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Exploring the synthesis conditions to control the morphology of gold-iron oxide heterostructures

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Nano Research 2019年第8期12卷 1781-1788页

作者： Pablo Tancredi Luelc Souza da costa Sebastian Calderon Oscar Moscoso-Londono Leandro M. Socolovsky Paulo J. ferreira Diego Muraca daniela Zanchet marcelo Knobel Laboratory of Amorphous Solids INTECINFaculty of EngineeringUniversity of Buenos Aires - CONICETBuenos AiresCP C1063ACVArgentina Department of Inorganic Chemistry Institute of ChemistryUniversity of Campinas (UNICAMP)CP615413083-970CampinasSPBrazil Brazilian Nanotechnology National Laboratory (LNNano) Rua Giuseppe Maximo Scolfaro 10000CampinasSPBrazil International Iberian Nanotechnology Laboratory (INL) Av. Mestre Jose Veiga s/n4715-330 BragaPortugal “Gleb Wataghin” Institute of Physics University of Campinas (UNICAMP)CEP 13083-859CampinasSPBrazil Autonomous University of Manizales Antigua Estacion del FerrocarrilManizalesCP 170001Colombia Facultad Regional Santa Cruz Universidad Tecnoldgica Nacional - CIT Santa Cruz (CONICET)- Av delos Inmigrantes 555Rio GallegosSanta CruzArgentina Materials Science and Engineering Program The University of Texas at AustinAustinTexas 78712USA

Gold-iron oxide nano-heterostructures with a clear and well-defined morphology were prepared via a seed-assisted method. The synthesis process and the events of heterogeneous nucleation during the decomposition of the iron precursor were carefully studied in order to understand the mechanism of the reaction and to tailor the architecture of the fabricated heterostructures. When employing Au seeds of 3 and 5 nm, nanoparticles with a dimer-like morphology were produced due to the occurrence of a single iron oxide nucleation event. Otherwise, multi-nucleation events could be favored by two mechanisms:(i) by the incorporation of a reducing agent and the slowing down of the heating protocol, leading to a core-shell system;(ii) by the increase of the Au seed size to 8 nm, leading to a flower-like system. Further increase of the Au seed size to 12 nm using similar synthesis conditions promotes the homogeneous nucleation and growth of the iron oxide phase, without formation of heterostructures. An in-depth study was performed on the gold-iron oxide heterostructures to confirm the epitaxial growth of the oxide domain over the Au seed and to analyze the elemental distribution of the components within the heterostructures. Finally, it was found that the modification of the plasmonic properties of the Au nanoparticles are strongly influenced by the architecture of the heterostructure, with a more pronounced damping effect for the systems produced after multi-nucleation events.

关键词： nanoparticles gold-iron oxide heterostructures heterogeneous nucleation epitaxial growth HR-microscopy

Governing Climate Change Risks： Implications for Mitigation and Adaptation

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Fudan Journal of the Humanities and Social Sciences 2016年第4期9卷 589-606页

作者： Fabiana Barbi Leila da costa ferreira Center for Environmental Studies and Research (Nepam) University of Campinas (Unicamp)Campinas Brazil Center for US-China Policy Studies (CUSCPS) San Francisco State University San FranciscoCA USA Rua dos Flamboyants 155 Cidade Universitaria Zeferino Vaz Campinas SP 13083-867Brazil

This article analyzed climate change risks from the perspective of con- temporary environmental risks and how they have been internalized by policy. In order to do so, the main characteristics of this type of risk were analyzed based on the contributions from social theory authors on contemporary environmental risks. Next, the implications of these characteristics for the production of policy responses to climate change risks were discussed. The two main types of policy responses to climate change in the literature were presented： mitigation and adaptation. Finally, their interaction, differences and possibilities for synergy were analyzed. Under- standing climate change as a contemporary environmental risk, the way it was presented in this article, implies a radical change in the development bases of society, since greenhouse gases emissions from human activities contribute to the aggravation of global warming. Climate change challenges the traditional ways of governing in many ways, since climate change policy should involve the ques- tioning of the current processes of development. Profound changes in ways of thinking and established political action are needed.

关键词： Climate change risks - Contemporary environmental risks Mitigation Adaptation Climate governance

Competition among rare earth elements on sorption onto six seaweeds

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Journal of Rare Earths 2021年第6期39卷 734-741,I0005页

作者： Joāo Pinto marcelo costa Bruno Henriques JoséSoares Mariana Dias Thainara Viana Nicole ferreira Carlos Vale JoséPinheiro-Torres Eduarda Pereira Department of Chemistry University of Aveiro3810-193 AveiroPortugal CESAM Department of ChemistryUniversity of Aveiro3810-193 AveiroPortugal LAQV-REQUIMTE Department of Chemistry&Central Laboratory of AnalysisUniversity of Aveiro3810-193 AveiroPortugal CIIMAR一Interdisciplinary Centre of Marine and Environmental Research MatosinhosPortugal N9VE-Nature Ocean and ValueLdaPortoPortugal Central Laboratory of Analysis University of Aveiro3810-193 AveiroPortugal

Sorption has been proposed as a promising approach towards a sustainable water decontamination and recently to the recycling of rare earth elements(REE).Although living seaweed have been shown to be capable of removing REE from contaminated solutions,no studies have yet compared the effects of REE competition on sorption onto different groups of *** effects were analysed in the present study by exposing six living seaweeds(Ulva lactuca,Ulva intestinalis,Fucus spiralis,Fucus vesiculosus,Gracilaria *** Osmundea pinnatifida)(3 g/L,fresh weight) to mono-element and multi-element solutions of Y,La,Ce,Pr,Nd,Eu,Gd,Tb and Dy(1 μmol/L).Results show a preference towards light REE in mono-element solutions,which is reduced when in competition with other *** competitive effect is less pronounced in heavy REE indicating that these are still able to bind to the macroalgae despite the presence of competing *** to water content(%),seaweed specific surface area(cm^(2)/g) shows to be an important factor in the sorption of REE,since larger surface area is associated with higher removal and larger competitive effect.

关键词： Bioaccumulation Wastewater e-waste Recovery Removal Marine macroalgae

Analysis of alternative parameters of dynamic resistance measurement in high voltage circuit breakers

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High Voltage 2019年第3期4卷 197-202页

作者： Herbet Filipe dos Santos Sousa Adriano costa de Oliveira George Victor Rocha Xavier Henrique Nunes de Santana Edson Guedes da costa Tarso Vilela ferreira Federal University of Campina Grande Campina GrandeBrazil Federal University of Sergipe AracajuBrazil

Throughout its lifetime,high-voltage circuit breaker(HVCB)contacts suffer from inevitable degradation processes,especially during the formation of electric *** degraded contacts can reduce the current interruption capacity and increase the chances of operational faults,which might lead to considerable financial ***,the use of efficient evaluating techniques is a key factor to achieve systems *** dynamic resistance measurement(DRM)is a technique that can be used to evaluate the degradation level of HVCB'*** stands out from the usual technique,static resistance measurement,by allowing the assessment of both the main contacts and the arcing contacts(ACs).Usually,the mean resistance or the area under the DRM curve is used to estimate the AC ***,DRM is a non-standardised technique and there are no specified parameters to evaluate the real wear ***,an analysis of alternative parameters extractible from the DRM technique is presented in this study,such as amplitude and variance of the DRM *** results attest the possible use of more than one parameter for the continuous evaluation of HVCB ACs,characterising the DRM as a more complete and precise diagnosis tool.

关键词： resistance parameters dynamic

Different no-till grain production systems with Urochloa *** soil microbial community structure,biomass and activity in a tropical Ultisol

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Soil Ecology Letters 2024年第1期6卷 119-129页

作者： Matheus Emannuel Oliveira Vieira Lucas dantas Lopes France Mario costa Viviane Talamini Edson Patto Pacheco marcelo ferreira Fernandes PPGAGRI Universidade Federal de SergipeAv.Marechal Rondons/n-49100-000-Sao CristovaoSEBrazil Embrapa Coastal Tablelands Av Govemador Paulo Barreto de Menezesn°3250-49025-040-AracajuSEBrazil

Integrated grain cropping systems promote soil health(SH)and *** biomass and activity(MBA)and community structure(MCS)are key to *** of maize with Urochloa pastures strongly impacts MBA and *** is more sensitive than MCS to shifts in grain cropping *** under continuous Urochloa increased microbial activity and AMF *** soils are prone to *** of conservation agricultural practices is essential to improve soil health,which is influenced by soil *** this study we analyzed shifts in microbial biomass and activity(MBA)and microbial community structure(MCS)based on fatty acid methyl esthers(FAMEs)between five no-till agricultural practices:maize monoculture(MM);maize annualy intercropped with Urochloa decumbens(M/Ud);M/Ud with soybean rotation every other year(M/Ud-S);M/Ud keeping the pasture for the next two years(M/Ud-Ud-Ud);and maize intercropped with *** keeping the pasture for the next two years(M/Ur-Ur-Ur).Results indicated that MBA was affected by the inclusion of Urochloa intercropping and by rotation with *** under a longer residence time with Urochloa in the field had higherβ-glucosidase activity and soil basal respiration,indicating a greater microbial *** was less affected than MBA by the investigated cropping *** changed only in the continuous pasture systems,which were enriched in arbuscular mycorrhyzal fungi(AMF).Additionally,the continuous pasture systems had lower microbial stress ratios than the other agricultural *** sum,our study showed that utilization of Urochloa *** longer periods in no-till agricultural practices contributes to increase microbial activity,AMF abundance and decrease microbial stress *** changes are primarily beneficial for soil health.

关键词： crop-pasture integration crop rotation no-tillage soil health microbial ecology

Evaluation of the efficiency of urban solid waste management in Brazil by data envelopment analysis and possible variables of influence

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Waste Disposal and Sustainable Energy 2024年第2期6卷 283-295页

作者： Isabel das Merces costa Marta ferreira Dias Margarita Robaina GOvCOPP-Research Unit on Governance Competitiveness and Public Policies and Analyst of UniversidadeEstadual de Feira de SantanaUniversidade de AveiroAveiroPortugal GOvCOPP-Research Unit on Governance Competitiveness and Public PoliciesDEGEIT-Department of EconomicsManagementIndustrial Engineering and TourismUniversidade de AveiroAveiroPortugal

This article has the general objective of estimating the efficiency of urban solid waste management in 940 Brazilian munici-palities through data Envelopment Analysis(DEA)technique and has specific objectives:(i)to estimate efficiency scores;(ii)to compare the performance between different groups of municipalities;and(ii)to analyze the profile of efficient munici-palities from the perspective of the guidelines of Law 12,305/2010 and socio-economic and environmental *** technique used was DEA with output-oriented and variable scale to return *** results showed higher efficiency scores in the municipalities with populations above 500,000 *** score variation ranged from 0.5(municipalities with populations<10,000 inhabitants)to 0.9(municipalities with more than 500,000 inhabitants).Of the sample set,only 12.34%of the municipalities were considered efficient,and when analyzing the efficient group,it was found that adherence to legislation was not a major factor in achieving efficiency.

关键词： Urban solid waste management data envelopment analysis Efficiency Brazil Municipalities

GO FAIR Brazil:A Challenge for Brazilian data Science

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data Intelligence 2020年第1期2卷 238-245,316,317页

作者： Luana Sales Patricia Henning Viviane Veiga Maira Murrieta costa Luis Fernando Sayao Luiz Olavo Bonino da Silva Santos Luis ferreira Pires Instituto Brasileiro em Informacao em Ciencia e Tecnologia Rio de Janeiro-RJ22290-160Brazil Universidade Federal do Estado do Rio de Janeiro Rio de Janeiro-RJ22290-240Brazil Fundacao Oswaldo Cruz Rio de Janeiro-RJ21040-900Brazil Ministerio da Ciencia TecnologiaInovacoes e ComunicacoesEsplanada dos MinisteriosBloco R-BrasiliaDFCEP 70067-900Brazil Comissao Nacional de Energia Nuclear Rua Gal.Severianon 90 Bairro:BotafogoCEP 22290-901-Rio de JaneiroBrazil GO FAIR International Support&Coordination Office(GFISCO) Leiden 2333 AAThe Netherlands University of Twente Enschede 7522 NHThe Netherlands

The FAIR principles,an acronym for Findable,Accessible,Interoperable and Reusable,are recognised worldwide as key elements for good practice in all data management *** understand how the Brazilian scientific community is adhering to these principles,this article reports Brazilian adherence to the GO FAIR initiative through the creation of the GO FAIR Brazil Office and the manner in which they create their implementation *** contextualise this understanding,we provide a brief presentation of open data policies in Brazilian research and government,and finally,we describe a model that has been adopted for the GO FAIR Brazil implementation *** Brazilian Institute of Information in Science and Technology is responsible for the GO FAIR Brazil Office,which operates in all fields of knowledge and supports thematic implementation ***,GO FAIR Brazil-Health is the first active implementation network in operation,which works in all health domains,serving as a model for other fields like agriculture,nuclear energy,and digital humanities,which are in the process of adherence *** report demonstrates the strong interest and effort from the Brazilian scientific communities in implementing the FAIR principles in their research data management practices.

关键词： FAIR principles GO FAIR GO FAIR Brazil Open Science Research data

Soil texture prediction through stratification of a regional soil spectral library

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Pedosphere 2022年第2期32卷 294-306页

作者： José Janderson ferreira costa élvio GIASSON Elisangela Benedet da SILVA Tales TIECHER Antonny Francisco Sampaio DE SENA Ryshardson Geovane Pereira de Oliveira E SILVA Department of Soil Science Faculty of AgronomyUniversity of Rio Grande do SulBento Gonçalves Avenue 7712Porto Alegre 91540-000Brazil Agricultural Research and Rural Extension Corporation of Santa Catarina Rodovia Admar Gonzaga 1347FlorianópolisSanta Catarina 88034-901Brazil

Knowing the spatial distribution of soil texture,which is a physical property,is essential to support agricultural and environmental decision *** texture can be estimated using visible,near infrared,and shortwave infrared(Vis-NIR-SWIR)***,the performance of spectroscopic models is variable because of soil ***,few studies address the effects of soil sample variability on the performance of the models,especially for larger spectral libraries that include soils that are more ***,the objectives of this study were to:i)apply Vis-based color parameters on the stratification of a regional soil spectral library;ii)evaluate the performance of the predictive models generated from the spectral library stratification;iii)compare the performance of stratified models(SMs)and the model without stratification(WSM),and iv)explain possible changes in prediction accuracy based on the ***,a regional soil spectral library with 1535 samples from the State of Santa Catarina,Brazil was *** reflectance data were obtained by Vis-NIR-SWIR spectroscopy in the laboratory using a spectroradiometer covering the 350–2500 nm spectral ***,silt,and clay fractions were determined using the pipette ***-two components of color parameters were derived from the Vis spectrum using the colorimetric models.A cubist regression algorithm was used to assess the accuracy of the applicability of the initial models(SMs and WSM)and of the validation between the *** order derivatives(FODs)at 0.5,1.5,and 2 intervals were used to explain possible changes in the performance of the *** SMs with higher contents of clay and iron oxides obtained the highest accuracy,and the most important spectral bands were identified,mainly in the 480–550 and 850–900 nm ranges and the 1400,1900,and 2200 nm ***,stratification of soil spectral libraries is a good strategy to improve regional assessments of soil resou

关键词： color parameters cubist regression fractional order derivatives soil spectroscopy spectroscopic model stratified model Vis-NIR-SWIR

A Creativity Training Program With Teachers： The Effects on Creativity and Academic Performance of Students With or Without ADHD （Attention Deficit Hyperactivity Disorder）

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Psychology Research 2013年第12期3卷 694-713页

作者： Patricia Villa da costa ferreira Mendonqa Casa Thomas Jefferson Brasilia Brazil