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Leaching process of phosphorus and iron from steelmaking slag into malic acid solution

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Journal of Iron and Steel Research International 2022年第6期29卷 951-960页

作者： ning-ning lv Chang Su Hui Kong Hai-chuan Wang Yuan-chi Dong Key Laboratory of Metallurgical Emission Reduction and Resources Recycling Ministry of EducationAnhui University of TechnologyMa’anshan 243002AnhuiChina School of Metallurgical Engineering Anhui University of TechnologyMa’anshan 243002AnhuiChina

In order to remove phosphorus element from steelmaking slag and decrease iron loss,malic acid was selected as the leaching agent to dissolve steelmaking ***,the influences of different factors,such as malic acid concentration,slag particle size,temperature,liquid/solid ratio and stirring speed,on the leaching ratios of phosphorus and iron were ***,the kinetics for the leaching process of phosphorus was *** results showed that the leaching ratios of phosphorus and iron increase significantly with increasing the malic acid solution concentration and liquid/solid *** the concentration of malic acid solution increases up to 0.01492 mol/L,about 80%phosphorus can be dissolved,and iron leaching ratio is less than 17%.In addition,decreasing slag particle size can obviously increase the leaching ratio of ***,temperature and stirring speed have no significant effect on the dissolution of phosphorus and *** leaching kinetics of phosphorus follows the unreacted shrinking core *** through product layer is the rate-limiting step of the leaching process,and the corresponding apparent activation energy is determined to be 3.32 kJ/***,a semi-empirical kinetic equation was established.

关键词： Leaching process Steelmaking slag Phosphorus Iron Malic acid solution

Size analysis of slag eye formed by gas blowing in ladle refining

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Journal of Iron and Steel Research International 2017年第3期24卷 243-250页

作者： ning-ning lv Liu-shun Wu Hai-chuan Wang Yuan-chi Dong Chang Su School of Metallurgical Engineering Anhui University of Technology Ma'anshan 243032 Anhui China Key Laboratory of Metallurgical Emission Reduction & Resources Recycling Ministry of Education Ma' anshan 243002 AnhuiChina

The formation of slag eye in a gas stirred ladle was studied through cold models and industrial trials. In the cold model,water and sodium tungstate solution were employed to simulate liquid steel,and silicon oil was employed to simulate slag. The simulation results revealed that the gas flow rate and bath height had strong effects on the slag eye size. In particular,the thickness of slag layer played a strong role in the slag eye size. In addition,the slag eye could not be formed when the thickness of the top layer was more than 4 cm in water-silicone oil ***,the section area of vessel had a great impact on the slag eye size. Industrial trials results showed a similar trend that the gas flow rate was very significant on the slag eye size. The predictions of the existing models showed larger predictions deviations compared with the experimental data. Moreover,a new model without fitting parameters was developed based on force balance and mathematical derivation,and verified by the experimental data. The new model provides the prediction with small deviations by comparing with the data acquired from cold models and industrial trials.

关键词： Slag eye Cold model Industrial trial Gas blowing Ladle refining

Phosphine-Relayed Aldehyde-Olefination and Aza-Wittig Reaction with 2,2,2-Trifluorodiazoethane

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Chinese Journal of Chemistry 2018年第8期36卷 723-730页

作者： Fa-Guang Zhang ning lv Yan Zheng Jun-An Ma Department of Chemistry Tianjin Key Laboratory of Molecular Optoelectronic Sciences and Tianjin Collaborative Innovation Center of Chemical Science & Engineering Tianjin University Tianjin 300072 China

Phosphine-relayed olefination and aza-Wittig reactions of readily available aldehydes with 2,2,2-trifluorodiazoethane （CF3CHN2） have been realized. This protocol enables the facile construction of a series of triflu... 详细信息

关键词： diazo compounds olefination Wittig reactions 2,2,2-trifluorodiazoethane phosphine

Effect of high Na2O addition on distribution of phosphorus in lowbasicity converter slag

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Journal of Iron and Steel Research International 2019年第1期26卷 42-51页

作者： Chang Su ning-ning lv Jin-xing Yang Liu-shun Wu Hai-chuan Wang Yuan-chi Dong School of Metallurgical Engineering Anhui University of TechnologyMa'anshan 243032AnhuiChina Key Laboratory of Metallurgical Emission Reduction and Resources Recycling(Anhui University of Technology) Ministry of EducationMa'anshan 243002AnhuiChina

In order to improve the dephosphorization efficiency of low-basicity converter slag and decrease the consumption of solid CaO,the effect of high Na2O addition(0-15 mass%)on the distribution of P2O5 between solid solution and matrix phase was *** thermodynamic properties of slag samples were calculated by FactSage 7.0 ***,the dissolution behavior of phosphorus element from slag was *** results show that the mass fraction of 2CaO*SiO2-2CaO*Na2O*P2O5 solid solution increases when the Na2O content is increased in ***,the amount of formed solid solution changes little when the Na2O addition is more than 10 mass%.Moreover,the content of Na2O in solid solution would reach saturation when adding 15 mass%Na2O into the *** the increase in Na2O content in slag,the distribution ratio of P2O5 between solid solution and matrix phase *** values are evidently higher than the results reported in the ***,the activity of P2O5 in matrix phase and the activity coefficient of P2O5 in solid solution are decreased with increasing the Na2O content in ***,the dissolution ratio of phosphorus in citric acid solution could be improved by adding Na2O into slag,but the increment of dissolution ratio would decrease when the Na2O content exceeds 10 mass%in slag.

关键词： Na2O addition-Low-basicity converter slag Phosphorus distribution ratio Thermodynamic property Phosphorus dissolution behavior

Distribution of P2O5 between solid solution and liquid phase in dephosphorization slag of CaO-SiO2-FeO-P2O5-Na2O system

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Journal of Iron and Steel Research International 2019年第11期26卷 1162-1170页

作者： Chuan-ming Du ning-ning lv Chang Su Wei-ming Liu Jin-xing Yang Hai-chuan Wang Institute of Multidisciplinary Research for Advanced Materials Tohoku UniversitySendaiMiyagi 980-8577Japan School of Metallurgical Engineering Anhui University of TechnologyMa'anshan 243032AnhuiChina Key Laboratory of Metallurgical Emission Reduction and Resources Recycling(Anhui University of Technology) Ministry of Education.Ma'anshan 243002Anhui.China

A multi-phase slag containing Na2O is potential to efficiently dephosphorize high-P hot *** dephosphorization,the generated slag with high P2O5 content is regarded as a P *** P2O5 was mainly concentrated in the 2CaO SiO2-3CaO P2O5 solid solution,the recovery of P from dephosphorization slag primarily depends on the separation of the solid solution from other *** distribution ratios of P2O5 between solid solution and liquid phase in the CaOSiO2-FeO-P2O5-Nslag system were *** results indicated that the addition of Na2O facilitated the enrichment of P2O5 in the solid solution because it increased not only the distribution ratio of P2O5 but also the mass fraction of the solid *** distribution ratio of P2O5 was independent of the P2O5 content in slag.A higher P2O5 content in slag resulted in higher P2O5 and Na2O contents in the solid *** distribution ratio of P2O5 increased with the total Fe content in the liquid phase,regardless of the valence of *** increase in the FeO content in slag brought a higher P2O5 content in the solid *** slag basicity increased,the distribution ratio of P2O5 increased,but the P2O5 content in the solid solution decreased.

关键词： Dephosphorization Steelmaking slag Distribution ratio P2O5 2CaO·SiO2-3CaO·P2O5 solid solution

Effect of annealing treatment on microstructure and mechanical properties of Al/Ni multilayer composites during accumulative roll bonding (ARB) process

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Journal of Iron and Steel Research International 2020年第1期27卷 96-104页

作者： Hui-wen Zhu Bao-yi Yu Hao Zhang Bo-ning Yu Shu-ning lv Li Zheng Run-xia Li School of Material Science and Engineering Shenyang University of TechnologyShenyang 110870LiaoningChina School of Mechanical Engineering Dongguan University of TechnologyDongguan 523808GuangdongChina

Al/Ni multilayer composites are produced by accumulative roll bonding process and then annealed with different temperatures and *** images,microstructure and mechanical properties of Al/Ni multilayer composites are *** for the macroscopic images,although there was an edge crack along the rolling direction at the third pass,the defect of composites was not serious and the forming quality of composites was relatively *** yield strength and elongation of Al/Ni multilayer composites are improved after the annealing treatment;however,with the increase in annealing temperature and time,the yield strength and ciongation of Al/Ni multilayer composites are *** the process of annealing treatment,aluminum atoms diffuse in the way of vacancy diffusion,which results in the formation of Al3Ni intermetallic phase at Al/Ni interface and Kirkendall void in the aluminum *** content of Al3Ni intermetallic phase and Kirkenckill void would increase with the increase in annealing temperature and time.

关键词： Al/Ni multilayer composite Accumulative roll bonding process Annealing treatment Interrnetallic phase

Research progress on naturally-occurring and semi-synthetic ocotillol-type ginsenosides in the genus Panax L.(Araliaceae)

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Chinese Journal of Natural Medicines 2021年第9期19卷 648-655页

作者： NIU Xue-Ni LUO Wen lv Chong-ning LU Jin-Cai Department of Traditional Chinese Medicine Shenyang Pharmaceutical UniversityShenyang 110016China

Ocotillol(OT)-type ginsenosides,one subtype of ginsenosides,consist of a dammarane skeleton and a tetrahydrofuran *** naturally-occurring OT-type ginsenosides exist in Panax species,particularly in Panax quinquefolius,which may be attributed to the warm and humid climate of its native *** now,merely 28 types of naturally-occurring OT-type ginsenosides have been *** contrast,semi-synthesized OT-type ginsenosides are attracted considerable *** ginsenosides can be obtained through oxidation and cyclization of side chains of dammarane-type ginsenosides,and other methods,which may change their physical and chemical properties and further improve their *** is also notable that the pharmacological activities of ginsenosides are closely related to the stereoisomers caused by the configuration at ***-synthesis of OT-type ginsenosides can facilitate our understanding of the biosynthesis,transformation and metabolism of OT-type ginsenosides in the *** review will systematically summarize the research progress on naturally-occurring and semi-synthetic OT-type ginsenosides,which provides a theoretical basis for their bioactivity-guided research.

关键词： Ocotillol-type ginsenosides Panax species Panax quinquefolius Structure-activity relationship

Involvement of NF-κB and the CX3CR1 Signaling Network in Mechanical Allodynia Induced by Tetanic Sciatic Stimulation

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Neuroscience Bulletin 2018年第1期34卷 64-73页

作者： Zhe-Chen Wang Li-Hong Li Chao Bian Liu Yang ning lv Yu-Qiu Zhang Institutes of Brain Science State Key Laboratory of Medical Neurobiology and Collaborative Innovation Center for Brain Science Fudan University Department of Anesthesiology Fudan University Shanghai Cancer Center Department of Oncology Shanghai Medical College Fudan University

Tetanic stimulation of the sciatic nerve （TSS） triggers long-term potentiation in the dorsal horn of the spinal cord and long-lasting pain hypersensitivity. CX3CL1- CX3CR1 signaling is an important pathway in neuronal- microglial activation. Nuclear factor nB （NF-KB） is a key signal transduction molecule that regulates neuroinflamma- tion and neuropathic pain. Here, we set out to determine whether and how NF-~B and CX3CR1 are involved in the mechanism underlying the pathological changes induced by TSS. After unilateral TSS, significant bilateral mechanical allodynia was induced, as assessed by the von Frey test. The expression of phosphorylated NF-nB （pNF-nB） and CX3CR1 was significantly up-regulated in the bilateral dorsal horn. Immunofluorescence staining demonstrated that pNF-κB and NeuN co-existed, implying that the NF-κB pathway is predominantly activated in neurons following TSS. Administration of either the NF-κB inhibitor ammo- nium pyrrolidine dithiocarbamate or a CX3CR1-neutralizing antibody blocked the development and maintenance of neuropathic pain. In addition, blockade of NF-κB down- regulated the expression of CX3CL1-CX3CR1 signaling,and conversely the CX3CRl-neutralizing antibody also down-regulated pNF-rd3. These findings suggest an involvement of NF-κB and the CX3CR1 signaling network in the development and maintenance of TSS-induced mechanical allodynia. Our work suggests the potential clinical application of NF-κB inhibitors or CX3CR 1-neutralizing antibodies in treating pathological pain.

关键词： CX3CR1 Mechanical allodynia NF-κB Tetanic sciatic stimulation Microglia Spinal dorsal horn

End-Output Coupling Efficiency Measurement of Silicon Wire Waveguides Based on Correlated Photon Pair Generation

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Chinese Physics Letters 2013年第7期30卷 92-95页

作者： lv ning ZHANG Wei GUO Yuan ZHOU Qiang HUANG Yi-Dong PENG Jiang-De State Key Laboratory on Integrated Optoelectronics Tsinghua National Laboratory for Information Science and TechnologyDepartment of Electronic EngineeringTsinghua UniversityBeijing 100084

A method to measure the end-output coupling efficiencies between silicon wire waveguides(SWWs)and optical fibers is proposed and *** end-output coupling efficiency is calculated through four measured counting rates based on the correlated photon pair generation in the *** provides a way to investigate and optimize the coupling processes at the input and output end of the optical waveguides separately.

关键词： Efficiency optical waveguides