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Nano-Micro Letters 2025年第2期17卷 376-386页

作者： Wei-Min Qin Zhongliang li Wen‑Xia Su Jia‑Min Hu Hanqin Zou Zhixuan Wu Zhiqin Ruan Yue‑Peng Cai kang li Qifeng Zheng School of Chemistry South China Normal UniversityGuangzhou 510006People’s Republic of China Key Laboratory of Functional Metal‑Organic Compounds of Hunan Province College of Chemistry and Material ScienceHengyang Normal UniversityHengyang 421008People’s Republic of China Guangzhou Key Laboratory of Energy Conversion and Energy Storage Materials Guangzhou 510006People’s Republic of China

Porous organic cages(POCs)with permanent porosity and excellent host–guest property hold great potentials in regulating ion transport behavior,yet their feasibility as solid-state electrolytes has never been testified in a practical ***,we design and fabricate a quasi-solid-state electrolyte(QSSE)based on a POC to enable the stable operation of li-metal batteries(LMBs).Benefiting from the ordered channels and cavity-induced anion-trapping effect of POC,the resulting POC-based QSSE exhibits a high li+transference number of 0.67 and a high ionic conductivity of 1.25×10^(−4) S cm^(−1) with a low activation energy of 0.17 *** allow for homogeneous li deposition and highly reversible li plating/stripping for over 2000 *** a proof of concept,the LMB assembled with POC-based QSSE demonstrates extremely stable cycling performance with 85%capacity retention after 1000 ***,our work demonstrates the practical applicability of POC as SSEs for LMBs and could be extended to other energy-storage systems,such as Na and K batteries.

关键词： Porous organic cage Cavity-induced anion-trapping Quasi-solid-state electrolyte Homogeneous li+flux lithium metal battery

Analysis of the anti-T2DM components in dichloromethane fraction of Schisandra sphenanthera and its mechanism

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Traditional Medicine Research 2025年第1期10卷 27-43页

作者： Shi-Bo Feng Hai-Hui Jiang Hui-li kang Yi Jiang Hua-Wei Zhang Xiao-Mei Song Yu-Ze li Wen-li Huang Dong-Dong Zhang Chong Deng School of Pharmacy Shaanxi University of Chinese MedicineXianyang 712046China School of Pharmacy and Shaanxi Qinling Application Development and Engineering Center of Chinese Herbal Medicine Shaanxi University of Chinese MedicineXianyang 712046China Key Laboratory for Research and Development of“Qin Medicine”of Shaanxi Administration of Traditional Chinese Medicine Xianyang 712046China Shaanxi Key Laboratory of Research and Application of“Taibai Qi Yao” Xianyang 712046China

Background:The type 2 diabetes mellitus(T2DM)pharmacodynamic study of various parts of Schisandra sphenanthera was conducted in the previous stage,and it was found that dichloromethane extracted part(SDP)had a significant hypoglycemic ***,the components of SDP were analyzed,and the specific mechanism of its anti-T2DM was ***:We used a high-fat,high-sugar diet in combination with streptozotocin to induce a T2DM rat model,and the model rats were divided into two groups according to body weight and blood ***,oral glucose tolerance test,fasting blood glucose,low density lipoprotein cholesterol,superoxide dismutase,insulin,glycated hemoglobin,total cholesterol,nonesterified free fatty acids,alanine aminotransferase,high-density lipoprotein cholesterol,aspartate aminotransferase,malondialdehyde,and glutathione peroxidase were measured,organ indices were calculated,and pathological sections of pancreas and liver were *** 16S rRNA V3–V4 region of intestinal flora was sequenced to explore the effect of SDP on biochemical indicators and intestinal *** on the above indicators,the anti-T2DM mechanism of SDP in Schisandra sphenanthera was ***:After six weeks of administration,the biochemical indices of diabetic rats were diminished compared to the control *** SDP could significantly increase the gut microbialα-diversity index,resulting in significant changes in the flora of T2DM rats,with increased richness and diversity,reduced harmful flora,and significantly back-regulated the levels of acetic acid,propionic acid,and butyric ***:SDP can improve the symptoms associated with elevated blood glucose,dyslipidemia,elevated fasting insulin levels,and damaged glucose tolerance in *** against T2DM may be through the control of intestinal flora to normalize and exert anti-diabetic effect;its main active components may be lignans and terpenoids.

关键词： Schisandra sphenanthera T2DM intestinal flora HPLC

Primary parenchymal squamous cell carcinoma of the kidney:A case report

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World Journal of Clinical Cases 2025年第4期13卷 34-40页

作者： Zhi-Hui Zheng Bo Shao Chao-Min Xu Ke Wang Jia-Zhu Wen li-kang Luo Jia-Cheng Guan Department of Ultrasound The Second People’s Hospital of QuzhouQuzhou 324000Zhejiang ProvinceChina Department of Radiology Shulan(Quzhou)HospitalQuzhou 324000Zhejiang ProvinceChina Department of Radiology The Second People’s Hospital of QuzhouQuzhou 324000Zhejiang ProvinceChina Department of Pathology The Second people’s Hospital of QuzhouQuzhou 324000Zhejiang ProvinceChina

BACKGROUND Primary squamous cell carcinoma(SCC)of the renal parenchyma is extremely rare,with only nine cases *** SUMMARY This study reports a 51-year-old man with primary SCC of the renal *** patient was admitted with recurrent dull pain and discomfort in the right lumbar region,which had worsened over 2 weeks,accompanied by painful gross *** antigen(SCCA)levels were elevated,and imaging revealed a renal mass with associated *** patient underwent laparoscopic unilateral nephrectomy and lymph node *** pathology confirmed highly differentiated SCC with necrosis in the right renal parenchyma,with negative renal pelvis and *** pathological stage was *** months after surgery,the tumor recurred with involvement of the liver,right psoas major muscle,and inferior vena *** patient refused chemotherapy and succumbed to the disease 6 months postoperatively due to disease *** We report a case of primary SCC of the renal parenchyma,a rare renal *** clinical symptoms,laboratory tests,and imaging findings are nonspecific,making accurate and timely diagnosis *** to the literature,for patients with renal calculi accompanied by a renal mass,elevated serum SCCA levels,and magnetic resonance imaging showing cystic or cystic-solid masses within the kidney with pseudocapsules and heterogeneous mild enhancement,the possibility of this disease should be considered.

关键词： Renal tumor Renal parenchyma Squamous cell carcinoma Renal calculi Computed tomography Case report

Synthesis, Crystal Structure and Antimicrobial Property of 4-Bromo-2-[(3-methypyridin-2-ylimino)methyl]phenol

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Chinese Journal of Structural Chemistry 2008年第2期27卷 230-232页

作者： ZHANG li li kang-Lan Institute of Green Chemistry Experiment and Teaching Lanzhou City University Lanzhou 730070 China

The title Schiff base compound 4-bromo-2-[（3-methylpyridin-2-ylimino）methyl]phenol was prepared and structurally characterized by elemental analysis, IR spectrum, and single-crystal X-ray diffraction. The crystal belongs to monoclinic, space group P2 1/n, with a = 4.4870（9）, b = 19.953（4）, c = 13.860（3）A, β = 93.13（3）°, V = 1239.0（4）A3 Z = 4, Dc = 1.561 g/cm3, C13H11BrN2O2 , Mr = 291.15, p = 3.302 mm-1 and F（000） = 584. The final refinement gave R = 0.0608 and wR = 0.1377 for 1329 observed reflections with I 〉 2σ（I）. X-ray diffraction reveals that the non-hydrogen atoms in the compound are nearly coplanar, with the mean deviation of 0.0197A from the plane. The molecule adopts an E configuration about the central C=N functional bond. The compound possesses moderate antimicrobial property.

关键词： Schiff base synthesis crystal structure antimicrobial

Thermodynamic investigation of phase equilibria in Al–Si–V system

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Journal of Materials Science & Technology 2018年第9期34卷 1592-1601页

作者： Qun Luo kang li Qian li State Key Laboratory of Advanced Special Steel & Shanghai Key Laboratory of Advanced Ferrometallurgy & School of Materials Science and Engineering Shanghai UniversityShanghai 200072 China Materials Genome Institute Shanghai UniversityShanghai 200444 China Shanghai Institute of Materials Genome Shanghai 200444 China

The Al-Si-V system is assessed to understand the phase equilibria of V-containing（3 d transition metal）Al-Si alloys, which are generally of great importance for technical applications. Four annealed alloys were prepared to study the phase equilibria of Al-rich corner（V ≤ 23.3 at.%, Si ≤ 57.6 at.%） in the temperature range of 500-930 ℃. The microstructure and phase constituents of the samples were determined by X-ray diffraction（XRD） and scanning electron microscopy（SEM） equipped with energy dispersive X-ray spectrometer（EDS）, The existence of ternary phase τ（Al（0.6） Si（1.4） V, TiSi2-type） was confirmed with the composition ranging from 17.98 to 18.59 at.% Al and 48.89-49.20 at.% Si. However, it did not equilibrate with fcc（Al） below 868℃, which was determined by differential scanning calorimetry（DSC）. The Si3 V5 appeared in Al58 5 Si（18.3） V（23.2） and Al64 7 Si（20.2） V（15.1） alloys annealed at 500 ℃. It nearly disappeared after3000 h-annealing and its thermodynamic stability was discussed. According to the measured phase relationships, the thermodynamic description of Al-Si-V system was optimized combing with the enthalpies of formation of binary and ternary compounds obtained by density functional theory（DFT）. The Si-V system was modified to obtain the congruent liquidus of Si3 V5 and enthalpy of formation of Si3 V5 and Si2 V with experimental data. By comparing the calculated phase equilibria and phase transitions with experimental data, it showed that a good agreement was reached. The description of Al-Si-V system could be used to guide the development of Al-Si alloys.

关键词： Phase equilibrium Al-Si alloy CALPHAD method Intermetallic compounds Enthalpy of formation

Development of EPDM composites reinforced by CNTs@SiO_(2)for thermal protection systems of aerospace propulsion:Significant improvement in oxidation and ablation resistance properties

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Chinese Journal of Aeronautics 2024年第2期37卷 471-481页

作者： li WANG Jiang li kang li Yiwei WANG Chenyang MA Science and Technology on Combustion Internal Flow and Thermal-Structure LaboratoryNorthwestern Polytechnical UniversityXi’an 710072China

Carbon Nanotubes(CNTs)reinforced Polymer-Matrix Composites(PMCs)is widely used as insulation materials in thermal protection system of aerospace ***,CNTs are prone to oxidation and have high thermal conductivities,which makes it difficult to improve the ablation resistance of insulation materials that contain ***_(2)was encapsulated onto the surface of CNTs(CNTs@SiO_(2)),which were then added to Ethylene Propylene Diene Monomer(EPDM)rubber to prepare the insulation *** analysis and ablation test were used to evaluate the resistance of the insulation materials to thermal oxidation and ***,scanning electron microscopy was performed to analyze their *** revealed that the addition of CNTs@SiO_(2)could visibly reduce the effects of hot corrosion and ablation on insulation *** C-CNTs@SiO_(2)-1 formulation had the best ablative ***,compared with the unencapsulated formulation(C-CNTs-10),the C-CNTs@SiO_(2)-1 formulation reduced the line ablation rate by 51%to 0.0130 mm/s after oxygen-acetylene ***,the ablation mechanism was investigated based on the effects of the CNTs@SiO_(2)additive on their ***,the improvement in ablation performance may be attributed to CNTs@SiO_(2)-induced decreases in thermal conductivity,improvement in the hot corrosion resistance in the char layer,and changes in the microstructure.

关键词： Polymer-Matrix Composites(PMCs) Carbon Nanotubes(CNTs) Thermal properties Ablation Oxidation

RP-HPLC Determination and Pharmacokinetic Comparison of Cinnamic Acid in Rat Plasma After Administration of Di-Gu-Pi Decoction and Pure Cinnamic Acid

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Chemical Research in Chinese Universities 2006年第1期22卷 56-60页

作者： li kang BI Kai-shun Department of Pharmacy Shenzhen Hospital Beijing University Shenzhen 518036 P.R. China College of Pharmacy Shenyang Pharmaceutical University Shenyang 110016 P.R. China

A sensitive, simple, and accurate method was developed for the determination and pharmacokinetic comparison of cinnamic acid in rat plasma after the administration of a Traditional Chinese Medicinal preparation, Di-Gu-Pi decoction, and pure cinnamic acid using RP-HPLC. Di-Gu-Pi was extracted with 5% aqueous sodium bicarbonate, which was followed by purification with ion exchange column chromatography. The plasma samples taken from rats were deproteinized with methanol. The reversed-phase （HPLC） system with a Diamonsil C18 column and methanol-acetonitfile-water （8： 32： 60, volume ratio）（adjusted to pH = 3.0 with glacial acetic acid） as the mobile phase was employed for the separation of cinnamic acid in the plasma samples. The detection was set at 272 nm and 3-（p-fluoro-phenyl）-2-propenoic acid was chosen as the internal standard. The calibration curve was linear in a range from 0. 10 to 25.0μg/mL （R2 = 0. 9988, n = 9）. The precision was 3.42%-10. 10%; the between-day precision was 2. 84%-8.91% ; the accuracy was - 1.51%-1.26% ; the mean recovery was 99. 9%. The method was found to be sensitive, simple, accurate and appropriate for the determination of cinnamic acid.

关键词： Di-Gu-Pi decoction Cinnamic Acid Pharmacokinetics RP-HPLC

Real-time object tracking via compressive feature selection

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Frontiers of Computer Science 2016年第4期10卷 689-701页

作者： kang li Fazhi HE Xiao CHEN School of Computer Science Wuhan University Wuhan 430072 China

Recently, compressive tracking （CT） has been widely proposed for its efficiency, accuracy and robustness on many challenging sequences. Its appearance model employs non-adaptive random projections that preserve the structure of the image feature space. A very sparse measurement matrix is used to extract features by multiplying it with the feature vector of the image patch. An adaptive Bayes classifier is trained using both positive samples and negative samples to separate the target from background. On the CT frame- work, however, some features used for classification have weak discriminative abilities, which reduces the accuracy of the strong classifier. In this paper, we present an online compressive feature selection algorithm（CFS） based on the CT framework. It selects the features which have the largest margin when using them to classify positive samples and negative samples. For features that are not selected, we define a random learning rate to update them slowly, It makes those weak classifiers preserve more target information, which relieves the drift when the appearance of the target changes heavily. Therefore, the classifier trained with those discriminative features couples its score in many challenging sequences, which leads to a more robust tracker. Numerous experiments show that our tracker could achieve superior result beyond many state-of-the-art trackers.

关键词： object tracking compressive sensing supervised learning real-time

Juvenile hormone signaling-a mini review

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Insect Science 2019年第4期26卷 600-606页

作者： kang li Qiang-Qiang Jia Sheng li Guangzhou Key Laboratory of Insect Development Regulation and Application Research Institute of Insect Science and Technology&School of Life SciencesSouth China Normal UniversityGuangzhouChina

Since it was first postulated by Wigglesworth in 1934, juvenile hormone (JH) is considered a status quo hormone in insects because it prevents metamorphosis that is initiated by the molting hormone 20-hydroxyecdysone (20E). During the last decade, significant advances have been made regarding JH signaling. First, the bHLH-PAS transcription factor Met/Gce was identified as the JH intracellular receptor. In the presence of JH, with the assistance of Hsp83, and through physical association with a bHLH?PAS transcriptional co-activator, Met/Gce enters the nucleus and binds to E-box-like motifs in promoter regions of JH primary?response genes for inducing gene expression. Second, the zinc finger transcription factor Kr-hl was identified as the anti-metamorphic factor which transduces JH signaling. Via Kr-hl binding sites, Kr-hl represses expression of 20E primary?response genes (i.e. Bi\ E93 and E5) to prevent 20E-induced metamorphosis. Third, through the intracellular signaling, JH promotes differ ent aspects of female reproduction. Nevertheless, this action varies greatly from species to species. Last, a hypothetical JH membrane receptor has been predicted to be either a GPCR or a tyrosine kinase receptor. In future, it will be a great challenge to understand how the JH intracellular receptor Met/Gce and the yet unidentified JH membrane receptor coordinate to regulate metamorphosis and reproduction in insects.

关键词： intracellular receptor juvenile hormone (JH) Kr-h 1 membrane receptor Met/Gce metamorphosis reproduction

Distribution of Equilibrium Free Energies in a Thermodynamic System with Broken Ergodicity

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Communications in Theoretical Physics 2008年第3期49卷 659-664页

作者： ZHOU Hai-Jun li kang Institute of Theoretical Physics the Chinese Academy of Sciences Beijing 100080 China

At low temperatures the configurational phase space of a macroscopic complex system （e.g., a spin-glass） of N - 10^23 interacting particles may split into an exponential number Ωs - exp（const × N） of ergodic sub-spaces （thermodynamic states）. It is usually assumed that the equilibrium collective behavior of such a system is determined by its ground thermodynamic states of the minimal free-energy density, and that the equilibrium free energies follow the distribution of exponentied decay. But actually for some complex systems, the equilibrium free-energy values may follow a Gaussian distribution within an intermediate temperature range, and consequently their equilibrium properties are contributed by excited thermodynamic states. Based on this analysis, the re-weighting parameter y in the cavity approach of spin-glasses is easily understood. Depending on the free-energy distribution, the optimal y can either be equal to or be strictly less than the inverse temperature β.

关键词： free-energy distribution spin-glass thermodynamic state cavity approach broken ergodicity