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Meso-substituted cationic 3-and 4-N-Pyridylporphyrins and their Zn(II)derivatives for antibacterial photodynamic therapy

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Journal of Innovative Optical Health Sciences 2022年第1期15卷 1-16页

作者： Aram G.Gyulkhandanyan marina H.Paronyan Anna G.Gyulkhandanyan Karapet R.Ghazaryan marina v.parkhats Boris M.Dzhagarov Maria v.Korchenova Ekaterina N.Lazareva Elena S.Tuchina Grigor v.Gyulkhandanyan valery v.Tuchin H.Buniatyan Institute of Biochemistry National Academy of Sciences of Armenia 5/1 Paruir Sevak Street Yerevan 0014Armenia INSERM U1204 Universite d'Evry vald'Essonne-Universite Paris-Saclay 1 Ruedu Pere JarlanBatiment Maupertuis91025Evry-CourcouronnesFrance B.I.Stepanov Institute of Physics National Academy of Sciences of Belarus 68-2 Nezavisimosti AvenueMinsk 220072Belarus Science Medical Center Saratov State University 83 Astrakhanskaya StreetSaratov 410012Russia Laboratory of Laser Molecular Imaging and Machine Learning(LMIML)National Research Tomsk State University 36 Lenin Avenue Tomsk 634050Russia Laboratory of Laser Diagnostics of Technical and Living Systems Institute of Precision Mechanics and Control Russian Academy of Sciences Saratov 410028Russia

Photodynamic inactivation of microorganisms known as antibacterial photodynamic therapy(APDT)is one of the most promising and innovative approaches for the destruction of pathogenic *** the photosensitizers(PSs),compounds based on cationic porphyrins/metalloporphyrins are most successfully used to inactivate *** of meso-substituted cationic pyridylporphyrins and metalloporphyrins with various peripheral groups in the third and fourth positions of the pyrrole ring have been synthesized in *** aim of this work was to determine and test the most e®ective cationic porphyrins and metalloporphyrins with high photoactivity against Gram negative and Gram positive *** was shown that the synthesized cationic pyridylporphyrins/metalloporphyrins exhibit a high degree of phototoxicity towards both types of bacteria,including the methicillinresistant *** *** complexes of porphyrins are more phototoxic than metal-free porphyrin *** e®ectiveness of these Zn–metalloporphyrins on bacteria is consistent with the level of singlet oxygen *** was found that the high antibacterial activity of the studied cationic porphyrins/metalloporphyrins depends on four factors:the presence in the porphyrin macrocycle of a positive charge(+4),a central metal atom(Zn2þÞand hydrophobic peripheral functional groups as well as high values of quantum yields of singlet *** results indicate that meso-substituted cationic pyridylporphyrins/metalloporphyrins cannd wider application in photoinactivation of bacteria than anionic or neutral PSs usually used in APDT.

关键词： Antibacterial photodynamic therapy cationic porphyrins/metalloporphyrins phototoxicity Zn-metalloporphyrins singlet oxygen quantum yield Gram negative and Gram positive bacteria S.aureus MRSA E.coli Salmonella typhimurium.

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Alien invasive species in Siberia:current status and problem

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Journal of Arid Land 2013年第4期5卷 428-433页

作者： marina v OLONOvA YuanMing ZHANG Tomsk State University Lenin ave.36Tomsk 634036Russia Key Laboratory of Biogeography and Bioresource in Arid Land Xinjiang Institute of Ecology and GeographyChinese Academy of Sciences

Although alien and invasive plant species have been researched extensively in the European part of Russia,the situation in Siberia is another ***,alien and invasive species in Siberia have not received much attention because this problem was not especially acute in *** lack of attention on alien and invasive species in Siberia is attributed to three major reasons：1） Low vegetative productivity and sparse human populations in the Siberian territory have limited botanical research interest in the area.2） Severe Siberian climate likely prevents many alien and invasive species from increasing their distribution into Siberia.3） Most Siberian plant communities have not been human-transformed and thus may be resistant to ***,recent increased economic activities have resulted in increasing plant migration to Siberia,and this process should be ***,global environmental changes may also have made Siberia more favorable for more alien and invasive ***,research on alien and invasive species has begun in the Altai-Sayan region（Western Siberia） and the Magadan region （Northeastern Asia）.

关键词： alien invasive plants global climate change economic development Siberia

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Rare and endangered plant species of the Chinese Altai Mountains

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Journal of Arid Land 2010年第3期2卷 222-230页

作者： marina v.OLONOvA Tomsk State University

Altai (also named Altay in China) Mountain Country (Mountain System) is a unique natural region,located on the border between different floristic regimes of the Boreal and ancient Mediterranean sub-kingdoms,where distribution of plant species is actually limited. It is known to have sufficient endemic floral biodiversity in the Northern Asia. Many plants of Altai Mountain System need effective care and proper conservation measures for their survival and longer-term protection. Important Plant Area identified as the IUCN (the International Union for Conservation of Nature),specified criteria attract global attention for protection of floral biodiversity across the world. The records of 71 plant species from the Chinese Altai Mountains attributed to the criterion A and the dark conifer forests of Chinese Altai Mountains satisfied the criterion C,which may help qualify to fulfill the national obligation of the Convention on Biological Diversity.

关键词： conservation Important Plant Area endemics Altai Mountain System

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First Asian record of Panthera(Leo)fossilis(Mammalia,Carnivora,Felidae)in the Early Pleistocene of Western Siberia,Russia

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Integrative Zoology 2014年第4期9卷 517-530页

作者： marina v.SOTNIKOvA Irina v.FORONOvA Geological Institute of Russian Academy of Sciences MoscowRussia v.S.Sobolev Institute of Geology and Mineralogy Siberian Branch of Russian Academy of SciencesNovosibirskRussia

A lion-like pantherine felid is described as Panthera(Leo)fossilis from the late Early Pleistocene sediments of the Kuznetsk Basin(Western Siberia,Russia).The find of *** first recorded in Asia considerably extends the current notion of the eastward expansion of the most ancient *** Siberian lion is geologically the oldest form and is dimensionally among the largest members of the group of fossil lions on the Eurasian conti*** known by mandibular remains only,it is readily distinguished from Panthera(Leo)spelaea by a heavy built mandibular corpus with rectangular profile in the cheek teeth area,a deep,well-outlined and narrow anterior section of the masseteric fossa,and a largeр4 supported by a big unreduced anterior *** Siberian lion shares these features with the European Middle Pleistocene *** and the American Late Pleistocene P.(Leo)atrox,which suggests their close *** originated from *** and was isolated in North America south of the Late Pleistocene ice *** explains why the American lion has retained more primitive features than the coeval Eurasian cave lion P.(L.)spelaea.

关键词： Early Pleistocene evolution Panthera fossilis relationships Western Siberia

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Ecological Niche Modelling Reveals the Peculiarities of Ecological Disjunction Between Two Sympatric Racerunners in Kazakhstan:Eremias lineolata(Nikolsky,1897)and Eremias scripta(Strauch,1867)

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Asian Herpetological Research 2023年第2期14卷 123-137页

作者： marina A.CHIRIKOvA Dmitry v.MALAKHOv Institute of Zoology Committee of Scientific Ministry of Science and Higher EducationAl-Farabi 93 AkademgorodokAlmaty 050060Kazakhstan

The ecological-niche models for two sympatric species,Eremias lineolata(Nikolsky,1897)and Eremias scripta(Strauch,1867),reveal evidence of spatial and temporal disjunction in the actual niches of both *** lineolata demonstrates a wide range of adaptations and,at the same time,has a greater need for winter precipitation and minimal temperature than *** explanations for the thermal diversity of both species are *** variables(monthly temperatures,monthly solar radiation,etc.)are traditionally important for ectotherm ***,as many as half of the key variables in both species are related to different aspects of environmental water balance(precipitation,air humidity,vapor pressure).There are several ways in which moisture may impact the lizard’s life *** humidity is related to soil temperature and may be important during winter *** summer,soil humidity may support successful *** during the warm months is a key factor in maintaining the moisture content of the *** winter,snow cover provides a better thermal balance of the soil’s top layers where winter shelters are *** niche modeling(ENM)is an interdisciplinary approach combining the geographical,climatic,ecological,and biological aspects of the wellbeing of *** interdisciplinary approach lifts biological studies onto a new,integrative level,providing a comprehensive view on species biology and answering the questions that might not be answered if the traditional methods for studying animals were used alone.

关键词： ecology Kazakhstan niche modelling racerunners species distribution

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Selective sorptive removal of Methyl Red from individual and binary component solutions by mesoporous organosilicas of MCM-41 type

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Journal of Environmental Sciences 2021年第1期33卷 59-71页

作者： Nadiia v.Roik Lyudmila A.Belyakova marina O.Dziazko Chuiko Institute of Surface Chemistry of NAS of Ukraine 17 General Naumov Str.Kyiv 03164Ukraine

Organosilicas with chemically immobilized 3-aminopropyl and Methyl Red-containing surface groups were prepared by sol-gel condensation of tetraethyl orthosilicate and(3-aminopropyl)triethoxysilane in the presence of dye as part of the mixed micelles or dyecontaining silane as silica *** hexagonally arranged mesoporous structure of synthesized materials was confirmed by low-temperature nitrogen adsorption-desorption,xray diffraction,and TEM *** composition of MCM-41-type organosilicas was established by FT-IR spectroscopy and chemical analysis of surface *** of Methyl Red by organosilicas was studied from diluted phosphate buffer solutions in dependence of medium p H,duration of contact,and equilibrium concentration of *** was found that effective removal of Methyl Red takes place at p H values within a range of *** curves of Methyl Red sorption on organosilicas were analyzed by the Lagergren,Ho-McKey,and Weber-Morris kinetic *** was found that the pseudo-second-order model fits the kinetics of Methyl Red sorption on all synthesized materials and the intraparticle diffusion is not the only one mechanism controlling the rate of Methyl Red sorptive *** parameters of equilibrium sorption of Methyl Red on organosilicas of MCM-41 type were calculated using Langmuir,Freundlich,Redlich-Peterson,and Brunauer-Emmett-Teller *** of acid dyes with geometry similar or substantially different from Methyl Red on mesoporous silicas was studied from single and binary component mixtures in aqueous solutions with p H 4.8 and *** was found that selective sorption process is highly dependent on the structural characteristics and protolytic state of silica surface as well as acid dye.

关键词： MCM-41 Sol-gel synthesis Methyl Red Chemical modification Selective sorption

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Model acupuncture point:Bone marrow-derived stromal stem cells are moved by a weak electromagnetic field

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World Journal of Stem Cells 2016年第10期8卷 342-354页

作者： Artem N Emelyanov marina v Borisova vera v Kiryanova Laboratory of High Laser and Magnetic Technology North-Western State Medical University Training Laboratory of Physical Chemistry Institute of ChemistrySt. Petersburg State University Department of Physical Therapy and Rehabilitation North-Western State Medical University

AIM To show the existence of a structural formative role of magnetic fields(MFs) with respect to biological objects by using our proposed model of an *** We introduced a magnetised 10-100 μT metal rod(needle) into culture dishes with a negatively charged working surface and observed during 24 h how cells were arranged by MFs and by electrical fields(EFs) when attached. Rat and human bone marrow-derived stromal stem cells(r BMSCs and h BMSCs), human nonadherent mononuclear blood cells, NCTCs and A172 cells, and Escherichia coli(E. coli) were evaluated. The dish containing BMSCs was defined as the model of an acupoint. r BMSCs proliferative activity affected by the needle was investigated. For investigating electromagnetic field structures, we used the gas discharge visualisation(GDv) *** During 24 h of incubation in 50-mm culture dishes, BMSCs or the nonadherent cells accumulated into a central heap in each dish. BMSCs formed a torus(central ring) with an inner diameter of approximately10 mm only upon the introduction of the needle in the centre of the dish. The cells did not show these effects in 35- or 90-mm culture dishes or hydrophobic dishes or rectangular cuvettes. NCTCs and A172 cells showed unstable the effects and only up to two weeks after thawing. Moreover, we observed that the appearance of these effects depended on the season. In winter, BMSCs showed no the effects. GDv experiments revealed that the resonant annular illumination gradually formed from 10 to 18-20 s in polar solutions with and without cell suspension of BMSCs, NCTCs and E. coli when using circular 50-mm dishes, stimulation at 115 v and switching of the electrode poles at 1 kH z. All these data demonstrate the resonant nature of the central ring. Significant influence of MFs on the rB MSC proliferation rate was not *** BMSCs can be moved by MFs when in the presence of a constant EF and MF, when the cells are in the responsive functional state, and whe

关键词： Stem cell movement Magnetic targeting Acupuncture Model acupoint Frizzled-related protein Biology resonance Cytoplasm movement Glycocalyx

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The role of singlet oxygen and hydroxyl radical in the photobleaching of meso-substituted cationic pyridyl porphyrins in the presence of folic acid

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Journal of Innovative Optical Health Sciences 2024年第5期17卷 67-80页

作者： Lusine Mkrtchyan Torgom Seferyan marina parkhats Sergei Lepeshkevich Boris Dzhagarov Gagik Shmavonyan Elena Tuchina valery Tuchin Grigor Gyulkhandanyan Laboratory of Bioengineering Institute of Biochemistry After H.Buniatyan of the NAS of Armenia 5/1 Paruyr Sevak StreetYerevan 0014Armenia Laboratory of Biomedical Research Institute of Biochemistry after H.Buniatyan of the NAS of Armenia 5/1 Paruyr Sevak StreetYerevan 0014Armenia B.I.Stepanov Institute of Physics NAS of Belarus 68-2 Nezavisimosti Avenue Minsk 220072Belarus National Polytechnic University of Armenia 105 Teryan Street Yerevan 0009Armenia Science Medical Centre Saratov State University 83 Astrakhanskaya StreetSaratov 410012Russia

Using a photosensitizer(PS),light,and oxygen,photodynamic therapy creates cytotoxic reactive oxygen species,such as singlet oxygen(1O2),that kill cancer *** cancer cell lines have up to 300 times more folic acid receptors than healthy ***,folic acid is often used to improve selectivity of *** poses a disadvantage for *** this paper,we have studied the photoinduced changes of meso-substituted cationic pyridyl porphyrins in the presence of folic acid using uorescence and absorption *** this work,it was demonstrated that L-histidine,which is a 1O2 quencher,and D-mannitol,which is a hydroxyl radical quencher,can reduce photobleaching of cationic porphyrins and their interaction products with *** implies both singlet oxygen and hydroxyl radicals are involved in ***,our study revealed certain important features of the photobleaching of cationic porphyrins in the presence of folic acid.

关键词： Photodynamic therapy cancer quenchers histidine mannitol

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Crystal-field levels of Nd3+ in a new langasite compound Nd3CrGe3Be2O14

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Journal of Rare Earths 2019年第11期37卷 1250-1254页

作者： Sergei A.Klimin Boris v.Mill marina N.Popova Institute of Spectroscopy Russian Academy of SciencesTroitskMoscow 108840Russia Faculty of Physics M.V.Lomonosov Moscow State UniversityMoscow 119991Russia

We report on the crystal-field(CF)levels of Nd^3+in Nd3CrGe3Be2O14,a representative of recently synthesized Be-containing *** are the first in the family to contain two magnetic subsystems,1 D chromium and Kagome-like rare-earth ***-resolution broad-band temperature-dependent spectra allow us to find all five CF Kramers doublets of the ground 4I9/2 CF multiplet and 38 levels of the excited 4I11/2,13/2,15/2,4F3/2,4F5/2+2H9/2,4F7/2+4S3/2 and 4F9/2 CF *** data form a basis for a future exploration of this interesting two-sublattice magnet with frustrated *** transitions between Kramers doublets of Nd^3+indicate magnetic activity of 1D-chromium chains at T<20 K.

关键词： Langasite Two magnetic subsystems High-resolution spectroscopy Crystal-field levels Magnetic correlations Rare earths

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Fluorescence of Single Conjugated Chains of MEH-PPv Dispersed in Polymer Matrix: What Do We See in the Microscope?

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Chinese Journal of Chemistry 2023年第19期41卷 2536-2544页

作者： Mingyi Xie marina v.Kuzimenkova Per-Olof Larsson Yuxi Tian Ivan G.Scheblykin Key Laboratory of Mesoscopic Chemistry of MOE School of Chemistry and Chemical EngineeringNanjing UniversityNanjingJiangsu210023 China Chemical Physics and NanoLund Lund UniversityPO Box 124SE-22100 LundSweden Pure and Applied Biochemistry Lund UniversityPO Box 124SE-22100 LundSweden

It has been a mystery that the detected fluorescence intensity of single MEH-PPv molecules is much lower than expected based on their chain *** this review,after re-evaluating of the literature data in the light of new specially designed experiments,we present a comprehensive explanation of this issue:The actual size of MEH-PPv molecules at single molecule level is much smaller than expected due to de-aggregation and chain scission,while static quenching("dark matter")also exists for large molecules,further reducing their brightness.

关键词： MEH-PPv Single molecule spectroscopy Brightness Fluorescence Molecular weight anrohonci

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