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Chinese Chemical Letters 2009年第10期20卷 1245-1247页

作者： Ling Ling Xi pei min zhang Yan Zhu Department of Chemistry Xixi Campus Zhejiang University Hangzhou 310028 China

A La^3＋-Cu/Pt modified electrode was fabricated by electrodepositing process in CuS04 solution by adding a small amount of lanthium compound, and it was employed for direct current （DC） amperometric detection of spectinomycin by anion-exchange chromatography. Without derivatization, this method can simultaneously determine the main component and impurities in spectinomycin pharmaceutical raw material. Ease of preparation, being applied in DC detection mode and good catalytic stability confirmed the interests of this modified electrode as amperometric sensor for the determination of spectinomycin.

关键词： Copper/platinum chemically modified electrode High performance anion-exchange chromatography Direct current amperometricdetection Spectinomycin

Indium-Mediated Addition of α-Bromoketone to Aldimines

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Chinese Chemical Letters 1997年第4期8卷 267-268页

作者： pei pei SUN and Yong min zhang(Department of Chemistry, Hangzhou University,Hangzhou, 310028) Department of Chemistry Hangzhou University Hangzhou 310028 China

The addition reaction of ω-bromoacetophenone to aldimines by indium metal in THF-H_2O gave β-aminoketones

关键词： Indium-Mediated Addition of Li Bromoketone to Aldimines

Design of efficient thermoelectric generators

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Science China Materials 2024年第1期67卷 377-378页

作者： min Liu Yanzhong pei Interdisciplinary Materials Research Center School of Materials Science and EngineeringTongji UniversityShanghai 201804China

Thermoelectricity,which enables direct conversion between heat and electricity,undergoes impressive developments in recent decades,and is particularly promising for recovering low-grade heat of<600 K[1,2].Currently,only Bi2Te3-based thermoelectric devices are commercialized[3].However,the scarcity of tellurium(Te)(Fig.1a)is the main *** leads to numerous recent efforts on the development of efficient nonBi2Te3 thermoelectrics as potential alternatives,and successful examples(Fig.1b)include Mg3Sb2-alloys[2,3]and MgAgSb[1,2].

关键词： enable efficient electricity

Determination of lisinopril using anion exchange chromatography with integrated pulsed amperometric detection

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Chinese Chemical Letters 2012年第3期23卷 335-338页

作者： Yu Xiu Liu Dan Shou Mei Lan Chen Zhi Dong Chen pei min zhang Yan Zhu School of Chemistry and Chemical Engineering Changzhou UniversityChangzhou 213164China Zhe Jiang Academy of Traditional Chinese Medicine Hangzhou 310007China College of Biology and Environment Engineering Zhejiang Shuren UniversityHangzhou 310015China Department of Chemistry Xixi CampusZhejiang UniversityHangzhou 310028China

A rapid and practical method for direct detection of lisinopril in anion exchange chromatography（AEC） has been developed with integrated pulsed amperometric detection（IPAD）.Dionex AS 18（250 mm×2 mm） and AG 18（50 mm×2 mm） columns and 40 mmol/L NaOH solution were used for ***-step potential waveform parameters were optimized to maximize the signal-to-noise ratio（S/N）.Utilizing the optimized waveform,the repeatability（intra-day） precision and intermediate（inter-day） precision were obtained with relative standard deviation（RSD） of 0.74,0.93,*** limit of quantification（LOQ） and limit of detection（LOD） were found to be 0.37,0.12ng/mL,respectively,with the correlation coefficient of 0.9998 over concentration range 0.01-1μg/*** present method was successfully applied to the determination of lisinopril in human *** recoveries of plasma sample spiked by 0.2μg/mL,0.8μg/mL lisinopril were 98.31-103.23%with RSD of 1.41%, 0.61%,respectively.

关键词： Lisinopril Integrated pulsed amperometry Anion exchange chromatography Angiotensin converting enzyme inhibitor Plasma

Very Short-Term Forecasting of Distributed PV Power Using GSTANN

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CSEE Journal of Power and Energy Systems 2024年第4期10卷 1491-1501页

作者： Tiechui Yao Jue Wang Yangang Wang pei zhang Haizhou Cao Xuebin Chi min Shi Computer Network Information Center of the Chinese Academy of Sciences Beijing 100190China University of Chinese Academy of Sciences Beijing 100190China School of Electrical Engineering Beijing Jiaotong UniversityBeijing 100044China State Grid Hebei Electric Power Co. Ltd.Shijiazhuang 050000China

Photovoltaic(PV)power forecasting is essential for secure operation of a power *** prediction of PV power can improve new energy consumption capacity,help power system planning,promote development of smart grids,and ultimately support construction of smart energy ***,different from centralized PV power forecasts,three critical challenges are encountered in distributed PV power forecasting:1)lack of on-site meteorological observation,2)leveraging extraneous data to enhance forecasting performance,3)spatial-temporal modelling methods of meteorological information around the distributed PV *** address these issues,we propose a Graph Spatial-Temporal Attention Neural Network(GSTANN)to predict the very short-term power of distributed ***,we use satellite remote sensing data covering a specific geographical area to supplement meteorological information for all PV ***,we apply the graph convolution block to model the non-Euclidean local and global spatial dependence and design an attention mechanism to simultaneously derive temporal and spatial ***,we propose a data fusion module to solve the time misalignment between satellite remote sensing data and surrounding measured on-site data and design a power approximation block to map the conversion from solar irradiance to PV *** conducted with real-world case study datasets demonstrate that the prediction performance of GSTANN outperforms five state-of-the-art baselines.

关键词： Distributed photovoltaic power forecasting graph convolutional networks satellite images spatial-temporal attention

Two-layer autonomous intelligence dynamic trajectory planning method based on shield-tunnel ring-geology interactions

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Underground Space 2024年第6期19卷 227-250页

作者： min Hu Bingjian Wu Huiming Wu Liefeng pei SILC Business School Shanghai UniversityShanghai 201800China SHU-SUCG Research Centre for Building Industrialization Shanghai 201800China Shanghai Tunnel Engineering Co. Ltd.Shanghai 200032China

To solve the problem that current attitude planning methods do not fully consider the interaction and constraints among the shield,segmental tunnel ring,and geology,and cannot adapt to the changes in the actual engineering environment,or provide feasible long-term and short-term attitude planning,this paper proposes autonomous intelligent dynamic trajectory planning(AI-DTP)to provide tunnel ring and centimeter-layer planning targets for a self-driving shield to meet long-term accuracy and short-term ***-DTP introduces the Frenet coordinate system to solve the problem of inconsistent spatial representation of tunnel data,segmental tunnel ring location,and surrounding geological conditions,designs the long short-term memory attitude prediction model to accurately predict shield attitude change trend based on shield,tunnel,and geology,and uses a heuristic algorithm for trajectory ***-DTP provides ring-layer and centimeter-layer planning objectives that meet the needs of long-term accuracy and short-term correction of shield attitude *** the Hangzhou-Shaoxing Intercity Railroad Tunnel Project in China,the‘‘Zhiyu”shield equipped with the AI-DTP system was faster and more accurate than the manually controlled shield,with a smoother process and better quality of the completed tunnel.

关键词： Shield tunnel Trajectory planning Attitude control Self-driving Machine learning

Determination of anions in lithium-ion batteries electrolyte by ion chromatography

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Chinese Chemical Letters 2016年第6期27卷 864-866页

作者： Bin-He Zhu Cheng-Zhu Ni Na-Ni Wang Xun-Yan Zhao Wei-Qiang Guo pei-min zhang Jia-Jie zhang Su-Qing Chen Wei-De Lv Yan Zhu Department of Chemistry Xixi Campus Zhejiang University Hangzhou 310028 China Department of Medicine Zhejiang Academy of Traditional Chinese Medicine Hangzhou 310007 China School of Pharmaceutical and Chemical Engineering Taizhou University Taizhou 317000 China Hangzhou Vocational & Technical College Hangzhou 310018 China

A sensitive and accurate method based on ion chromatography was established for determination of five lithium salts in lithium-ion batteries electrolytes. Chromatographic analyses were carried out on an anion exchange column at flow rate of 1 m L/min. Under the optimal conditions, five target anions（BF4^-,PF6^-, TFSI^-, BOB^-and FSI^-） exhibited satisfactory linearity with a correlation coefficient of 0.9996. The relative standard derivations of the target anions were less than less than 0.94%（n = 7）. The limits of detections were in the range of 0.068–0.29 mg/L with average spiked recoveries ranging from 96.8% to 105.1%.

关键词： Ion chromatography Lithium salts Lithium-ion batteries electrolyte

The centrosymmetric to non-centrosymmetric transformation induced by alkaline-earth cations producing infrared nonlinear optical AeMn_(6)Ga_(6)S_(16)(Ae=Ca,Sr)

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Science China Chemistry 2024年第9期67卷 2941-2948页

作者： Yang-Ping zhang Shao-min pei Wen-Fa Chen Bin-Wen Liu Xiao-ming Jiang Guo-Cong Guo State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of MatterChinese Academy of SciencesFuzhou 350002China Fujian Science&Technology Innovation Laboratory for Optoelectronic Information of China Fuzhou 350108China School of Physical Science and Technology Shanghai Tech UniversityShanghai 201210China

Non-centrosymmetric(NCS)structure is an indispensable prerequisite for second-order nonlinear optical(NLO)***,the mainstream approach for designing new NCS structures still relies on chemical substitution,necessitating an urgent infusion of fresh *** this work,two isomorphic sulfides AeMn_(6)Ga_(6)S_(16)(Ae=Ca,1;Sr,2)are afforded by modifying the skeleton of centrosymmetric(CS)Mn_(2)Ga_(2)S_(5) via introducing strong electropositive alkaline-earth ***,the incorporation of Ca^(2+)/Sr^(2+)cations allows the elementary[MnGaS_(9)]_(∞)chains to reconfigure into bumpy[MnS_(6)]-[GaS_(4)]layers in a new engagement manner,thus enabling the conversion from CS to NCS *** modifications cause not only strong second-harmonic generation(SHG)responses(~1.5×benchmark AgGaS_(2)@1,700 nm),but also significantly feasible bandgaps(2.60-2.64 e V)compared to the sulfide Mn_(2)Ga_(2)S_(5)(1.36 e V),which ultimately facilitate ultrahigh laser-induced damage thresholds(4.4-6.6×AgGaS_(2)@1,064 nm for compounds 1 and 2).The present study offers an ingenious approach for the transformation of CS to NCS structure.

关键词： second-harmonic generation non-centrosymmetrical structure NLO functional motif solid-state method

Direct ink writing of multifunctional gratings with gel-like MXene/norepinephrine ink for dynamic electromagnetic interference shielding and patterned Joule heating

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Nano Research 2024年第3期17卷 1585-1594页

作者： pei-Zhu Jiang Zhiming Deng Peng min Lvxuan Ye Cheng-zhang Qi Hao-Yu Zhao Ji Liu Hao-Bin zhang Zhong-Zhen Yu Beijing Key Laboratory of Advanced Functional Polymer Composites Beijing University of Chemical TechnologyBeijing 100029China State Key Laboratory of Organic-Inorganic Composites College of Materials Science and EngineeringBeijing University of Chemical TechnologyBeijing 100029China School of Chemistry CRANN and AMBERTrinity College DublinDublin D02PN40Ireland

Intelligent electromagnetic interference(EMI)shielding modulators with a wide tuning range and cyclic stability are urgently needed but their fabrication remains challenging.A gel-like MXene/norepinephrine ink is developed and multifunctional MXene gratings with wide EMI shielding effectiveness(SE)tuning range,superior reversibility,and high mechanical flexibility are constructed by direct ink writing approach for dynamic EMI shielding and patterned Joule heating *** modulable MXene/norepinephrine grating with a high conductivity of 3510 S·cm-1 can conveniently realize the seamless modulation of the EMI SE by adjusting the angle between the MXene grating filaments and the electric field of the incident electromagnetic waves,offering highly reversible switching between shielding“On”(28.0 dB)and“Off”(0.5 dB)***,due to the optimized integration of the MXene ink and the rationally designed pattern,a superior specific EMI SE of 95,688.2 dB·cm^(2)·g^(-1) is achieved in the“On”***,the MXene/norepinephrine ink can be used to fabricate many complex patterned gratings with superior stability,instant responsibility,and superb mechanical flexibility,exhibiting a unique patterned Joule heating *** writing of multifunctional gratings paves a means for developing intelligent EMI shielding materials,wearable electronic devices,and advanced thermal management materials.

关键词： MXene ink direct ink writing electromagnetic interference shielding multifunctional gratings Joule heating

Flexible bidirectional self-powered photodetector with significantly reduced volume and accelerated response speed based on hydrogel and lift-off GaN-based nanowires

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Fundamental Research 2024年第2期4卷 369-378页

作者： min Jiang Yukun Zhao Penghui Zheng Jianya zhang Wenxian Yang min Zhou Yuanyuan Wu Renjun pei Shulong Lu Key Lab of Nanodevices and Applications Suzhou Institute of Nano-Tech and Nano-Bionics(SINANO)Chinese Academy of Sciences(CAS)Suzhou 215123China School of Nano-Tech and Nano-Bionics University of Science and Technology of ChinaHefei 230026China CAS Key Laboratory of Nano-Bio Interface Suzhou Institute of Nano-Tech and Nano-BionicsChinese Academy of SciencesSuzhou 215123China Nanchang Research Institute Suzhou Institute of Nano-Tech and Nano-BionicsChinese Academy of SciencesNanchang 330200China

Due to the wide range of potential applications for next-generation multi-functional devices,the flexible selfpowered photodetector(PD)with polarity-switchable behavior is essential but very challenging to be ***,a wearable bidirectional self-powered PD based on detached(Al,Ga)N and(In,Ga)N nanowires has been proposed and demonstrated *** from the photovoltage-competing dynamics across(Al,Ga)N and(In,Ga)N nanowire photoelectrodes,such PD can generate the positive(33.3 mA W−1)and negative(-0.019 mA W−1)photo-responsivity under ultraviolet(UV)and visible illumination,respectively,leading to the bidirectional photocurrent *** to the introduction of quasi solid-state hydrogel,the PD can work without the liquid-electrolyte,thus remarkably reducing the volume from about 482 cm3 to only 0.18 ***,the use of hydrogel is found to enhance response speed in the UV range by reducing the response time for more than 95%,which is mainly attributed to the increased open circuit potential and reduced ion transport *** the GaN connecting segment is pretty thin,the piezoelectric charges generated by stress are proposed to have only a limited effect on the photocurrent ***,both the stable on-off switching characteristics and photocurrent densities can still be achieved after being bent 400 *** an excellent flexibility,this work creates opportunities for technological applications of bidirectional photocurrent PDs in flexible optoelectronic devices,e.g.,wearable intelligent sensors.

关键词： Flexible photodetector Bidirectional photocurrent Lift-off GaN-based nanowires Hydrogel Self-powered device