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Cr-assisted low-temperature densification of(Ti,Zr,Nb,ta,Mo)C high-entropy carbides with ultrafine grain and enhanced hardness

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Journal of Advanced Ceramics 2024年第6期13卷 780-788页

作者： Yang Liu Jiaji Liang Weiming Guo Shikuan Sun Yu Tian Hua-tay lin School of Electromechanical Engineering Guangdong University of TechnologyGuangzhou 510006China State Key Laboratory of High Performance Tools Guangdong University of TechnologyGuangzhou 510006China School of Material Science and Energy Engineering Foshan UniversityFoshan 528000China

While the use of low-melting-point metals as sintering aids for high-entropy carbide(HEC)ceramics has been well established,their existence can compromise hardness due to residual metallic *** study demonstrates an innovative strategy to meet this challenge,where(Ti,Zr,Nb,ta,Mo)C high-entropy carbide ceramics with ultrafine grains and enhanced hardness are obtained through chromium(Cr)-metal-assisted spark plasma sintering(SPS)at a temperature as low as 1600℃.The results show that the addition of 5 vol%Cr promotes the formation of highly densified single HEC phase ceramics with a high relative density(98.4%)and an ultrafine-grained microstructure(0.17μm).This low-temperature densification mechanism can be attributed to Cr’s solid-solution effect within the matrix and the increased carbon vacancies generated during *** grain size of the(Ti,Zr,Nb,ta,Mo)C ceramics with 5 vol%Cr metal addition is significantly smaller than that of Cr-free(Ti,Zr,Nb,ta,Mo)C ceramics sintered at 2000℃(3.03μm)or via traditional low-temperature liquid-phase sintering(1.3–1.5μm).Importantly,the addition of 5 vol%Cr substantially increased the hardness of the ceramics,with a remarkable increase from 23.57 to 28.16 GPa compared to that of the pure(Ti,Zr,Nb,ta,Mo)C ceramics,owing to the fine-grain strengthening and solid-solution strengthening *** work highlights the uniqueness of Cr metal as a sintering aid in achieving densification and hardness improvements in(Ti,Zr,Nb,ta,Mo)C ceramics,offering a promising strategy for improving the properties of HEC materials for further development in the near future.

关键词： solid solution sinterability hardness enhancement (Ti,Zr,Nb,ta,Mo)C high-entropy carbide(HEC)ceramics

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基于Kalman滤波与应变信号的舰船轴系推力辨识研究

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噪声与振动控制 2024年第2期44卷 32-36,43页

作者：马相龙吴昊薛林塔娜饶柱石邹冬林上海船舶设备研究所上海200031 上海交通大学机械系统与振动全国重点实验室上海200240

在线、实时、准确监测舰船螺旋桨推力对船-机-桨匹配设计、舰船快速性预报及推进轴系健康管理等具有重要意义。然而,受轴系振动及环境干扰等测量噪声影响,螺旋桨推力产生的微弱应变信号易被测量噪声淹没,导致难以准确测量推力。当前,一... 详细信息

在线、实时、准确监测舰船螺旋桨推力对船-机-桨匹配设计、舰船快速性预报及推进轴系健康管理等具有重要意义。然而,受轴系振动及环境干扰等测量噪声影响,螺旋桨推力产生的微弱应变信号易被测量噪声淹没,导致难以准确测量推力。当前,一些常用的信号降噪方法,比如傅里叶变换、小波分析等均是基于纯数据降噪,未考虑测量数据中潜藏的力学机制。不同于这类降噪方法,Kalman滤波可同时考虑测量数据噪声及数据中的力学机制,对目标实现最小方差无偏估计,因而有更高的估计精度。因此,本文利用Kalman滤波结合应变测量信号提出一种螺旋桨推力高精度、在线辨识方法。以恒定转速、变转速及低频波动转速3种工况为例,研究了不同信噪比下本文方法的推力辨识精度与鲁棒性。研究表明,在信噪比仅为20 d b时,推力辨识最大相对误差仅为4.85%,因此本文方法在低信噪比下仍有很高的辨识精度与鲁棒性。同时,本文提出方法属于时域辨识方法,在转速突变、螺旋桨缠绕渔网等突发工况时亦能实时跟踪推力变化,因此可用于螺旋桨推力及轴系状态的在线、实时监测。

关键词：振动与波 Kalman滤波推力辨识应变测量在线监测

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Identification of novel targets and mechanisms of wogonin on lung cancer,bladder cancer,and colon cancer

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未来食品学报(英文) 2024年第3期4卷 267-279页

作者： lin Zhou Yunran Hu Changxing Gao Congci Yu Zhiting Sun Weihong Ge Hui Yang Department of Pharmacy Affiliated Drum Tower Hospital of Nanjing University Medical SchoolNanjing 210008China China Pharmaceutical University Nanjing Drum Tower Hospital Nanjing 210008China Hospital for Skin Disease Institute of DermatologyChinese Academy of Medical Sciences and Peking Union Medical CollegeNanjing 210042China Department of Scientific Research Affiliated Drum Tower Hospital of Nanjing University Medical SchoolNanjing 210008

Wogonin(WOG)has been demonstrated to have anti-cancer activity,but the mechanisms remain *** this study,new targets of WOG were predicted for lung cancer,bladder cancer,and colon cancer by using bioinformatics *** might primarily suppress cancers via regulating arachidonic acid,Ras,MAPK,linoleic acid,PI3K Akt,and folate biosynthesis pathways.3-(4,5-dimethylthiazol-2-yl)-5-(3-carboxymethoxyphenyl)-2-(4-sulfophenyl)-2H-tetrazolium(MTS)assay showed that WOG inhibited the proliferation of A549 ***-time quantitative reverse transcription PCR(RT-qPCR)results indicated that anti-lung cancer effect of WOG was achieved by regulating the expression of 18 target genes,including AKRIbI0,AKRIC3,bDNF,CAVI,CXCL2,CYP2b6,CYP4F3,DAO,EGF,ENO3,IL6,PLA2Glb,PLA2G2F,PLA2G4A,PTGES,SLCOIbI,SLCOIb3,and *** Kaplan-Meier survival curves further confirmed that DAO,PLA2G1b,SLCO1b3 and TFAP2A were essential targets via which WOG affected lung cancer ***,bDNF,FGF2,and PTGS1 were predicted to be the targets via which WOG alleviated cancer proliferation and invasion in bladder *** for colon cancer,WOG might induce autophagy and inhibit proliferation by down-regulating NTF4 and *** study will provide clue for using wOG as a promising antineoplastic agent in basic and translational research,and bring light to the application of herbs containing WOG as food supplements.

关键词： Wogonin targets Lung cancer bladder cancer Colon cancer

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tabOX: A water-soluble tetraanionic rectangular molecular container for conjugated molecules and taste masking for berberine and palmatine

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Chinese Chemical Letters 2024年第5期35卷 175-178页

作者： Qihan lin Jiabin Xing Yue-Yang Liu Gang Wu Shi-Jia Liu Hui Wang Wei Zhou Zhan-Ting Li Dan-Wei Zhang Department of Chemistry Shanghai Key Laboratory of Molecular Catalysis and Innovative MaterialsFudan UniversityShanghai 200438China

A water-soluble macrocycle that bears four carboxylate anions has been designed and prepared,which forms a rectangular cavity that can efficiently encapsulate discrete electron-deficient aromatic compounds,including berberine and *** macrocycle is revealed to be highly biocompatible and able to inhibit the bitter taste of the two drugs.

关键词： Macrocycle Multianion Molecular container Molecular recognition bitter taste masking

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tabHLH27 orchestrates root growth and drought tolerance to enhance water use efficiency in wheat

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Journal of Integrative Plant biology 2024年第7期66卷 1295-1312页

作者： Dongzhi Wang Xiuxiu Zhang Yuan Cao Aamana batool Yongxin Xu Yunzhou Qiao Yongpeng Li Hao Wang Xuelei lin Xiaomin bie Xiansheng Zhang Ruilian Jing baodi Dong Yiping Tong Wan Teng Xigang Liu Jun Xiao Key Laboratory of Plant Cell and Chromosome Engineering Institute of Genetics and Developmental BiologyChinese Academy of SciencesBeijing 100101China University of Chinese Academy of Sciences Beijing 100049China Center for Agricultural Resources Research Institute of Genetics and Developmental BiologyChinese Academy of SciencesShijiazhuang 050022China Key Laboratory of Crop biology College of Life SciencesShandong Agricultural UniversityTai'an 271018China State Key Laboratory of Crop Gene Resources and breeding Institute of Crop SciencesChinese Academy of Agricultural SciencesBeijing 100081China Ministry of Education Key Laboratory of Molecular and Cellular biology Hebei Research Center of the Basic Discipline of Cell BiologyHebei Collaboration Innovation Center for Cell Signaling and Environmental AdaptationHebei Key Laboratory of Molecular and Cellular BiologyCollege of Life SciencesHebei Normal UniversityShijiazhuang 050024China Centre of Excellence for Plant and Microbial Science(CEPAMS) JIC‐CASBeijing 100101China

Cultivating high-yield wheat under limited water resources is crucial for sustainable agriculture in semiarid *** water scarcity,plants activate drought response signaling,yet the delicate balance between drought tolerance and development remains *** genome-wide association studies and transcriptome profiling,we identified a wheat atypical basic helix-loop-helix(b HLH)transcription factor(TF),tab HLH27-A1,as a promising quantitative trait locus candidate for both relative root dry weight and spikelet number per spike in *** HLH27-A1/b1/D1 knockout reduced wheat drought tolerance,yield,and water use efficiency(WUE).tab HLH27-A1 exhibited rapid induction with polyethylene glycol(PEG)treatment,gradually declining over *** activated stress response genes such as ta CbL8-b1 and ta CPI2-A1 while inhibiting root growth genes like ta SH15-b1 and ta WRKY70-b1 under short-term PEG *** distinct transcriptional regulation of tab HLH27-A1 involved diverse interacting factors such as ta AbI3-D1 and tab *** variations of tab HLH27-A1influence its transcriptional responses to drought stress,with tab HLH27-A1^(Hap-II)associated with stronger drought tolerance,larger root system,more spikelets,and higher WUE in ***,the excellent tab HLH27-A1^(Hap-II)was selected during the breeding process in China,and introgression of tab HLH27-A1^(Hap-II)allele improved drought tolerance and grain yield,especially under water-limited *** study highlights tab HLH27-A1's role in balancing root growth and drought tolerance,providing a genetic manipulation locus for enhancing WUE in wheat.

关键词： drought tolerance GWAS root growth wheat WUE

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轻合金矩形管件充液压制成形缺陷及横截面尺寸控制

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中国有色金属学报 2024年第6期34卷 1952-1963页

作者：温时宇崔晓磊林鹏哈尔滨工业大学金属精密热加工国家级重点实验室哈尔滨150001 太原理工大学材料科学与工程学院太原030024

管材充液压制是一种先进的低载荷液压成形工艺,可用于整体成形复杂薄壁管状构件。与内高压成形不同,充液压制过程中内压只起支撑作用避免失稳屈曲,主要通过模具压制获得管件外形轮廓。压制过程管坯厚向存在拉-压应力梯度,导致卸载后管... 详细信息

管材充液压制是一种先进的低载荷液压成形工艺,可用于整体成形复杂薄壁管状构件。与内高压成形不同,充液压制过程中内压只起支撑作用避免失稳屈曲,主要通过模具压制获得管件外形轮廓。压制过程管坯厚向存在拉-压应力梯度,导致卸载后管件截面易产生回弹,影响尺寸精度。本研究通过对5052、AZ31b和ta1三种管材进行充液压制成形实验,分析了支撑内压和环向压缩率对矩形管件横截面尺寸的影响规律。结果表明:当支撑内压为0.6p_(s)~0.8p_(s)时,管件截面的回弹最小,此时最大回弹量小于1.5 mm,对应回弹率小于5.2%,上、下圆角半径相差小于0.1 mm。通过控制环向压缩率可减小管件回弹,截面尺寸与设计尺寸相差小于0.2 mm,尺寸偏差小于0.7%。对于5052-H、5052-O、AZ31b-M和ta1-Y矩形管件,其控制尺寸精度所需的环向临界压缩率分别为1.8%、1.7%、1.9%和1.8%。

关键词：充液压制成形轻合金管材成形缺陷尺寸精度支撑内压

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The effects of pressure, temperature, and depth/diameter ratio on the microvia filling performance of Ag-coated Cu micro-nanoparticles for advanced electronic packaging

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International Journal of Smart and Nano Materials 2022年第4期13卷 543-560页

作者： Guannan Yang Shaogen Luo bo Luo Yan Zuo Shiwo ta Tingyu lin Zhaohui Zhao Yu Zhang Chengqiang Cui State Key Laboratory of Precision Electronic Manufacturing Technology and Equipment Guangdong University of TechnologyGuangzhouGuangdongChina Jihua Laboratory FoshanGuangdongChina State Key Laboratory of Advanced Materials and Electronic Components Fenghua Advanced Technology Co.LtdZhaoqingGuangdongChina Guangdong Fozhixin Microelectronics Technology Research Co.Ltd FoshanGuangdongChina beijing Compo Advanced Technology Co.Ltd BeijingChina

Conductive fillers made from metal nanoparticles offer many advan-tages for the fabrication of a variety of electronic devices,but when they have a porous structure,their poor conductivity limits their adoption in many *** this study,an Ag-coated Cu micro-nanoparticle paste is used to achieve compact filling of blind vias on flexible copper clad polyimide laminates through a multistep filling and sintering *** filled blind vias achieve a resistivity as low as 6.2μΩ·cm,which is comparable that of electroplated blind *** sintering pressure and temperature promote the filling performance,while the conductivity deteriorates at a via depth/diameter ratio greater than 1:*** element simulations reveal a stress inhomogeneity in vias with large depth/diameter ratios,which is the key to understanding the evolution of the conductive properties of a paste-filled *** study provides an effective method for high-performance microvia filling as well as insights into the mechanism that influences its performance.

关键词： Ag-coated Cu micronanoparticles vertical interconnection microvia filling sintering

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A Deep Learning-based Continuous blood Pressure Measurement by Dual Photoplethysmography Signals

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Computers, Materials & Continua 2022年第2期70卷 2937-2952页

作者： Chih-ta Yen Sheng-Nan Chang Liao Jia-Xian Yi-Kai Huang Department of Electrical Engineering Taiwan Ocean UniversityKeelung202301Taiwan Department of Internal Medicine National Taiwan UniversityYun-Lin BranchDou-Liu640Taiwan Department of Electrical Engineering National Formosa UniversityYunlin632Taiwan

This study proposed a measurement platform for continuous blood pressure estimation based on dual photoplethysmography(PPG)sensors and a deep learning(DL)that can be used for continuous and rapid measurement of blood pressure and analysis of cardiovascular-related *** proposed platform measured the signal changes in PPG and converted them into physiological indicators,such as pulse transit time(PTT),pulse wave velocity(PWV),perfusion index(PI)and heart rate(HR);these indicators were then fed into the DL to calculate blood *** hardware of the experiment comprised 2 PPG components(i.e.,Raspberry Pi 3 Model b and analog-todigital converter[MCP3008]),which were connected using a serial peripheral *** DL algorithm converted the stable dual PPG signals acquired from the strictly standardized experimental process into various physiological indicators as input parameters and finally obtained the systolic blood pressure(SbP),diastolic blood pressure(DbP)and mean arterial pressure(MAP).To increase the robustness of the DL model,this study input data of 100 Asian participants into the training database,including those with and without cardiovascular disease,each with a proportion of approximately 50%.The experimental results revealed that the mean absolute error and standard deviation of SbP was 0.17±0.46 *** mean absolute error and standard deviation of DbP was 0.27±0.52 *** mean absolute error and standard deviation of MAP was 0.16±0.40 mmHg.

关键词： Deep learning(DL) blood pressure continuous non-invasive blood pressure measurement photoplethysmography(PGG)

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Human dendritic cell-specific ICAM-3-grabbing non-integrin downstream signaling alleviates renal fibrosis via Raf-1 activation in systemic candidiasis

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Cellular & Molecular Immunology 2019年第3期16卷 288-301页

作者： Wen-Yu Chen Sheng-Yang Wu ta-Chun lin Shuei-Liong lin betty A.Wu-Hsieh Graduate Institute of Immunology College of MedicineNational Taiwan UniversityTaipeiTaiwanChina Graduate Institute of Physiology College of MedicineNational Taiwan UniversityTaipeiTaiwanChina

We generated a human dendritic cell-specific ICAM-3-grabbing non-integrin(DC-SIGN)transgenic mouse in which renal tubular epithelial cells expressed *** transgenic mice were infected with Candida albicans intravenously to study how DC-SIGN expression affected the pathogenesis of systemic *** discovered that,while *** infection induced renal fibrosis in both transgenic and littermate control mice,the transgenic mice had significantly lower levels of Acta2,Col1a2,Col3a1,and Col4a1 mRNA transcripts compared to the ***-1,an emerging biomarker for kidney injury,along with Tnf,Il6,and Tgfb1 transcripts,were lower in infected transgenic mice,and yet,the levels of Il10 remained comparable to the *** renal CD45+infiltrating cells were the source of Tnf,Il6,and Il10,LTL+renal proximal tubular epithelial cells were TGF-β1 producers in both infected transgenic and littermate ***-SIGN-expressing tubular epithelial cells produced less TGF-β1 in response to *** *** vivo experiments demonstrated that renal proximal tubular epithelial cell production of TGF-β1 was key to ***-induced renal fibrosis and *** of transgenic mice induced a marked increase of phosphorylated Raf-1 and p38 in the ***,ERK1/2 and JNK phosphorylation was more pronounced in the infected-littermate ***,treating the infected transgenic mice with a Raf-1 inhibitor increased the levels of the Tgfb1,Kim1,and Acta2 *** results indicate that DC-SIGN signaling,through activation of Raf-1 and p38 and suppression of JNK and ERK1/2 phosphorylation,reduces TGF-β1 production and ***-induced renal *** study reveals for the first time the effect of DC-SIGN expression on ***-induced renal fibrosis.

关键词： DC-SIGN Candida albicans Renal fibrosis TGF-β1 Raf-1

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数据驱动方法揭示单原子掺杂金红石氧化物在甲烷活化过程中的活性位点

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Science China Materials 2024年第4期67卷 1231-1242页

作者：卫奋飞葛冰青董佩佩万强胡茜茜林森 College of Chemistry Fuzhou UniversityFuzhou 350002China Institute(College)of Integrative Medicine Dalian Medical UniversityDalian 116044China Department of Chemistry and Materials Science Zhejiang Normal UniversityJinhua 321004China Kuang Yaming Honors School Nanjing UniversityNanjing 210023China

金属氧化物通常用于甲烷的活化和转化,但总是受到过度氧化的影响.引入单原子是解决这一难题的一种有吸引力的方法,但掺杂单原子的实际作用仍存在争议.因此,开发性能描述符来预测掺杂表面上不同位点之间的反应性至关重要.在这项工作中,... 详细信息

金属氧化物通常用于甲烷的活化和转化,但总是受到过度氧化的影响.引入单原子是解决这一难题的一种有吸引力的方法,但掺杂单原子的实际作用仍存在争议.因此,开发性能描述符来预测掺杂表面上不同位点之间的反应性至关重要.在这项工作中,采用单原子(D_(guest),D=Ti,V,Cr,Mn,Nb,Mo,Ru,Rh,ta,Re,Os,Ir,Pt,Si,Ge和Sn)掺杂的金红石型金属氧化物(MO_(2),M=Ru,Rh,Ir,Pt,Mo)作为模型催化剂,利用密度泛函理论计算和数据驱动方法研究了甲烷在不同表面位点上的活化情况,并阐明了此类掺杂表面的实际活性位点.利用机器学习方法,从特征组合描述符的大空间中获得了多维描述符,从而可以统一预测D_(guest)和M_(host)上活化CH_(4)的能垒,而不受过渡态计算的影响.最后,MO_(2)上客体位点对选择性氧化的调节作用得到了证实.我们的工作证明了掺杂剂在催化过程中的复杂作用,所开发的描述符有助于确定活化能,为基于金红石氧化物的催化剂提供潜在的选择性氧化位点.

关键词：金属氧化物单原子选择性氧化过度氧化特征组合描述符数据驱动方法催化过程

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