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Carbon resources Conversion 2022年第4期5卷 271-288页

作者： miguel ruiz Adam Schnitzer Claire courson Guillain Mauviel LrGP CNRSUniversity of LorraineENSIC1 Rue GrandvilleNancyFrance University of Lorraine LERMaBENSTIB27 Rue Philippe S´eguinPO Box 1041F-88051 EpinalFrance Institut of Chemistry and Processes for Energy Environment and HealthICPEES–UMR 7515University of Strasbourg25 Rue Becquerel67087 StrasbourgFrance

Gasification experiments were carried out in a pilot scale fluid bed reactor operated under allothermal mode and low fluidisation regime with iron-doped olivine and char as catalyst for in-situ tar *** catalyst combination resulted in a reduction of 50%in the overall tar yield with respect to the reference ***,the integration of an oxidative Hot Gas Filtration unit downstream the gasification reactor led to a further reduction in overall tar yield and relatively clean gas was obtained(approx.1 g/Nm3,benzene-free).The tar dew point of the resulting producer gas was estimated to 80℃,only 40℃ above the threshold value recommended for its valorisation in standard internal combustion ***,catalyst elutriation and char hold-up took place to a large extent inside the *** analysis of catalyst samples at different Time-On-Stream(TOS)revealed:(i)a considerable loss of iron oxides during the first hour of test because of the interparticle mechanical attrition(mostly surface abrasion)and partial reduction of hematite to magnetite and wustite but,stable composition at higher TOS,(ii)the loss of the iron oxide coverage of Fe/olivine particles and the formation of agglomerates with increasing TOS and,(iii)the amount of carbon deposited in the surface of the Fe/olivine particles increased with TOS,but in any case,these carbon deposits can be completely oxidized above 650℃.

关键词： Gasification Tar Oxidative hot gas filtration Char Iron-doped olivine

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Catalytic steam methane reforming enhanced by CO_2 capture on CaO based bi-functional compounds

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Journal of Energy Chemistry 2017年第5期26卷 1014-1025页

作者： Francesca micheli Manuela Sciarra Claire courson Katia Gallucci Institut de Chimie et Procédés pour l'énergie l'Environnement et la Santé UMR CNRS 7515 ECPM University of Strasbourg Department of Industrial Engineering University of L'Aquila

Sorption enhanced steam methane reforming（SE-SMr） was performed to maximize hydrogen production and contemporary remove COfrom the product stream using bi-functional sorbent-catalyst *** were tested at two different scales: micro and laboratory. The CaO amount varied in the CaO-CaAlOsorbent system synthesized by wet mixing(CaO content of 100 wt%, 56 wt%, 30 wt%, or 0 wt% and balance of CaAlO) which were upgraded to bi-functional compounds by impregnation of 3 wt% of Ni. Nitrogen adsorption（BET/BJH）, X-ray Diffraction（XrD）, Temperature-Programmed reduction（TPr） and Scanning and Transmission Electronic microscopy（SEM and TEM, respectively） analyses were performed to characterize structural and textural properties and reducibility of the bi-functional materials and evaluate their catalytic behavior. A fixed sorbent composition CaO-CaAlO(56 wt% of CaO and CaAlObalance), was chosen to study the effect of different weight hourly space times（WHST） and CHstream compositions in SE-SMr activity. Impregnated mayenite at both micro and laboratory scales showed stable Hcontent of almost 74%, with CHconversion of 72% similarly to the values reported by the sample containing 30 wt% of CaO in the *** with 30 wt% of CaO showed promisingly behavior, enhancing Hcontent up to almost 94.5%.When the sorption enhanced reaction is performed roughly 89% of CHconversion is achieved, and after the pre-breakthrough, the catalyst worked at the thermodynamic level. During cycling sorption/regeneration experiments, even if COremoval efficiency slightly decreases, CHconversion and Hyield remain stable.

关键词： Sorption enhanced steam methane reforming By-functional sorbent-catalyst compounds Calcium oxide Nickel catalyst Mayenite

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