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Portable fluorogenic probe for monitoring of volatile amine vapour and food spoilage

Chinese Chemical Letters 2024年第3期35卷 257-261页

作者： Jian-Hao Zhao Wen-Xing Xu Bin Li Wei Xu Wu-Kun Zhang Ming-Shuai Yuan Hui-Zi Li qing-guo he Xiang Ma Jian-Gong Cheng Yan-Yan Fu State Key Lab of Transducer Technology Shanghai Institute of Microsystem and Information TechnologyChinese Academy of SciencesShanghai 200050China Center of Materials Science and Optoelectronics Engineering University of the Chinese Academy of SciencesBeijing 100039China School of Physical Science and Technology ShanghaiTech UniversityShanghai 201210China Key Laboratory for Advanced Materials and Feringa Nobel Prize Scientist Joint Research Center Frontiers Science Center for Materiobiology and Dynamic Chemistry School of Chemistry and Molecular EngineeringEast China University of Science and TechnologyShanghai 200237China

There are urgent needs of volatile amine gas sensors with high-performance in food quality control,disease monitoring and environmental ***-film fluorescent probe is suitable for amine vapour sensing due to its high sensitivity,high selectivity,and no polluting ***,a novel fluorescent probe based on indacenodithiophene structure withπconjugated system was designed and *** experimental results show that the films prepared by this material exhibit rapid and distinct fluorescence quenching after being exposed to saturated vapours of primary amine,secondary amine and tertiary amine represented by n-propylamine,diethylamine and trimethylamine,*** quenching of fluorescence is 84%,87%and 96%,respectively,within 10 *** detection mechanism of probe for primary amine is based on specific chemical reaction,while the detection mechanism for secondary amine and tertiary amine is intramolecular charge *** experiments show that the detection limit of the fluorescent probe for trimethylamine,an important marker of food spoilage,could reach 4.610 ***-site detection based on spoilage of small yellow croaker suggests the material possesses the potential for food freshness *** simple fluorogenic probe is an original approach to simplify real-time visual monitoring of volatile amine vapour.

关键词： Fluorescent probe Volatile amine Gas sensing Trimethylamine Food spoilage

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基于TC-CCES的冷热电联供系统热力性能分析

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热能动力工程 2024年第2期39卷 74-81页

作者：郭庆贺谢尉扬傅洪军肖刚浙江省清洁能源与碳中和重点实验室浙江杭州310027 浙江浙能电力股份有限公司浙江杭州310007 温州燃机发电有限公司浙江温州325013

为了更好地理解CO_(2)作为储能工质在热力学方面的特性,基于跨临界压缩二氧化碳储能系统(TC-CCES),结合CO_(2)易液化的特性,采用Aspen Plus软件构建了冷热电联产(CCHP)系统热力学模型,分析了回热器热水流量、低压节流阀压降及第一级压... 详细信息

为了更好地理解CO_(2)作为储能工质在热力学方面的特性,基于跨临界压缩二氧化碳储能系统(TC-CCES),结合CO_(2)易液化的特性,采用Aspen Plus软件构建了冷热电联产(CCHP)系统热力学模型,分析了回热器热水流量、低压节流阀压降及第一级压缩机出口压力对CCES-CCHP系统性能的影响。结果表明:在基础运行工况下,CCES-CCHP系统电效率为41%,能量效率为1.16;当回热器热水流量、第一级压缩机出口压力变化时,系统电效率与能量效率变化趋势相反;当低压节流阀压降增大时,系统电效率和能量效率均呈下降趋势;CCES-CCHP系统与TC-CCES系统相比,能量利用效率提升19.50%。

关键词：跨临界压缩二氧化碳储能超临界冷热电联供数值模拟

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基于模型预测控制的重型自卸车差动制动防侧翻控制研究

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制造业自动化 2024年第1期46卷 7-16,26页

作者：付众铖郭庆贺胡明茂郭栋廖子文湖北汽车工业学院机械工程学院十堰442002 重庆理工大学车辆工程学院重庆400000 东风商用车有限公司十堰442002

为有效解决重型自卸车在极限工况下易侧翻失稳的问题,提出了一种基于模型预测控制的差动制动防侧翻控制方法。建立了重型自卸车九自由度车辆动力学模型,以零力矩点侧倾评价指标作为自卸车的侧翻评价指标,通过差动制动控制的方法为四个... 详细信息

为有效解决重型自卸车在极限工况下易侧翻失稳的问题,提出了一种基于模型预测控制的差动制动防侧翻控制方法。建立了重型自卸车九自由度车辆动力学模型,以零力矩点侧倾评价指标作为自卸车的侧翻评价指标,通过差动制动控制的方法为四个车轮提供制动力矩,以提高自卸车的行驶稳定性。为验证所提出的防侧翻控制方法的有效性,在鱼钩工况和阶跃工况下,以传统PID差动制动控制和无控制为对比,进行了MATLAB/Simulink与Trucksim的联合仿真,仿真结果显示,相比PID差动制动控制,所提出的基于模型预测控制的差动制动控制方法具有更好的抗侧翻能力,且稳定性较好。

关键词：重型自卸车模型预测控制差动制动零力矩点防侧翻

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Microstructural evolution,mechanical properties and degradation mechanism of PS-PVD quasi-columnar thermal barrier coatings exposed to glassy CMAS deposits

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Rare Metals 2024年第7期43卷 3329-3340页

作者： Zi-Yue Yu Liang-Liang Wei Xing-Ye guo Bao-Peng Zhang qing he Hong-Bo guo School of Materials Science and Engineering Beihang UniversityBeijing100191China Key Laboratory of High-Temperature Structure Materials and Protective Coatings(Ministry of Industry and Information Technology) Beihang UniversityBeijing 100191China Surface Engineering Research Institute Chinese Academy of Agricultural Mechanization SciencesBeijing 100083China

Thermal barrier coatings(TBCs) applied in aeroengines tend to be attacked by molten calcia-magnesiaalumino-silicate(CMAS) at high operating ***-stabilized zirconia(YSZ) coatings with quasicolumnar microstructure were fabricated by plasma spray physical vapor deposition(PS-PVD) *** chemic al changes,micros tructural transform ation,mechanical properties and degradation mechanisms of the CM AS-interacted TBCs in the thermal cycling tests were *** YSZ grains were dissolved in the CMAS melts,and then the ZrO_(2) grains were reprecipitated with spherical shape,accompanying with phase transformation from tetragonal(t) to monoclinic(m).The thermal cycling tests reveal that the YSZ coating fails at the early stage due to the attack of *** fractures in intracolumns lead to partial spallation of the *** failure of the coating occurs at the interfaces between thermally grown oxides(TGO) layer and YSZ topcoat;especially,the hardness and Young's modulus of the YSZ coatings increase intensively,as the coatings were infiltrated by the CMAS for a long time.

关键词： CMAS Thermal barrier coatings Young's modulus Thermal cycling behavior PS-PVD

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Warming intensified the effects of nitrogen addition on N_(2)O emissions from alpine meadow in the northern qinghai-Tibet Plateau

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Advances in Climate Change Research 2024年第1期15卷 101-112页

作者： Ming-Jie LI Yi-qing GE Hasbagan GANJURJAV guo-Zheng HU Hong-Bao WU Jun YAN Shi-Cheng he qing-Zhu GAO Institute of Environment and Sustainable Development in Agriculture Chinese Academy of Agricultural SciencesBeijing 100081China National Agricultural Experimental Station for Agricultural Environment Nagqu 852100China Ecology and Nature Conservation Institute Chinese Academy of ForestryBeijing 100091China College of Resource and Environment Anhui Science and Technology UniversityFengyang 233100China Nagqu Agriculture Animal Husbandryand Prataculture Science and Technology Research and Extension CenterNagqu 852100China Tongliao Experimental Middle School Tongliao 028000China

Warming and nitrogen(N)addition may impact soil nitrous oxide(N_(2)O)emissions,but the relationship between plant community composition and soil microbial activities remains *** a two-year field study in the qinghai-Tibet Plateau,open-top chambers were used to quantify the effects of warming,N-addition,and their interactions on N_(2)O *** found that the N-addition greatly increased N_(2)O emissions by 77.4%in 2018 when compared to the control *** contrast,warming showed little effect on N_(2)0 emissions but did increase the activity of enzymes associated with soil nitrification and denitrification.A combined effect of warming and N-addition of resulted in 208.6%(2018)and 90.8%(2019)increase in N_(2)0 emissions,respectively,compared to the individual treatments of warming or *** warming in alpine meadows is causally linked to increased legume biomass which is further intensified with the *** legume biomass(phed microbial carbon/nitrogen(MBC/MBN)(phe addition of warming further intensifies this *** increased dominance of legumes and microbial N content contributes to this *** outcomes suggest that warming and atmospheric N deposition can stimulate N_(2)O emissions of alpine meadows inthefuture.

关键词： Alpine meadow Community composition Nitrogen addition Nitrous oxide flux qinghai-Tibet Plateau Warming

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Dynamically switchable porphyrin-based molecular tweezer for on-off fullerene recognition

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Chinese Chemical Letters 2024年第6期35卷 283-287页

作者： Zhimin Sun Xin-Hui guo Yue Zhao qing-Yu Meng Li-Juan Xing he-Lue Sun College of Chemistry and Materials Science Hebei Key Laboratory of Organic Functional MoleculesHebei Normal UniversityShijiazhuang 050024China

herein,a novel molecular tweezer based on 2,2'-bipyridine-bridged porphyrin subunits was constructed for efficient fullerenes *** syn conformation of the molecule,which was obtained by Zn(Ⅱ)coordination,gives rise to a proper cavity to interact with fullerene guests to form a stable 1:1 complex in toluene *** exhibits distinct binding selectivity towards C_(60)over C_(70).Moreover,the fullerene recognition capacity can be adequately suppressed by importing H_(2)PO_(4)^(-)to competitively capture Zn(Ⅱ)along with syn-anti conformational ***,the molecular tweezer regenerated to bind the fullerene by introducing the Ca^(2+)into the ***,the association-disassociation process can be switched reversibly and repeatedly.

关键词： Molecular tweezer Fullerene recognition Supramolecular chemistry Conformation conversion Coordination

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Escape probability for isotropic emitters near Kerr black hole with astrometric

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Communications in Theoretical Physics 2024年第5期76卷 128-133页

作者： Yu-Xuan Han qing-Hua Zhu qing-guo Huang CAS Key Laboratory of Theoretical Physics Institute of Theoretical PhysicsChinese Academy of SciencesBeijing 100190China School of Physical Sciences University of Chinese Academy of SciencesNo.19A Yuquan RoadBeijing 100049China Department of Physics Chongqing UniversityChongqing 401331China School of Fundamental Physics and Mathematical Sciences Hangzhou Institute for Advanced Study UCASHangzhou 310024China

The paper investigates the escape probability for isotropic emitters near a Kerr black *** propose a new approach to obtain the escape probability in a general manner,going beyond previous case-by-case *** approach is based on studies of the black hole shadow with astrometric observable and can be applied to emitters with an arbitrary 4-velocities and locations,even to the emitters outside of the equatorial *** also consider representative examples illustrating how escape probabilities vary with distance,velocity,and inclination ***,this new approach provides an effective method for studying escape probabilities near Kerr black holes.

关键词： Kerr black hole photon escape probability isotropic emitters

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Recent progresses in the development of tubular segmented-in-series solid oxide fuel cells:Experimental and numerical study

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International Journal of Minerals,Metallurgy and Materials 2024年第3期31卷 427-442页

作者： Shuo Han Tao Wei Sijia Wang Yanlong Zhu Xingtong guo Liang he Xiongzhuang Li qing Huang Daifen Chen School of Energy and Power Jiangsu University of Science and TechnologyZhenjiang 212003China College of Materials Science and Engineering Nanjing Forestry UniversityNanjing 210037China

Solid oxide fuel cells(SOFCs)have attracted a great deal of interest because they have the highest efficiency without using any noble metal as catalysts among all the fuel cell ***,traditional SOFCs suffer from having a higher volume,current leakage,complex connections,and difficulty in gas *** solve these problems,Rolls-Royce has fabricated a simple design by stacking cells in series on an insulating porous support,resulting in the tubular segmented-in-series solid oxide fuel cells(SIS-SOFCs),which achieved higher output *** work systematically reviews recent advances in the structures,preparation methods,perform-ances,and stability of tubular SIS-SOFCs in experimental and numerical ***,the challenges and future development of tubular SIS-SOFCs are also *** findings of this work can help guide the direction and inspire innovation of future development in this field.

关键词： solid oxide fuel cell segmented-in-series tubular experimental study numerical study

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Prescribed Performance Tracking Control of Time-Delay Nonlinear Systems With Output Constraints

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IEEE/CAA Journal of Automatica Sinica 2024年第7期11卷 1557-1565页

作者： Jin-Xi Zhang Kai-Di Xu qing-guo Wang IEEE the State Key Laboratory of Synthetical Automation for Process Industries Northeastern UniversityShenyang 110819China Institute of Artificial Intelligence and Future Networks Beijing Normal UniversityZhuhai 519087 Guangdong Key Laboratory of Artificial Intelligence and Multi-Modal Data Processing Beijing Normal University-Hong Kong Baptist University United International CollegeZhuhai 519087

The problem of prescribed performance tracking control for unknown time-delay nonlinear systems subject to output constraints is dealt with in this paper. In contrast with related works, only the most fundamental requirements, i.e., boundedness and the local Lipschitz condition, are assumed for the allowable time delays. Moreover, we focus on the case where the reference is unknown beforehand, which renders the standard prescribed performance control designs under output constraints infeasible. To conquer these challenges, a novel robust prescribed performance control approach is put forward in this ***, a reverse tuning function is skillfully constructed and automatically generates a performance envelop for the tracking error. In addition, a unified performance analysis framework based on proof by contradiction and the barrier function is established to reveal the inherent robustness of the control system against the time delays. It turns out that the system output tracks the reference with a preassigned settling time and good accuracy,without constraint violations. A comparative simulation on a two-stage chemical reactor is carried out to illustrate the above theoretical findings.

关键词： Nonlinear systems output constraints prescribed performance reference tracking time delays

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Synthesis and properties of a star-shaped organic material with triphenylamine and N-vinyl carbazole units

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Chinese Chemical Letters 2007年第8期18卷 920-922页

作者： qing guo he Jian Gong Cheng Feng Lian Bai Shanghai Institute of Microsystem and Information Technology Chinese Academy of Sciences Shanghai 200050 China Key Laboratory of Organic Solids Centre for Molecular Science Institute of Chemistry Chinese Academy of Sciences Beijing 100080 China

A starburst tripbenylamine cored N-vinyl carbazole （V-Cz） branched compound was designed and synthesized via optimized heck reaction in a yield of 40-60%. Moderate yield came from decomposition of V-Cz and self-coupling of triiodo-triphenylamine. TCz-TPA adopts a highly twisted propeller conformation by molecular mechanical optimization. It is readily soluble for its highly twisted conformation. Transparent and pinhole free films could be easily fabricated by spin-coating for its starburst structure. It emits blue-greenish light in CH2Cl2 peaked at 460 nm with a narrow full-width at half-maximum （FWHM） of 65 nm. As compared,

关键词： Starburst Triphenylamine Carbazole heck reaction Photoluminescence

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