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Effect of different metal sulfate precursors on structural and catalytic performance of zirconia in dehydration of methanol to dimethyl ether

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燃料化学学报 2018年第1期46卷 67-74页

作者： abd el-Aziz A.Said mohamed abd el-aal Chemistry Department Faculty of ScienceAssiut University71516 AssiutEgypt

ZrO_2 was treated with 10% SO_4^(2-) from different metal sulfate precursors for methanol dehydration to dimethyl *** the samples exhibited tetragonal phase and no diffraction peaks corresponding to metal sulfates or metal oxides were *** FT-IR results revealed that there were different interactions between sulfate and ZrO_2,and this had a great effect on the surface area of the *** catalytic activity was measured over the catalysts in the temperature range of 100-300 ℃.The results revealed that sulfated zirconia with CuSO_4·5 H_2O and Al_2(SO_4)_3·16 H_2O showed the best catalytic *** maximum yield of DME ≈87% was obtained over CuSZ at a reaction temperature of 275 ℃.Moreover,the catalytic activity of the catalysts was correlated well with their surface acidity that measured by dehydration of isopropanol.

关键词： MSO 4/ZrO2 甲醇脱水 DME

3D FEM simulations and experimental validation of plastic deformation of pure aluminum deformed by ECAP and combination of ECAP and direct extrusion

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Transactions of Nonferrous Metals Society of China 2017年第6期27卷 1338-1352页

作者： mohamed Ibrahim abd el aal Mechanical engineering Department College of Engineering Prince Sattam Bin Abdulaziz UniversityWadi Addawasir Kingdom of Saudi Arabia Mechanical Design & Production Department Faculty of Engineering Zagazig University Zagazig Egypt

Rigid-viscoplastic3D finite element simulations(3D FEM)of the equal channel angular pressing(ECAP),thecombination of ECAP+extrusion with different extrusion ratios,and direct extrusion of pure aluminum were performed ***3D FEM simulations were carried out to investigate the load-displacement behavior,the plastic deformationcharacteristics and the effective plastic strain homogeneity of Al-1080deformed by different forming *** simulationresults were validated by microstructure observations,microhardness distribution maps and the correlation between the effectiveplastic strain and the microhardness ***3D FEM simulations were performed successfully with a good agreement with theexperimental *** load-displacement curves and the peak load values of the3D FEM simulations and the experimentalresults were close from each *** microhardness distribution maps were in a good conformity with the effective plastic straincontours and verifying the3D FEM simulations *** ECAP workpiece has a higher degree of deformation homogeneity thanthe other deformation *** microhardness values were calculated based on the average effective plastic *** microhardness values fitted the experimental results *** microstructure observations in the longitudinal andtransverse directions support the3D FEM effective plastic strain and microhardness distributions result in different formingprocesses.

关键词： equal channel angular pressing (ECAP) extrusion finite element method (FEM) microhardness deformation homogeneity microstructure

Influence of ECAP as grain refinement technique on microstructure evolution, mechanical properties and corrosion behavior of pure aluminum

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Transactions of Nonferrous Metals Society of China 2015年第12期25卷 3865-3876页

作者： mohamed Ibrahim abd el aal M.M.SADAWY Mechanical Design and Production Department Faculty of Engineering Zagazig University Mining and Petroleum Engineering Department Al-Azhar University

Pure aluminum samples were processed by equal channel angular pressing（ECAP） up to 10 passes at room temperature. The effects of the ECAP number of passes on the microstructure evolution, the mechanical properties, deformation homogeneity and corrosion behavior of the processed samples were fully investigated. The imposed strain resulted in an obvious reduction in the grain size from 390 μm before ECAP down to 1.8, 0.4, and 0.3 μm after ECAP up to 2, 4 and 10 passes, respectively. The microhardness, deformation homogeneity and tensile strength were increased while the elongation decreased with the increase of ECAP number of passes. Immersion tests, open circuit potential, Tafel polarization, cyclic polarization and potentiostatic measurements in 3.5% Na Cl solution revealed an obvious improvement in the corrosion resistance of ECAP processed samples compared with the as-cast sample. The increase of the number of passes can be used successfully in producing ultra-fine grained（UFG） bulk pure aluminum sample with a high misorientation angle, reasonably high mechanical properties and corrosion resistance.

关键词： equal channel angular pressing(ECAP) microstructure mechanical properties corrosion resistance passive film pitting

Prospective Study of Holter Monitoring in Pediatric Patients at Sohag University Hospital

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World Journal of Cardiovascular Diseases 2020年第7期10卷 460-472页

作者： Safaa Ali Feby Sobhy mohamed abd el aal Shiamaa Mahamoud Sohag University Hospital Sohag Egypt

Background: To estimate the various indications, values and misuses of Holter monitoring in the diagnosis and management of pediatric patients. Methods: The study was a prospective observational study, carried out at Pediatric Arrhythmia Clinic and at PICU of Sohag University Hospital over two years from 09/2017 to 09/2019. It encountered 80 pediatric patients (34 females), their age ranged from 29 days to 15 years with mean age of 6.18 years. All patients were subjected to echocardiography, 12 leads ECG and holter monitoring for 24 hours. Minimum, mean, maximum heart rate, rhythms and corrected QT were evaluated. Indications of Holter examination, its abnormalities were analyzed, also its positive diagnosis and management were defined. Results: Palpitations and syncopy were the main indications for holter examination 22 (27.50%) patients for each, abnormal examination in 17 (21.25%), chest pain in 13 patients (16.25%) and cardiomyopathy (7.5%) (one with Hypertrophic Cardiomyopathy and five with Dilated Cardiomyopathy). There were 50 (62.50%) patients had abnormalities in Holter recordings. The highest contribution to diagnosis was in cardiomyopathy (83.3%) where the most common abnormalities were ventricular tachycardia (50%) and ventricular premature beats in (33.3%). An abnormal ECG was significantly associated with a higher diagnostic yield (p = 0.0001). Conclusion: The most important indications for Holter monitoring include palpitations, syncope, abnormal physical exam findings, chest pain, and cardiomyopathy. Holter monitoring is an extremely important tool in the assessment of patients with dilated cardiomyopathy. HM detects serious arrhythmias to identify patients who are at increased risk for

关键词： Holter Pediatric Arrhythmia ECG

Dysprosium oxide,alumina,and graphene oxide reinforced polycaprolactone thin films:Thermal stability,morphology,and cell viability

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Journal of Rare Earths 2024年第7期42卷 1337-1343,I0005页

作者： mohamed Tharwat elabbasy mohamed R.Atteya Mai A.Samak Mousa abdelrahman Tahani AlMahmoud M.A.el-Morsy A.A.Menazea M.F.H.abd el-Kader Department of Public Health College of Public Health and Health InformaticsUniversity of Ha'ilHa'il2440Saudi Arabia Food Control Department Faculty of Veterinary MedicineZagazig UniversityZagazig44519Egypt Department of Physical Therapy College of Applied Medical SciencesUniversity of Ha'ilHa'ilSaudi Arabia Department of Histology and Cell Biology Faculty of MedicineZagazig UniversityZagazig44519Egypt College of Nursing University of Ha'ilHa'ilSaudi Arabia College of Science and Humanities in Al-Kharj Physics DepartmentPlasma Technology and Material Science UnitPrince Sattam Bin Abdulaziz UniversityAl-kharj11942Saudi Arabia Physics Department Faculty of ScienceUniversity of DamiettaNew Damietta34517Egypt Spectroscopy Department Physics Research InstituteNational Research CentreDokki12622GizaEgypt Biophysics Department Faculty of ScienceCairo UniversityGizaEgypt

Developing a biomaterial for wound healing applications is still a ***,dysprosium oxide(Dy_(2)O_(3)),aluminum oxide(Al_(2)O_(3)),and graphene oxide(GO)were embedded in cast films based on polycaprolactone(PCL)to be examined for wound dressing *** techniques were used to characterize the fabricated films including X-ray diffraction(XRD),Fourier transform infrared spectroscopy(FTIR),Raman,and scanning electron microscopy(SEM),besides their biological *** thermogravimetric analysis(TGA)exhibits high thermal stability as the scaffold weight decreases slightly to 98.6%after raising the temperature from room temperature to 280℃.The cell viability was investigated and it is shown that the viable cells grow up to approximately 93%at 75μg/***,the cell attachment shows excellent behavior as the cells attach on most of the surface of the modified PCL which shows high biocompatibility.

关键词： Wound healing Polycaprolactone Dy_(2)O_(3) Al_(2)O_(3) Biocompatible Rare earths

Eco-toxicity and health risk assessment of polycyclic aromatic hydrocarbons in surface sediments of Burullus Lake in Egypt

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China Geology 2024年第3期7卷 460-468页

作者： Hanan E Osman mohamed H E el-Morsy Hazem T abd el-Hamid Department of Biology Faculty of Applied ScienceUmm Al-Qura UniversityMecca 24382Saudi Arabia Deanship of Scientific Research Umm Al-Qura UniversityMakkah 24372Saudi Arabia National Institute of Oceanography and Fisheries(NIOF) Cairo 11865Egypt Botany and Microbiology Department Faculty of ScienceAl-Azhar UniversityCairo 11651Egypt

Polycyclic aromatic hydrocarbons(PAHs)are ubiquitous environmental contaminants of growing concern due to their potential ecological and human health *** study presents a comprehensive assessment of PAHs contamination in the surface sediments of Burullus Lake,a vital and second largest delta lake in *** aim was to evaluate the eco-toxicity and potential health risks associated with the presence of these *** seven sediment samples were collected from various drains in the southern part of Burullus *** extraction method was employed to extract PAHs(16PAHs)from the sediment ***,target compounds were located using *** results showed that samples contained PAHs levels ranging from 0.038×10^(-6)to 0.459×10^(-6),which is considered heavily polluted by the European standard for PAHs ***,there was no apparent source of PAHs in the elKhashah drain or the Brinbal Canal,as HPLC found none of the *** most prevalent compound in sediment samples along the study area was *** diagnostic indices in the present study indicated that the hydrocarbons in the region originated from pyrolytic and man-made sources along the drains of Burullus *** principal component analysis(PCA)and diagnostic ratios revealed that coal combustion and pyrolytic sources were responsible for the PAHs contamination in the surface *** non-carcinogenic risk(HI),which is the product of the HQs for the adult and child populations,respectively,was *** values under 1,therefore,demonstrated that they had no carcinogenic effects on human *** and MEQs in the sediments of Burullus Lake do not have a cancer-causing impact on *** the safety of nearby wildlife,aquatic life,and people,all activities that raise petroleum hydrocarbon levels in Burullus Lake must be adequately regulated and *** to the ecological risk assessment,there is little chance that PAHs will be found

关键词： Polycyclic aromatic hydrocarbons Diagnostic indices Toxicity Delta lake sediment Burullus Lake Human health risk Aquatic ecosystem HPLC Coal combustion

Privacy-preserved learning from non-i.i.d data in fog-assisted IoT:A federated learning approach

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Digital Communications and Networks 2024年第2期10卷 404-415页

作者： mohamed abdel-Basset Hossam Hawash Nour Moustafa Imran Razzak mohamed abd elfattah Faculty of Computers and Informatics Zagazig UniversityZagazigSharqiyah44519Egypt School of Engineering and Information Technology University of New South Wales@ADFACanberraACT2600Australia Deakin University Geelong Waurn Ponds CampusAustralia Computer Science Department Misr Higher Institute for Commerce and ComputersMansoura35511Egypt

With the prevalence of the Internet of Things(IoT)systems,smart cities comprise complex networks,including sensors,actuators,appliances,and cyber *** complexity and heterogeneity of smart cities have become vulnerable to sophisticated cyber-attacks,especially privacy-related attacks such as inference and data poisoning *** Learning(FL)has been regarded as a hopeful method to enable distributed learning with privacypreserved intelligence in IoT *** though the significance of developing privacy-preserving FL has drawn as a great research interest,the current research only concentrates on FL with independent identically distributed(i.i.d)data and few studies have addressed the non-i.i.d *** is known to be vulnerable to Generative Adversarial Network(GAN)attacks,where an adversary can presume to act as a contributor participating in the training process to acquire the private data of other *** paper proposes an innovative Privacy Protection-based Federated Deep Learning(PP-FDL)framework,which accomplishes data protection against privacy-related GAN attacks,along with high classification rates from non-i.i.d ***-FDL is designed to enable fog nodes to cooperate to train the FDL model in a way that ensures contributors have no access to the data of each other,where class probabilities are protected utilizing a private identifier generated for each *** PP-FDL framework is evaluated for image classification using simple convolutional networks which are trained using MNIST and CIFAR-10 *** empirical results have revealed that PF-DFL can achieve data protection and the framework outperforms the other three state-of-the-art models with 3%–8%as accuracy improvements.

关键词： Privacy preservation Federated learning Deep learning Fog computing Smart cities

Depositional Environment,Petrophysical Evaluation and electrical Properties of Zeit Formation,Northwestern Shore of Gulf of Suez,Egypt

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Journal of Earth Science 2024年第5期35卷 1720-1737页

作者： mohamed M.Gomaa Emad A.abd el Aziz Geophysical Sciences Department National Research CentreEl-Behoos St.DokkiCairo 12622Egypt

The Zeit sand reservoir is one of the most prolific formations at Northwestern side of the Gulf of *** this research we will try to coordinate between electrical,petrophysical properties,depositional environment and facies discrimination in order to evaluate the hydrocarbon potentiality of studied Zeit *** statistical parameters for potassium(K),thorium(Th)and Th/U ratio contents have a general increase towards northwestern parts,whereas uranium(U)content has a general increase towards southeastern *** sandstone facies is distinguished from the other facies by its thorium content>4 ppm.U has high carbonate content(U≥1 ppm).Rocks'electrical properties vary greatly depending on a number of *** measurements were taken at frequencies range of(5×10^(-4)Hz-100 kHz)for fully saturated samples(clayey sandstone)with NaCl(20 gm/L).As salinity,clay content,and frequency increase,consequently does the electrical *** continental condition are present in northwestern part(back-sea)which is distinguished by high K percent,high Th,high Th/U ratio,and low U *** K,Th,and Th/U ratio contents,with high U contents,characterize the marine depositional environment that existed around the east and southeastern parts(foresea coincide with the dipping of strata).Furthermore,the studied Zeit Formation has good petrophysical properties that coincide with marine *** middle and eastern parts(around ISS-94 and CSS-288)is a good reservoir(porosity 36%-39%,shale content<15%,hydrocarbon saturation 71%-92%,and net pay thickness 17-63 feet).

关键词： Zeit Formation petrophysical evaluation depositional environment Spectral Gamma Ray electrical properties gulf of Suez sedimentology

Pyronaridine combined with diminazene aceturate inhibits Babesia in vitro and in vivo

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Asian Pacific Journal of Tropical Biomedicine 2024年第3期14卷 93-99页

作者： Shimaa abd el-Salam el-Sayed mohamed Z.Sayed-Ahmed Shaimaa Ahmed Awad Ali Nourah Alsadaan Nawazish Alam Mahmoud S.Alkhoudary Ikuo Igarashi mohamed abdo Rizk National Research Center for Protozoan Diseases Obihiro University of Agriculture and Veterinary MedicineInada-ChoObihiroHokkaido 080-8555Japan Department of Biochemistry and Chemistry of Nutrition Faculty of Veterinary MedicineMansoura UniversityMansoura 35516Egypt Department of Clinical Pharmacy College of PharmacyJazan UniversityJazan 45142Saudi Arabia Medical-Surgical Department College of NursingJouf UniversitySakaka 72388Saudi Arabia Critical Care and Emergency Nursing Faculty of NursingMansoura UniversityEgypt College of Nursing Jouf UniversitySakaka 72388Saudi Arabia Faculty of Pharmacy Mansoura UniversityMansoura 35516DakahliaEgypt Department of Internal Medicine and Infectious Diseases Faculty of Veterinary MedicineMansoura UniversityMansoura 35516Egypt

Objective:To evaluate the combination therapy of pyronaridine tetraphosphate and diminazene aceturate against Babesia in vitro and in ***:Bioinformatic analysis was performed using atom pair *** in vitro combination test was performed against Babesia bovis and Theileria ***,the in vivo chemotherapeutic efficacy of pyronaridine tetraphosphate in combination with diminazene aceturate was investigated against the growth of Babesia microti in mice using a fluorescence inhibitory ***:Pyronaridine tetraphosphate and diminazene aceturate exhibited nearly similar molecular *** in vitro combination of pyronaridine tetraphosphate and diminazene aceturate was synergistic on Babesia bovis and additive on Theileria *** addition,5 mg/kg pyronaridine tetraphosphate combined with 10 mg/kg diminazene aceturate inhibited Babesia microti growth significantly compared with those observed after treatment with 25 mg/kg diminazene aceturate alone from day 6 post treatment to day 12 post *** combination therapy also normalized the hematological parameters of infected ***:An oral dose of pyronaridine tetraphosphate combined with a subcutaneous dose of diminazene aceturate inhibits Babesia in vitro and in mice,suggesting it might be a new paradigm for the treatment of babesiosis.

关键词： Babesia Pyronaridine tetraphosphate Diminazene aceturate Babesiosis Theileria